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At least 613 records · Page 34

Development of a Point of Care Technology for Military Medical Applications in Austere Environments

NASA, Lawrence Livermore National Laboratory (LLNL) and the Department of Defense (DoD) share a common interest in compact medical diagnostic technologies—also known as “point of care testing” (POCT) technologies. For NASA, the need is to take care of astronauts on deep space missions. For LLNL, the focus is on technologies needed to support homeland security applications. For DoD, the need is to support warfighters in military theaters of operation, especially for prolonged field care and en route care. A recently patented technology, “Portable Medical Diagnosis Instrument” (U.S. Patent 9824870), co-invented by NASA and LLNL, is being developed further in a partnership between NASA, LLNL and Travis Air Force Base, with a focus on military applications. This instrument, the NASA-LLNL Medical Tricorder, can be used for a wide range of clinical samples including breath, saliva and blood. One component of the Tricorder is the NASA E-Nose, a carbon nanotube-based chemical sensor, integrated into a hand-held smart phone, that can detect and measure “breath biomarkers” in the gas phase of exhaled breath. The response of the NASA E-Nose is rapid, which makes it possible to detect various gas-phase substances in real time. The NASA E-Nose, with modification, can also be used for breath condensate analysis. Another component of the Tricorder is a miniaturized microfluidic analyzer, under development by LLNL, that does not require any pumps. The microfluidic analyzer can detect and measure biomarkers in liquid samples, such as blood, saliva and breath condensate. This microfluidic system requires small quantities of liquid sample and can perform analysis very rapidly (seconds to minutes), which makes it possible to detect relevant biomarkers in near real time in the field. The Clinical Investigation Facility (CIF) at Travis Air Force Base is currently conducting research with the goal to develop improved field-able technologies and procedures for the emergency response to life threatening injuries soldiers may receive in theater. This work includes experimental large animal systems and comprehensive collection of clinical specimens and physiological data. NASA and LLNL are partnering with Travis to test and further develop the Tricorder technology for high priority military applications, initially focused on lung injury models and traumatic brain injury.

Loftus, David J.↗

xEMU Suit Integrated Audio Communications System: Ambient and EVA Pressure Testing System Performance

Testing across several airlock and EVA thermal and pressure scenarios has demonstrated that the Integrated Audio System of NASA’s Exploration Extravehicular Mobility Unit (xEMU) spacesuits transmits and receives intelligible audio communications without the use of a commcap or similar worn device. The xEMU audio system consists of internal loudspeakers and digital microphones (Integrated Communications System –ICS) combined with an adaptive Acoustic Echo Canceller (AEC), outbound voice operated transmission (VOX), and automatic gain control (AGC). Transducers are mounted in an “exploded commcap” configuration with helmet-attached speakers near the ears and three microphones positioned at the collar. The AGC removes inbound audio signals (e.g.,suit, Mission Control, Lander, C&W tones) from the outbound comms stream, reducing echo and feedback (squeal) in low-noise suit environments. The reduction of worn communication equipment increases crewmember comfort, range of movement, and situational awareness. However, test results also highlight the need for proper fan, duct, pump, and gas flow integration with suit acoustics and audio. Ductwork may serve as waveguides for various component and structure-borne noise. Sharply angled ducts can generate turbulent-flow noise. Gas flow from inlets above the crewmember’s head can generate noise when cascading over the faceplate and collar (or commcap) microphones. Sufficient acoustic noise levels (1) require increased gain to boost inbound audio, and (2) may distort signals resulting in AEC disruption or artifacts. Suit-noise levels decline with reduced pressure (density), but then elevated speech and audio effort/power become necessary. Whether the Integrated Audio System, commcap, or other device is used, suit acoustic noise can mask speech in outbound comms. This reduces intelligibility and requires other AECs/devices to suppress comms noise. Yet, adjusting a few components may yield significant improvement. We discuss xEMU audio functionality, demonstrate how acoustical treatment combined with inbound signal conditioning improved clarity during tests, and discuss future modifications.

xEMU↗

xEMU Suit Integrated Audio Communications System: Ambient and EVA Pressure Testing System Performance

Testing across several airlock and EVA thermal and pressure scenarios has demonstrated that the Integrated Audio System of NASA’s Exploration Extravehicular Mobility Unit (xEMU) spacesuits transmits and receives intelligible audio communications without the use of a commcap or similar worn device. The xEMU audio system consists of internal loudspeakers and digital microphones (Integrated Communications System –ICS) combined with an adaptive Acoustic Echo Canceller (AEC), outbound voice operated transmission (VOX), and automatic gain control (AGC). Transducers are mounted in an “exploded commcap” configuration with helmet-attached speakers near the ears and three microphones positioned at the collar. The AGC removes inbound audio signals (e.g.,suit, Mission Control, Lander, C&W tones) from the outbound comms stream, reducing echo and feedback (squeal) in low-noise suit environments. The reduction of worn communication equipment increases crewmember comfort, range of movement, and situational awareness. However, test results also highlight the need for proper fan, duct, pump, and gas flow integration with suit acoustics and audio. Ductwork may serve as waveguides for various component and structure-borne noise. Sharply angled ducts can generate turbulent-flow noise. Gas flow from inlets above the crewmember’s head can generate noise when cascading over the faceplate and collar (or commcap) microphones. Sufficient acoustic noise levels (1) require increased gain to boost inbound audio, and (2) may distort signals resulting in AEC disruption or artifacts. Suit-noise levels decline with reduced pressure (density), but then elevated speech and audio effort/power become necessary. Whether the Integrated Audio System, commcap, or other device is used, suit acoustic noise can mask speech in outbound comms. This reduces intelligibility and requires other AECs/devices to suppress comms noise. Yet, adjusting a few components may yield significant improvement. We discuss xEMU audio functionality, demonstrate how acoustical treatment combined with inbound signal conditioning improved clarity during tests, and discuss future modifications.

xEMU↗

Seismic monitoring of CO 2 geosequestration using multi-well 4D DAS VSP: Stage 3 of the CO2CRC Otway project

An important part of any CO 2 geosequestration project is to ensure CO 2 containment and conformance in the subsurface. This is generally done by implementing a comprehensive, risk-based Measurement, Monitoring and Verification plan, a key element of which is active time-lapse seismic monitoring. However, high cost and environmental impact of the standard surface seismic monitoring dictate the need for a cost-effective and environmentally friendly alternative. An opportunity to develop such method emerges with advances in distributed acoustic sensing (DAS) technology, which turns an optical fibre into a seismic sensor with dense spatial sampling. DAS can be permanently deployed in multiple wells across the geosequestration site providing a robust and non-intrusive network of seismic receivers. This approach was developed and tested in the CO2CRC Otway project, where injection of 15 kt of CO 2 at 1.5 km depth was monitored with a 4D vertical seismic profiling (VSP) using five borehole DAS arrays and mobile vibroseis sources. The 4D DAS VSP in each of the five wells provides broadly consistent images of the CO 2 plume with some differences due to different illumination of the target horizon, lateral variation of velocities, and seismic anisotropy. When the newly injected CO 2 reaches a CO 2 plume created as a result of an earlier injection into the same formation ~600 m updip, 4D DAS VSP shows a change in reflectivity in that area and beyond. Furthermore, this shows a potential of 4D DAS VSP for monitoring gas injection into gas-saturated reservoirs.

58 GEOSCIENCES↗

Broccoli seed extract rich in polysaccharides and glucoraphanin ameliorates DSS ‐induced colitis via intestinal barrier protection and gut microbiota modulation in mice

Abstract BACKGROUND Broccoli has received widespread attention because of its anti‐inflammatory and antioxidant effects. The present study aimed to explore the composition of broccoli seed extract (BSE) and its effect on colitis induced by dextran sulfate sodium (DSS). RESULTS BSE mainly comprises glucoraphanin and polysaccharides composed of arabinose, galactose, glucose and mannose. Animal experiments suggested that BSE intervention effectively reversed body weight loss, suppressed the levels of proinflammatory interleukin‐6, tumor necrosis factor‐α and interleukin‐1β, and elevated the levels of anti‐inflammatory interleukin‐10 and the activities of superoxide dismutase and glutathione in DSS‐induced colitis mice. According to histopathologic and immunohistochemical analysis of colon tissue, BSE intervention may repair the intestinal barrier by upregulating mRNA levels and the expression of tight junction proteins (claudin‐1, occludin and zonula occludens‐1). Gas chromatography–mass spectrometry (MS) analysis demonstrated that cecal short‐chain fatty acids in mice with BSE administration were significantly increased compared with the model group. Sulforaphane and sulforaphane‐ N ‐acetylcysteine were only detected in BSE group mice by ultra‐performance liquid chromatography‐MS analysis. In addition, BSE intervention evidently increased the abundance of Alistipeds , Coriobacteriaceae UCG‐002 and Bifidobacterium and decreased the abundance of Escheichia‐Shinella , Lachnospiraceae others , Parabacteroides , Ruminococcaceae others and Turicibacter , which possibly promoted carbohydrate metabolism and short‐chain fatty acid production. CONCLUSION The present study aimed to elucidate the effect of BSE on colitis and found that BSE, as a novel food ingredient, has great potential for the improvement of colitis. © 2022 Society of Chemical Industry.

Wu, Jiaying↗

Parametric Inlet Tested in Glenn's 10- by 10-Foot Supersonic Wind Tunnel

The Parametric Inlet is an innovative concept for the inlet of a gas-turbine propulsion system for supersonic aircraft. The concept approaches the performance of past inlet concepts, but with less mechanical complexity, lower weight, and greater aerodynamic stability and safety. Potential applications include supersonic cruise aircraft and missiles. The Parametric Inlet uses tailored surfaces to turn the incoming supersonic flow inward toward an axis of symmetry. The terminal shock spans the opening of the subsonic diffuser leading to the engine. The external cowl area is smaller, which reduces cowl drag. The use of only external supersonic compression avoids inlet unstart--an unsafe shock instability present in previous inlet designs that use internal supersonic compression. This eliminates the need for complex mechanical systems to control unstart, which reduces weight. The conceptual design was conceived by TechLand Research, Inc. (North Olmsted, OH), which received funding through NASA s Small-Business Innovation Research program. The Boeing Company (Seattle, WA) also participated in the conceptual design. The NASA Glenn Research Center became involved starting with the preliminary design of a model for testing in Glenn s 10- by 10-Foot Supersonic Wind Tunnel (10 10 SWT). The inlet was sized for a speed of Mach 2.35 while matching requirements of an existing cold pipe used in previous inlet tests. The parametric aspects of the model included interchangeable components for different cowl lip, throat slot, and sidewall leading-edge shapes and different vortex generator configurations. Glenn researchers used computational fluid dynamics (CFD) tools for three-dimensional, turbulent flow analysis to further refine the aerodynamic design.

Slater, John W.↗

X-ray Computed Tomography of Irradiated and Unirradiated AGR-3/4 Compacts

X-ray Computed Tomography (XCT) has been utilized to image and characterize compacts from the combined third and fourth irradiation of the Advanced Gas Reactor (AGR) Program, AGR-3/4, fuel. The experiment contained tristructural isotropic (TRISO)-coated fuel particles as well as designed-to-fail (DTF) fuel particles. Two irradiated compacts, representing the lower and higher range of AGR-3/4 burnup (4.85% and 14.92% fissions per initial heavy metal atom FIMA) were examined. These represent the first known highly irradiated TRISO fuel compacts to be examined via X-ray CT. Additionally, two unirradiated compacts from the same production batch as the examined irradiation compacts were also imaged for a baseline comparison. As XCT of irradiated TRISO compacts is not a commonly implemented characterization technique, a significant portion of the report focuses on developed methodology and imaging conditions. A specialized sample shielding device was developed and fabricated specifically to limit received dose to staff during sample preparation for XCT and to minimize excess gamma radiation dose to sensitive electronic components with the utilized X-ray system. Significant penetration through the uranium oxycarbide fuel kernels by significantly hardening the X-ray beam with specialized proprietary filters acquired from Carl Zeiss NTS Ltd. The filter utilized resulted in an average X ray photon energy of ~110 keV which approaches uranium’s K-edge (~115 keV), maximizing penetration for a microfocus X-ray source. The gamma-radiation emitted from the irradiated AGR-3/4 TRISO compacts, has the same properties and mechanisms for interaction with matter as X-rays, thus the detection of gamma-radiation by the utilized X-ray detectors was initially a concern. However, although ?-rays did produce an observable signal on the X-ray detector, its contribution to the overall imaging results appeared negligible upon 3D reconstruction. The neglibile impact on the resulting 3D reconstructed volumes were likely the result of: (1) a significantly lower detection efficiency for ?-rays relative to X-rays; (2) An X-ray flux at the detector several orders of magnitude higher than that of the impinging ?-rays from the irradiated compacts. These results suggest that irradiated compacts with significantly higher radiation fields can be examined in the future if an acceptable route for sample handling and preparation can be determined. Additionally, the 3D imaging results of XCT can provide a valuable means of assessing compacts. While in many ways complimentary to traditional post irradiation examination techniques such as optical ceramography, XCT can provide additional insight into compact features traditionally difficult to discern directly from cross-sectional imaging alone. Preliminary analyses on kernel size, morphology (aspect ratio and sphericity), and kernel orientation were presented. Sphericity, a simple morphological shape descriptor, was utilized to screen for kernel extrusions within the high burnup compact. The number of kernel extrusions identified via XCT represented an approximate two-fold increase from the quantity of extruded particles observed (via optical ceramography) in adjacent compacts from the same irradiation capsule. While numerical analysis of the compact datasets was highly preliminary, initial results show promise for providing complimentary metrics to current AGR-3/4 PIE and potentially additional insight into the processes driving TRISO fuel degradation during reactor operation. Additional analyses to be performed at a later date include a more detailed examination of kernel size, kernel sphericity (and observed kernel extrusions), and sphericity. Given all particles can be observed in a single data volume possible correlation of spatial position with observed kernel features will also be made at a later date.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Development of a PEMFC Power System with Integrated Balance of Plant

Autonomous Underwater Vehicles (AUV s) have received increasing attention in recent years as military and commercial users look for means to maintain a mobile and persistent presence in the undersea world. Compact, neutrally buoyant power systems are needed for both small and large vehicles. Batteries are usually employed in these applications, but the energy density and therefore the mission duration are limited with current battery technology. At a certain energy or mission duration requirement, other means to get long duration power become feasible. For example, above 10 kW-hrs liquid oxygen and hydrogen have better specific energy than batteries and are preferable for energy storage as long as a compact system of about 100 W/liter is achievable to convert the chemical energy in these reactants into power. Other reactant forms are possible, such as high pressure gas, chemical hydrides or oxygen carriers, but it is essential that the power system be small and light weight. Recent fuel cell work, primarily focused on NASA applications, has developed power systems that can meet this target power density. Passive flow-through systems, using ejector driven reactant (EDR) flow, integrated into a compact balance of plant have been developed. These systems are thermally and functionally integrated in much the same way as are automotive, air breathing fuel cell systems. These systems fit into the small volumes required for AUV and future NASA applications. Designs have been developed for both a 21" diameter and a larger diameter (LD) AUV. These fuel cell systems occupy a very small portion of the overall energy system, allowing most of the system volume to be used for the reactants. The fuel cell systems have been optimized to use reactants efficiently with high stack efficiency and low parasitic losses. The resulting compact, highly efficient fuel cell system provides exceptional reactant utilization and energy density. Key design variables and supporting test data are presented. Future development activities are described.

Wynne, B.↗

Leveraging the bioeconomy for carbon drawdown

Stringent climate change mitigation scenarios rely on large-scale drawdown of carbon dioxide from the atmosphere. Amongst drawdown technologies, bioenergy with carbon capture and sequestration (BECCS) has received considerable attention in the climate mitigation literature. Recently, attention has shifted further from a relatively narrow focus on BECCS to a broader focus on Biomass Carbon Removal and Storage (BiCRS). The concept of BiCRS has the potential to enable a future where the climate mitigation value of biomass resources is more valuable than the energy value, due to the potential to remove and sequester large quantities atmospheric CO2. This article provides a qualitative overview of prominent BiCRS technologies from which a set of the most promising technologies are assessed quantitively through life cycle assessment. There are numerous opportunities to incorporate carbon removal and management within the bioeconomy, but the majority of immediate carbon removal potential exists in four bioproducts: bioenergy, bioplastics, biochar, and wood products. We analyze the life cycle greenhouse gas emissions and disposition of sequestered carbon over 10 000 years for four bioproducts representative of each broader category: an advanced BECCS pathway, biopolyethylene, oriented strand board, and biochar soil amendment. We find that the BECCS pathway has the greatest magnitude and durability of CO2 storage over all time horizons. However, non-BECCS pathways achieve 34–64% of the drawdown magnitude relative to BECCS and retain 55–67% of their initial drawdown over 100 years (central estimate). We identify three engineering strategies for enhancing carbon drawdown: reducing biomass supply chain emissions, maximizing carbon stored in long-lived products, and extending the term of carbon storage. Finally, we highlight the need to characterize both the magnitude and permanence of carbon drawdown as a means for policymakers and technology developers to deploy limited biomass resources to maximize mitigation benefits.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

A Burning Rate Emulator (BRE) for Study in Microgravity

A gas-fueled burner, the Burning Rate Emulator (BRE), is used to emulate condensed-phase fuel flames. The design has been validated to easily measure the burning behavior of condensed-phase fuels by igniting a controlled stream of gas fuel and diluent. Four properties, including the heat of combustion, the heat of gasification, the surface temperature, and the laminar smoke point, are assumed to be sufficient to define the steady burning rate of a condensed-phase fuel. The heat of gasification of the fuel is determined by measuring the heat flux and the fuel flow rate. Microgravity BRE tests in the NASA 5.2 s drop facility have examined the burning of pure methane and ethylene (pure and 50 in N2 balance). Fuel flow rates, chamber oxygen concentration and initial pressure have been varied. Two burner sizes, 25 and 50 mm respectively, are chosen to examine the nature of initial microgravity burning. The tests reveal bubble-like flames that increase within the 5.2s drop but the heat flux received from the flame appears to asymptotically approach steady state. Portions of the methane flames appear to locally detach and extinguish at center, while its shape remains fixed, but growing. The effective heat of gasification is computed from the final measured net heat flux and the fuel flow rate under the assumption of an achieved steady burning. Heat flux (or mass flux) and flame position are compared with stagnant layer burning theory. The analysis offers the prospect of more complete findings from future longer duration ISS experiments.

diffusion flames↗

Leveraging the bioeconomy for carbon drawdown

Stringent climate change mitigation scenarios rely on large-scale drawdown of carbon dioxide from the atmosphere. Amongst drawdown technologies, bioenergy with carbon capture and sequestration (BECCS) has received considerable attention in the climate mitigation literature. Recently, attention has shifted further from a relatively narrow focus on BECCS to a broader focus on Biomass Carbon Removal and Storage (BiCRS). The concept of BiCRS has the potential to enable a future where the climate mitigation value of biomass resources is more valuable than the energy value, due to the potential to remove and sequester large quantities atmospheric CO 2 . This article provides a qualitative overview of prominent BiCRS technologies from which a set of the most promising technologies are assessed quantitively through life cycle assessment. There are numerous opportunities to incorporate carbon removal and management within the bioeconomy, but the majority of immediate carbon removal potential exists in four bioproducts: bioenergy, bioplastics, biochar, and wood products. We analyze the life cycle greenhouse gas emissions and disposition of sequestered carbon over 10,000 years for four bioproducts representative of each broader category: an advanced BECCS pathway, biopolyethylene, oriented strand board, and biochar soil amendment. We find that the BECCS pathway has the greatest magnitude and durability of CO 2 storage over all time horizons. However, non-BECCS pathways achieve 34–64% of the drawdown magnitude relative to BECCS and retain 55–67% of their initial drawdown over 100 years (central estimate). We identify three engineering strategies for enhancing carbon drawdown: reducing biomass supply chain emissions, maximizing carbon stored in long lived products, and extending the term of carbon storage. Finally, we highlight the need to characterize both the magnitude and permanence of carbon drawdown as a means for policymakers and technology develo pers to deploy limited biomass resources to maximize mitigation benefits.

09 BIOMASS FUELS↗

A Review of Monitoring Technologies for Trace Air Contaminants in the International Space Station

NASA issued a Request For Information (RFI) to identify technologies that might be available to monitor a list of air pollutants in the ISS atmosphere. After NASA received responses to the RFI, an expert panel was assembled to hear presentations from 9 technology proponents. The goal of the panel was to identify technologies that might be suitable for replacement of the current Volatile Organics Analyzer (VOA) within several years. The panelists consisted of 8 experts in analytical chemistry without any links to NASA and 7 people with specific expertise because of their roles in NASA programs. Each technology was scored using a tool that enabled rating of many specific aspects of the technology on a 4-point system. The maturity of the technologies ranged from well-tested instrument packages that had been designed for space applications and were nearly ready for flight to technologies that were untested and speculative in nature. All but one technology involved the use of gas chromatography for separation, and there were various detectors proposed including several mass spectrometers and ion mobility spectrometers. In general there was a tradeoff between large systems with considerable capability to address the target list and smaller systems that had much more limited capability.

James, John T.↗

Coatings for Oxidation and Hot Corrosion Protection of Disk Alloys

Increasing temperatures in aero gas turbines is resulting in oxidation and hot corrosion attack of turbine disks. Since disks are sensitive to low cycle fatigue (LCF), any environmental attack, and especially hot corrosion pitting, can potentially seriously degrade the life of the disk. Application of metallic coatings are one means of protecting disk alloys from this environmental attack. However, simply the presence of a metallic coating, even without environmental exposure, can degrade the LCF life of a disk alloy. Therefore, coatings must be designed which are not only resistant to oxidation and corrosion attack, but must not significantly degrade the LCF life of the alloy. Three different Ni-Cr coating compositions (29, 35.5, 45wt. Cr) were applied at two thicknesses by Plasma Enhanced Magnetron Sputtering (PEMS) to two similar Ni-based disk alloys. One coating also received a thin ZrO2 overcoat. The coated samples were also given a short oxidation exposure in a low PO2 environment to encourage chromia scale formation. Without further environmental exposure, the LCF life of the coated samples, evaluated at 760C, was less than that of uncoated samples. Hence, application of the coating alone degraded the LCF life of the disk alloy. Since shot peening is commonly employed to improve LCF life, the effect of shot peening the coated and uncoated surface was also evaluated. For all cases, shot peening improved the LCF life of the coated samples. Coated and uncoated samples were shot peened and given environmental exposures consisting of 500 hrs of oxidation followed by 50 hrs of hot corrosion, both at 760C). The high-Cr coating showed the best LCF life after the environmental exposures. Results of the LCF testing and post-test characterization of the various coatings will be presented and future research directions discussed.

LCF life↗

Empirical correlations for prediction of minimum miscible pressure and near-miscible pressure interval for oil and CO 2 systems

Although near-miscible CO 2 flooding has recently received considerable attention, no criteria are available to predict its applicability to a specific reservoir. Evaluating the viability of near-miscible flooding requires experimental exploration of a specific region in pressure–temperature space. The near-miscible pressure field is bounded on one side in P, T space by the MMP (minimum miscible pressure). This paper provides robust empirical correlations to estimate the MMP for both pure and impure CO 2 and for prediction of the near-miscible pressure region for CO 2 -oil. Many slim tube analyses, lacking high density data points, systematically underestimate the MMP, when the near miscible region is not accounted for. They are based on 147 published data sets that include: slim tube experimental determination of MMP; interfacial tension (IFT) between oil and CO 2 ; concentration of solution gas; and purity of the CO 2 . This paper is the first to begin a systematic exploration of the pressure-temperature space within which near-miscible effects characterize CO 2 floods. Our new correlations provide a basis for identifying and investigating the nature of near miscible effects associated with existing CO 2 floods. For a case study of an offshore field we determined that lower and upper pressure boundaries for effective near-miscible flooding, are 0.87 MMP and 1.07 MMP at reservoir temperatures. The proposed model is the first empirical correlation for the prediction of near-miscible pressure region, it will provide the basis for both screening the relative potential of oil reservoirs for economically viable miscible or near-miscible CO 2 -flooding.

42 ENGINEERING↗

Multipurpose Thermal Insulation Test Apparatus

A multi-purpose thermal insulation test apparatus is used for testing insulation materials, or other components. The test apparatus is a fluid boil-off calorimeter system for calibrated measurement of the apparent thermal conductivity (k-value) of a specimen material at a fixed vacuum level. The apparatus includes an inner vessel for receiving a fluid with a normal boiling point below ambient temperature, such as liquid nitrogen, enclosed within a vacuum chamber. A cold mass assembly, including the inner vessel and thermal guards, is suspended from the top of the vacuum chamber. Handling tools attach to the cold mass assembly for convenient manipulation of the assembly and for the installation or wrapping of insulation test materials. Liquid nitrogen is typically supplied to the inner vessel using a fill tube with funnel. A single port through the top of the vacuum chamber facilitates both filling and venting. Aerogel composite stacks with reflective films are fastened to the top and the bottom of the inner vessel as thermal guards. The comparative k-value of the insulation material is determined by measuring the boil-off flow rate of gas, the temperature differential across the insulation thickness, and the dimensions (length and diameters) of the test specimen.

Fesmire, James E.↗

Effects of Various Heat Treatments on the Ballistic Impact Properties of Inconel 718 Investigated

Uncontained failures of aircraft engine fan blades are serious events that can cause equipment damage and loss of life. Federal Aviation Administration (FAA) certification requires that all engines demonstrate the ability to contain a released fan blade with the engine running at full power. However, increased protection generally comes at the expense of weight. Proper choice of materials is therefore imperative to an optimized design. The process of choosing a good casing material is done primarily through trial and error. This costly procedure could be minimized if there was a better understanding of the relationships among static material properties, impact properties, and failure mechanisms. This work is part of a program being conducted at the NASA Glenn Research Center at Lewis Field to study these relationships. Ballistic impact tests were conducted on flat, square sheets of Inconel 718 that had been subjected to different heat treatments. Two heat treatments and the as-received condition were studied. In addition, results were compared with those from an earlier study involving a fourth heat treatment. The heat treatments were selected on the basis of their effects on the static tensile properties of the material. The impact specimens used in this study were 17.8-cm square panels that were centered and clamped over a 15.2-cm square hole in a 1.27-cm-thick steel plate. Three nominal plate thickness dimensions were studied, 1.0, 1.8, and 2.0 mm. For each thickness, all the specimens were taken from the same sheet of material. The projectile was a Ti-6Al-4V cylinder with a length of 25.4 mm, a diameter of 12.7 mm, and a mass ranging from 14.05 to 14.20 g. The projectiles were accelerated toward the specimens at normal incidence using a gas gun with a 2-m-long, 12.7-mm inner-diameter barrel. The ballistic limit for each heat treatment condition and thickness was determined by conducting a number of impact tests that bracketed as closely as possible the velocity required to penetrate the specimen.

Pereira, J. Michael↗

LCF Life of As-Deposited and Annealed NiCr-Y Coatings for Oxidation and Hot Corrosion Protection of Disk Alloys

Increasing temperatures in aero gas turbines is resulting in oxidation and hot corrosion attack of turbine disks. Since disks are sensitive to low cycle fatigue (LCF), any environmental attack, and especially hot corrosion pitting, can seriously degrade the life of the disk. Application of metallic coatings is one means of protecting disk alloys from this environmental attack. However, the presence of a metallic coating can degrade the LCF life of a disk alloy. Therefore, coatings must be designed which are not only resistant to oxidation and corrosion attack, but do not significantly degrade the LCF life of the alloy.Three different NiCr-Y coating compositions (29, 35.5, 44 wt.% Cr, all with 0.1 wt.% Y) were applied at two thicknesses by Plasma Enhanced Magnetron Sputtering (PEMS) to two similar Ni-based disk alloys. One Ni-35.5Cr-0.1Y coating also received a thin ZrO2 overcoat. The coated samples were also given a short thermal anneal in a low PO2 environment to encourage bonding of the coating and substrate as well as initiating formation of a chromia scale. Without further environmental exposure, the LCF life of coated and uncoated samples was evaluated at 760°C in air. The LCF lifetime of all coated samples was less than that of uncoated samples. The LCF life scaled with the Cr content and the high-Cr, thin coating showed the highest LCF life. Pre and post-test characterization of the various coatings, including identification of crack initiation sites, will be presented and the effect of the coating on the LCF life discussed.

low cycle fatigue↗

L'CO/LFIR Relations with CO Rotational Ladders of Galaxies Across the Herschel SPIRE Archive

We present a catalog of all CO (carbon monoxide) (J (total angular momentum quantum number) equals 1-0 through J equals 13-12), [CI], and [NII] lines available from extragalactic spectra from the Herschel SPIRE (Spectral and Photometric Imaging Receiver) Fourier Transform Spectrometer (FTS) archive combined with observations of the low-J CO lines from the literature and from the Arizona Radio Observatory. This work examines the relationships between L (sub FIR (Far Infra Red)), L prime (sub CO), and L (sub CO) / L (sub CO, 1-0). We also present a new method for estimating probability distribution functions (PDFs) from marginal signal-to-noise ratio Herschel FTS spectra, which takes into account the instrumental "ringing" and the resulting highly correlated nature of the spectra. The slopes of Log (L (sub FIR)) versus Log (L prime (sub CO)) are linear for all mid- to high-J CO lines. The mid- to high-J CO luminosity relative to CO J equals 1-0 increases with increasing L (sub FIR), indicating higher excitement of the molecular gas, though these ratios do not exceed approximately 100. The luminosities relative to CO J equals 1-0 remain relatively at from J equals 6-5 through J equals13-2, across many orders of magnitude of L (sub FIR). Qualitative comparisons to current theoretical models do not match these flat SLED (spectral line energy distributions) shapes, indicating the need for more comprehensive modeling of the excitation processes of warm molecular gas in nearby galaxies.

Submillimeter Data↗