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At least 613 records · Page 34

Standoff Detection of Chemical Plumes Using Swept-ECQCL Remote Detection Technology: Results from EMRTC Complex Terrain Dual Tracer Experiment

As part of the Complex Terrain Dual Tracer Experiments performed in support of the LYNM program, a swept-wavelength external cavity quantum cascade laser (swept-ECQCL) remote detection system was deployed to measure chemical plume propagation with high temporal resolution. The swept-ECQCL remote detection technology was initially developed at PNNL, and is now under further development at Opticslah, LLC under SBIR funding from DOE (DOE SBIR Phase I Project DE-SC0019855, Remote Detection Technologies, Program Manager Chris Ramos). The swept-ECQCL technology provides a single-frequency infrared laser source which is rapidly scanned over a large wavelength range to measure the infrared absorption of gases, liquids, or solids. Analysis of the measured infrared absorption spectrum is used to detect, identify, and quantify the chemical species which are present. While most previous laser-based techniques used small wavelength tuning ranges to measure only a few isolated spectral lines of a few species, the swept-ECQCL provides the large tuning range needed to measure multiple species simultaneously, and to detect broad absorption features from large molecules or condensed phase materials. In addition, the swept-ECQCL systems have high enough spectral resolution and sensitivity to measure narrow lines of small molecules and determine isotope ratios. The remote detection system for gas plumes is based on the swept-ECQCL technology, and consists of a swept-ECQCL source, infrared detector, control electronics, and beam transmitting and alignment optics. The remote detection system directs the infrared output of the swept-ECQCL to a target retro reflector typically located at ~10-10,000 m distance. The swept-ECQCL wavelength is varied continuously over a large wavelength range (>1000 nm) at rates up to 1000 Hz. The swept ECQCL light reflected from the remote target is collected and focused onto an infrared photodetector. By measuring the detector signal continuously as the swept-ECQCL wavelength is varied, a time-series of absorption spectra are measured for the gases along the beam line of-sight. Based on analysis and fitting of the measured absorption spectra, the time-dependent chemical concentrations of species are determined. Multiple species and mixtures can be detected simultaneously, for all species with absorption features above the sensor noise floor. The sensor output is thus a continuous, high-speed record of identified chemicals along with their concentrations and isotope ratios of interest. The high-speed operation enables low-noise operation in conditions of atmospheric turbulence and allows tracking of fluctuating concentrations in transient chemical plumes as needed for reliable remote detection applications. All components operate with minimal cooling requirements and no cryogens are needed. In addition, the output infrared light is invisible with an intensity below the maximum permissible exposure (MPE) threshold of 100 mW/cm2 for these infrared wavelengths and thus eye safe. The measurement concept for plume detection using the swept-ECQCL remote detection system is as follows. The ECQCL beam is directed toward a remote retro-reflector, which reflects the beam back to the ECQCL system where it is focused onto an infrared photodetector. The line-of-sight from the ECQCL system to the retro-reflector defines the measurement path. The detected infrared signal is recorded continuously and detects the absorption of molecular species along the measurement path. Before a plume release, the system measures absorption from atmospheric constituents, which in this LWIR band consist primarily of lines from H 2 O and CO 2 , with additional weaker absorption from N 2 O, NH 3 , and O 3 possibly contributing. The system then measures any changes in absorption due to the tracer compounds when they enter the measurement path. The shape of absorption features is used to distinguish and identify the different tracer compounds, and the strength of the absorption is used to determine the path-integrated concentration – also called the column density.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Maximizing RHIC Deliverable Luminosity with Dynamic Telescopic Beta* Squeeze

To benefit fully from the exceptional performance of the Relativistic Heavy Ions Collider (RHIC) Stochastic Cooling system during heavy ions physics store, the betatron amplitude β ∗ at a given col lision point (IP) can be squeezed from its design value by using the available space in the quadrupole triplets from smaller beam emittances. This should allow reaching new heights in deliverable lumi nosity for both STAR and PHENIX experiments. Prior to 2014, RHIC lattice designs only squeezed the interaction regions (IR’s) down to β ∗ = 0.70 m. To get past this limitation, one can use a telescopic scheme where the non-experimental insertions surrounding STAR and PHENIX are used to generate and close a β-beat wave contributing to the final squeeze in the two IP’s of interest. The following presents the various steps of the implementation in RHIC of this telescopic scheme and the corresponding changes in collision rates and specific luminosity. A full feasibility study with a review of hardware and beam dynamics limitations is also included.

43 PARTICLE ACCELERATORS↗

Determination of oxygen in silicon and carbide by activation with 27.2 meV alpha particles

The Si sample was polished on one side, and on the other side Ni was applied chemically and soldered with Pb to a water cooled Cu substrate. Optical quartz standard was fixed from the other side. Si carbide samples were soldered to a substrated with In. The prepared samples were irradiated in a cyclotron with a 27.2 MeV alpha particle beam. The layers were removed from the Si and Si carbide samples by grinding and the positron activity of F-18(t sub 1/2 110 min) was measured by using a gamma, gamma coincidence spectrometer with two NaI(TI) crystals. For analysis of Si carbide, the activity decay curve of the samples was recorded to find the contribution of the positron activity of Cu-65(t sub 1/2 12.9 hr) which formed from Ni impurity on irradiation.

Dolgolenko, A. P.↗

A two-dimensional analysis of laser heat addition in converging nozzles

The two-dimensional equations of motion describing the interaction between a laser beam and a flowing gas are considered. An implicit numerical scheme is used to solve these equations for unchoked flow through a converging-diverging nozzle. Separate grids are used for the fluid dynamics and the radiation equations. The effects of beam focusing and cross-beam intensity profiles are included. The calculations are based upon real gas properties for all quantities except the gas absorptivity, which is taken as a constant. The solutions contain the expected hot central core region with cool gas near the walls. This results in steep temperature gradients in both the streamwise and cross-stream directions. The absorption zone acts as a blockage in the nozzle causing a nonuniform velocity profile at the inlet and an overall decrease in mass flow. The absorption region also forces the streamlines to move away from the axis of symmetry, although this effect is not strong.

Molvik, G. A.↗

Solar power absorption in a glass tube

The optics of a glass tube to be used in near-Earth space at the focus of a solar concentrator has been examined, and an equation for the power absorbed from multiple-reflected light beams in the tube wall has been developed. The equation has been used to calculate the power absorbed by a highly transmissive form of fused silica. The equilibrium temperature reached by the tube with only radiative cooling has also been examined, and it shows a significant rise with large solar concentrations. The results apply specifically to cylindrical containment vessels for space-based solar-pumped lasers and generally to any similarly irradiated tubes.

Williams, Michael D.↗

A space qualified thermal imaging system using a Pt Si detector array

EDO Corporation, Barnes Engineering Division designed and constructed a high resolution thermal imaging system on contract to Lockheed for use in the SDI Star Lab. This employs a Pt Si CCD array which is sensitive in the spectral range of 3 to 5 microns. Star Lab will be flown in the Shuttle bay and consists basically of a large, reflecting, tracking telescope with associated sensors and electronics. The thermal imaging system is designed to operate in the focal plane of this telescope. The configuration of the system is illustrated. The telescope provides a collimated beam output which is focussed onto the detector array by a silicon objective lens. The detector array subtends a field of view of 1.6 degrees x 1.22 degrees. A beam switching mirror permits bypassing the large telescope to give a field of 4 degrees x 3 degrees. Two 8 position filter wheels are provided, and background radiation is minimized by Narcissus mirrors. The detector is cooled with a Joule-Thompson cryostat fed from a high pressure supply tank. This was selected instead of a more convenient closed-cycle system because of concern with vibration. The latter may couple into the extremely critical Starlab tracking telescope. The electronics produce a digitized video signal for recording. Offset and responsivity correction factors are stored for all pixels and these corrections are made to the digitized output in real time.

Astheimer, Robert W.↗

Fe-Ti-Cr-Oxides in Martian Meteorite EETA79001 Studied by Point-counting Procedure Using Raman Spectroscopy

Fe-Ti-Cr-Oxide minerals contain much information about rock petrogenesis and alteration. Among the most important in the petrology of common intrusive and extrusive rocks are those of the FeO-TiO2-Cr2O3 compositional system chromite, ulv spinel-magnetite, and ilmenite-hematite. These minerals retain memories of oxygen fugacity. Their exsolution into companion mineral pairs give constraints on formation temperature and cooling rate. Laser Raman spectroscopy is anticipated to be a powerful technique for characterization of materials on the surface of Mars. A Mars Microbeam Raman Spectrometer (MMRS) is under development. It combines a micro sized laser beam and an automatic point-counting mechanism, and so can detect minor minerals or weak Raman-scattering phases such as Fe- Ti-Cr-oxides in mixtures (rocks & soils), and provide information on grain size and mineral mode. Most Fe-Ti-Cr-oxides produce weaker Raman signals than those from oxyanionic minerals, e.g. carbonates, sulfates, phosphates, and silicates, partly because most of them are intrinsically weaker Raman scatters, and partly because their dark colors limit the penetration depth of the excitation laser beam (visible wavelength) and of the Raman radiation produced. The purpose of this study is to show how well the Fe-Ti-Cr-oxides can be characterized by on-surface planetary exploration using Raman spectroscopy. We studied the basic Raman features of common examples of these minerals using well-characterized individual mineral grains. The knowledge gained was then used to study the Fe-Ti-Cr-oxides in Martian meteorite EETA79001, especially effects of compositional and structural variations on their Raman features.

Wang, Alian↗

Rhenium Mechanical Properties and Joining Technology

Iridium-coated rhenium (Ir/Re) provides thermal margin for high performance and long life radiation cooled rockets. Two issues that have arisen in the development of flight Ir/Re engines are the sparsity of rhenium (Re) mechanical property data (particularly at high temperatures) required for engineering design, and the inability to directly electron beam weld Re chambers to C103 nozzle skirts. To address these issues, a Re mechanical property database is being established and techniques for creating Re/C103 transition joints are being investigated. This paper discusses the tensile testing results of powder metallurgy Re samples at temperatures from 1370 to 2090 C. Also discussed is the evaluation of Re/C103 transition pieces joined by both, explosive and diffusion bonding. Finally, the evaluation of full size Re transition pieces, joined by inertia welding, as well as explosive and diffusion bonding, is detailed.

Reed, Brian D.↗

Development of a Space Irradiance Simulator for Advanced Studies and Materials Research

A lab-scale experimental apparatus that mimics the solar-thermal environment of space has recently been developed and tested at NASA Kennedy Space Center in support of novel materials research for future space science and exploration applications. The Space Irradiance Simulator (SIRS) apparatus exposes specimens up to roughly 61 mm in diameter to a similar thermal environment that exists at distances as close as 0.4 AU from the Sun. This includes a high vacuum environment, access to a deep cryogenic background temperature with optical properties that closely imitate a blackbody, and irradiance from a broadband solar “point” source at fluxes as high as 9300 W/m2. Cooling is provided by a Gifford-McMahon cryocooler capable of 25 W of cooling power at 20 K, with a base temperature of 14 K. A commercially available Xeon lamp acts as the solar source, creating broadband electromagnetic radiation with a spectrum similar to that of the Sun. Light is beamed through the vacuum chamber and onto a sample suspended within the cold-mass via a flexible quartz fiber bundle in conjunction with a custom vacuum feedthrough. The system design, fabrication, and operation are discussed; and results from the initial checkout testing of the system are presented.

A. M. Swanger↗

Combining molecular beam epitaxy and low-energy electron microscopy with in situ magnetic susceptibility measurements within an integrated ultrahigh vacuum system

Quantum two-dimensional materials, including ultrathin superconducting films, are of great current research interest. These films are typically fabricated under ultra-high vacuum (UHV) conditions and are sensitive to the environment—prone to oxidation and contamination when exposed to the atmosphere. This hampers the study of their intrinsic properties by standard ex situ techniques. Here, we present a variable-temperature mutual inductance probe system integrated under UHV with molecular beam epitaxy (MBE) synthesis and low-energy electron microscopy, enabling nondestructive in situ characterization of superconducting thin films. The system employs a reflection-type configuration and reaches a low temperature (∼4 K) using a high-cooling-power, vibration-isolated cryocooler. In conclusion, we demonstrate the system performance by measuring the superconducting critical temperature in a copper-oxide thin film.

2D materials↗

Uncertainty Quantification of Monolithic Tungsten Target Block Fatigue

The current STS spallation target design consists of 21 water cooled, tantalum clad, monolithic tungsten blocks. The target wheel assembly rotates such that each target block receives a direct proton pulse every 1.4 seconds (21 blocks / 15 Hz pulses). The quasi-steady heating induced by the repetitive beam pulses creates a significant mean stress distribution in the target. On top of this, the rapid energy deposition from a proton pulse induces dynamic stress waves that are of the same order of magnitude as the mean stresses. Over the design goal of 5,000 operational hours per year for a decade, each target must withstand over 130 million repetitions of these dynamic stress events. The fatigue life prediction of the target blocks is a complex sequence of simulations that depend upon a set of input parameters. For the tungsten block, the end goal is the fatigue factor-of-safety (FOS). This study documents a new structural analysis routine using software available to U.S. national laboratories (e.g. CUBIT, Sierra Multiphysics, Dakota) that enables more rapid target fatigue analysis. The increased throughput is amenable to parameter sensitivity and uncertainty quantification (UQ) studies. A set of input parameters (ultimate strength, fatigue strength, density, elastic modulus, Poisson’s ratio, thermal conductivity, coefficient of thermal expansion, specific heat, flow rate) with expected ranges are documented based on literature data, recent experimental testing, and engineering judgement. UQ bounds the resulting fatigue FOS at [0.5, 3.4] using epistemic interval analysis. These bounds are expected to be wider due to model effects (discretization) and beam effects (focus, offset) that were not included. Parameter sensitivity underscores the importance of ultimate strength and fatigue strength of irradiated tungsten on the fatigue calculations.

43 PARTICLE ACCELERATORS↗

Description of A 2.3 kW power transformer for space applications

The paper describes the principal features and special testing of a high-frequency high-power low-specific-weight (0.57 kg/kW) 2.3-kW electronic power transformer developed for space applications. The transformer is operated in a series resonant inverter supplying beam power to a 30-cm mercury ion thruster. High efficiency (above 98.5%) is obtained through careful detailed design. A number of unique heat removal techniques are discussed which control the winding temperature using only the available conductive cooling.

Hansen, I.↗

Sunlight-Pumped Laser

Organic iodide gas is stimulated by portion of Sun's spectrum to emit laser light. Chopper forms pulses from beam of Xenon-Arc light. Chopper is only necessary to avoid buildup of laser-quenching species in sealed tube of present experiment. Perfluoropropyliodide lasing medium functions at temperatures of about 670 K, a fact that reduces cooling requirements in space.

Weaver, W. R. J.↗

Observations of Far-Infrared Molecular Emission Lines from the Orion Molecular Cloud

The Orion Nebula was the subject of intensive study for over one hundred years. Recently, several far infrared transitions among the low-lying levels of OH were observed toward IRc2. The OH is thought to be abundant, and plays an important role in the chemical evolution of shock and post-shock regions. The OH emission serves as a sensitive probe of the temperature and density for the shock-processed gas. A rigorous treatment of the radiative transfer of these measured transitions was performed using the escape probability formalism. From this analysis, the temperature of the OH-emitting region was determined to be on the order of 40K. This suggests that the gas is part of the post-shock gas that has cooled sufficiently, most likely by way of radiative cooling by CO. Such cooling from shock temperatures of several degrees can be accomplished in 100 years. A molecular hydrogen density of 3 million/cubic cm and an OH column density of 1.0 x 10 to the 17th /sq cm is found. The beam filling factor is determined to be 36%.

Viscuso, P. J.↗

High power phase locked laser oscillators

The feasibility of mechanizing an adaptive array of independent laser oscillators for generation of a high power coherent output was experimentally investigated. Tests were structured to evaluate component/system requirements for delivery of energy to a low-earth orbit satellite. Initial experiments addressed the control issues of phase locking unstable resonators at low power levels. A successful phase lock demonstration formed the basis for the design and fabrication of the high power, water-cooled, control mirror subsequently installed in the NASA LeRC high power laser. Tests were performed to characterize the operational limits of the laser system and included quantitative assessment of the frequency stability, noise sources, and optical properties of the beam.

Hayes, C. L.↗

Validation of multi-temperature nozzle flow code NOZNT

A computer code NOZNT (Nozzle in n-Temperatures), which calculates one-dimensional flows of partially dissociated and ionized air in an expanding nozzle, is tested against five existing sets of experimental data. The code accounts for: a) the differences among various temperatures, i.e., translational-rotational temperature, vibrational temperatures of individual molecular species, and electron-electronic temperature, b) radiative cooling, and c) the effects of impurities. The experimental data considered are: 1) the sodium line reversal and 2) the electron temperature and density data, both obtained in a shock tunnel, and 3) the spectroscopic emission data, 4) electron beam data on vibrational temperature, and 5) mass-spectrometric species concentration data, all obtained in arc-jet wind tunnels. It is shown that the impurities are most likely responsible for the observed phenomena in shock tunnels. For the arc-jet flows, impurities are inconsequential and the NOZNT code is validated by numerically reproducing the experimental data.

Park, Chul↗

Design of a High Flux Beam Characterization Device for Falling Particle Receivers

This paper outlines the design and error analysis for a flux characterization device (i.e. flux wand) which traverses the aperture of a falling particle receiver cavity providing the incident power measurement needed for the calculation of receiver efficiency without significantly disrupting receiver output. The design features a linear actuator, water cooled extension arm, and refractory bar. The refractory bar/flux wand is a diffusely reflective surface which reflects light as it is translated across the receiver aperture to provide a light intensity distribution that is correlated to a measured flux. The component sizing, constrained by a typical 30 frame per second camera and a 4-point average of the measured reflectance, is presented. Simulation reveals the error that results from a 5% variation in flux wand reflectance is within 4% of the true value.

Schroeder, Nathan↗

Using DUNE to shed light on the electromagnetic properties of neutrinos

We study future DUNE sensitivity to various electromagnetic couplings of neutrinos, including magnetic moments, milli-charges, and charge radii. The DUNE PRISM capabilities play a crucial role in constraining the electron flavored couplings. We find that DUNE will be able to place the strongest beam based constraint on the muon-neutrino magnetic moment by improving on LSND’s bounds by roughly a factor of two, although Borexino’s constraint from solar neutrinos will be stronger. For the muon neutrino millicharge DUNE can place the leading beam based bound, with two orders of magnitude improvement compared to the existing COHERENT constraint, suggesting that DUNE can be useful for light mediators more generally. Despite this strength, the millicharge bounds are not competitive with strong bounds from stellar cooling, beta-decay, and matter stability. Finally, DUNE may be able to test the SM prediction for the muon neutrino charge radius, by placing a constraint two times better than CHARM-II and CCFR experiments.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗