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At least 595 records · Page 33

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NASA NTRS1982

Some characteristics of polymers in composite materials and as electrical conductors

The characteristics of carbon fibers (CF) made from polyacrylonitrile (PAN) materials are discussed, together with research on conducting polymers. CF materials have better mechanical properties, chemical inertness, and higher stiffness than metallic materials but are subject to environmental instability, flammability, and delamination fatigue. Polymerization procedures for the monopolymer PAN are described, noting the use of SEM and X-ray diffraction techniques for studying the fiber structure. High modulus and strength of CF are caused by covalent sp(2) bonds in hexagonal carbon rings, which are stronger than the same links in diamonds. Details of the molecular chain structures and macroformations, stress-strain as a function of temperature, and thermosetting and glass transition temperatures of polymers are provided. Computational quantum chemistry techniques are being applied to studying electrical conductance in polymers, mainly to discover ways to stabilize the materials. Doped CH(x) has exhibited photovoltaic properties and other polymers have become superconductors at cryogenic temperatures.

Hansen, C. F.↗

NASA NTRS1984

Experiments with phase transitions at very high pressure

A diamond anvil cell is described which was developed for studying hydrogen and other materials to pressure above 100 PGa, including measurements at low temperature. The benefits of X-ray diffraction using synchrotron radiation and using a fixed anode source are examined as well as the optimization of X-ray diffraction at low temperature. A Ge diode detector was incorporated into apparatus for measuring optical absorption, reflectance, and fluorescence in order to enable luminescence studies and Raman spectra were obtained. Results of experiments on Si, Ge, GaP, InAs, hydrogen, benzene, nitrogen, graphite, and the superconductor CeCu2Si2 are given.

Spain, I. L.↗

NASA NTRS1984

A flying superconducting magnet and cryostat for magnetic suspension of wind-tunnel models

The engineering practicality of a persistent high-field superconducting solenoid cryostat as a magnetic suspension and balance system (MSBS) for wind-tunnel testing of aircraft and missile models is examined. The test apparatus is a simple solenoid of filamentary NbTi superconductor with a cupronickel matrix. The apparatus, with a length-to-diameter ratio of 6 to 1 and a radius of 32 mm, used a 0.25 mm wire with a critical current of 27 A in an external field of 6 T. The total heat inleak of 150 mW was achieved. Helium boiloff rates were tested over a range of operating conditions, including pitch attitudes from 10 deg nose down to 90 deg nose up; the rate was estimated as low, but the aerodynamic acceptability of venting gaseous helium has not been determined. It is shown that the effectiveness of the concept increases with increasing scale, and performance in excess of that of conventional ferromagnets is achievable with reduction in size and costs, and with aptness to transonic wind-tunnel testing. Detailed specifications and schematics are included.

Britcher, C.↗

NASA NTRS1985

Superconducting magnet

Extensive computer based engineering design effort resulted in optimization of a superconducting magnet design with an average bulk current density of approximately 12KA/cm(2). Twisted, stranded 0.0045 inch diameter NbTi superconductor in a copper matrix was selected. Winding the coil from this bundle facilitated uniform winding of the small diameter wire. Test coils were wound using a first lot of the wire. The actual packing density was measured from these. Interwinding voltage break down tests on the test coils indicated the need for adjustment of the wire insulation on the lot of wire subsequently ordered for construction of the delivered superconducting magnet. Using the actual packing densities from the test coils, a final magnet design, with the required enhancement and field profile, was generated. All mechanical and thermal design parameters were then also fixed. The superconducting magnet was then fabricated and tested. The first test was made with the magnet immersed in liquid helium at 4.2K. The second test was conducted at 2K in vacuum. In the latter test, the magnet was conduction cooled from the mounting flange end.

Source record↗

NASA NTRS1987

Three-Axis Superconducting Gravity Gradiometer

Gravity gradients measured even on accelerating platforms. Three-axis superconducting gravity gradiometer based on flux quantization and Meissner effect in superconductors and employs superconducting quantum interference device as amplifier. Incorporates several magnetically levitated proof masses. Gradiometer design integrates accelerometers for operation in differential mode. Principal use in commercial instruments for measurement of Earth-gravity gradients in geo-physical surveying and exploration for oil.

Paik, Ho Jung↗

NASA NTRS1986

Superconducting gravity gradiometer for space and terrestrial applications

A three-axis superconducting gravity gradiometer with a potential sensitivity better than Eotvos per sq root Hz is currently under development for applications in space. Although such a high sensitivity may be needed for only a limited number of terrestrial applications, superconductivity offers many extraordinary effects which can be used to obtain a gravity gradiometer with other characteristics necessary for operation in a hostile moving-base environment. Utilizing a number of recently devised techniques which rely on certain properties of superconductors, a design for a sensitive yet rugged gravity gradiometer with a high degree of stability and a common-mode rejection ratio greater than 10 to the 9th is produced. With a base line of 0.11 m, a sensitivity of 0.1 Eotvos per sq root Hz is expected in an environment monitored to a level of 0.01 m/sq sec sq root Hz for linear vibration and 7 x 10 to the -6th rad/s sq root Hz for angular vibration. A conventional stabilized platform can be used at this level. The intrinsic noise level, which is two orders of magnitude lower, could be achieved by monitoring the attitude with a superconducting angular accelerometer which is under development. In addition, the new gradiometer design has the versatility of adapting the instrument to different gravity biases by adjusting stored dc currents.

Moody, M. V.↗

NASA NTRS1987

Magnetic studies of high Tc superconducting (La0.9Sr0.1)2CuO4-y

The magnetic moment of La(0.9Sr0.1)2CuO4-y was measured as a function of temperature and magnetic field, and the onset of superconductivity was found to occur at a temperature of 35 K. At 2 K, the dc magnetic susceptibility was found to reach 83 percent of perfect diamagnetism. Field studies have shown that the sample is a type-II superconductor and that the temperature dependences of the critical fiedls are anomalous. Its critical fields, kappa, and lambda(eff) are much larger than those for (La0.9Ba0.1)2CuO4-y, and their temperature dependences cannot be explained in terms of BCS theory.

Zirngiebl, E.↗

NASA NTRS1987

Consortium for Materials Development in Space. Technical section

Several topics related to materials development in space are discussed. Physical vapor transport crystal growth, the mass spectroscopic facility, surface coatings and catalyst production by electrodeposition, mass transfer by diffusion, electrooptical organic materials, and high temperature superconductors are among the topics covered.

Source record↗

NASA NTRS1988

Static magnetic ordering of CeCu2.1Si2 found by muon spin relaxation

Zero- and longitudinal-field muon spin relaxation measurements on a polycrystal sample of a heavy fermion superconductor CeCu2.1 Si2 (T(c) = 0.7 K) have revealed an onset of static magnetic ordering below T approximately 0.8 K. The line shapes of the observed spectra in zero field indicate a wide distribution of static random local fields at muon sites, suggesting that the ordering is either spin glass or incommensurate spin-density-wave state. The observed width of the random local field at T = 0.05 K corresponds to a small averaged static moment of the order of 0.1 micro-B per formula unit.

Uemura, Y. J.↗

NASA NTRS1988

Analysis of the performance of the space ultravacuum research facility in attached and free-flyer mode

The old concept of using the wake of a spacecraft to obtain an ultrahigh vacuum is revisited with a somewhat different emphasis. Since it is possible to configure a wake shield so that a surface of interest does not subtend any walls that could become contaminated, it appears that it should be possible to achieve a contamination-free, ultrahigh vacuum capability with infinite pumping speed even in the presence of high heat loads and moderate gas loads. With the new interest in developing thin films with precision controlled synthetic microstructures such as superlattices, mixed metal oxide high temperature superconductors, rare-earth magneto-optical devices, and nano-crystalline alloys, the ability to work with a variety of different materials without cross contamination should be of significance. This paper analyzes the performance of the conceptual design for a Space Ultravacuum Research Facility (SURF), both in a Shuttle-attached mode and as a free-flyer. It is shown that even in the Shuttle-attached mode, it should be possible to obtain vacuum levels equivalent to 10 to the -10 Torr with O and N2 as the primary constituents. This should be sufficient to demonstrate the feasibility of the concept, particularly the infinite pumping speed and virtual elimination of contamination aspects. As a free-flyer the SURF will be limited primarily by the gas load associated with the process being performed. For chemical beam epitaxy (CBE) it is shown that equivalent vacuum levels of 10 to the -14 Torr should be possible at 300 km.

Naumann, Robert J.↗

NASA NTRS1987

Quadrupolar Kondo effect in uranium heavy-electron materials?

The possibility of an electric quadrupole Kondo effect for a non-Kramers doublet on a uranium (U) ion is a cubic metallic host is demonstrated by model calculations showing a Kondo upturn in the resistivity, universal quenching of the quadrupolar moment, and a heavy-electron anomaly in the electronic specific heat. With inclusion of excited crystal-field levels, some of the unusual magnetic-response data in the heavy-electron superconductor UBe13 may be understood. Structural phase transitions at unprecedented low temperatures may occur in U-based heavy-electron materials.

Cox, D. L.↗

NASA NTRS1987

Magnetic field penetration depth of La(1.85)Sr(0.15)CuO4 measured by muon spin relaxation

Muon-spin-relaxation measurements have been performed on a high-Tc superconductor La(1.85)Sr(0.15)CuO4. In an external transverse magnetic field of 500 G, a magnetic field penetration depth of 2000 A at T = 10 K has been determined from the muon-spin-relaxation rate which increased with decreasing temperature below Tc. From this depth and the Pauli susceptibility, the superconducting carrier density is estimated at 3 x 10 to the 21st per cu cm. The zero-field relaxation rates above and below Tc were equal, which suggests that the superconducting state in this sample is not associated with detectable static magnetic ordering.

Kossler, W. J.↗

NASA NTRS1987

All NbN tunnel junction fabrication

The development of SIS tunnel junctions based on NbN for mixer applications in the submillimeter range is reported. The unique technological challenges inherent in the development of all refractory-compound superconductor-based tunnel junctions are highlighted. Current deposition and fabrication techniques are discussed, and the current status of all-NbN tunnel junctions is reported.

Leduc, H. G.↗

NASA NTRS1988

Evidence for a common high-temperature superconducting effect in La(1.85)Sr(0.15)CuO4 and YBa2Cu3O7

The paper reports the positron-annihilation lifetime and Doppler-broadening energy spectra in La(1.85)Sr(0.15)CuO4 superconductors for T = 10-297 K. A strong temperature dependence in positron lifetime and momentum distribution parameters is observed for positron-electron annihilation data while the sample is in the superconducting state, but not while it is in the normal state. Experimental evidence is presented that the superconducting mechanisms in La(1.85)Sr(0.15)CuO4 and YBa2Cu3O7 are similar and it is suggested that this is a consequence of a common physics involving the delicate balance between localized- and itinerant-electron behavior.

Jean, Y. C.↗

NASA NTRS1988

Rugged low-resistance contacts to YBa2Cu3O(x)

Rugged low-resistance contacts to a high-T(c) superconductor YBa2Cu3O(x) were made by melting gold onto the sample surface, where it diffused into the sample pores making a strong mechanical contact in the form of a bead. Contact resistances lower than 50 microohm were obtained, allowing passage, without heating, of a direct current of about 5 A while the sample remained in the superconducting state at 20 K. Results of SEM and of contact-resistance, critical-current, and shear-strength measurements on these contacts are included.

Caton, R.↗

NASA NTRS1987

Ion nitriding; Proceedings of the International Conference, Cleveland, OH, Sept. 15-17, 1986

The present conference discusses plasma-assisted surface coating/modification processes, the applications to date of ion nitriding, the effects of nitrogen on metal surfaces, ion nitriding mechanisms in Cr, Al and Cr + Al-containing 1040 steel, ion nitriding of Al and its alloys, life enhancement for forging dies, novel anode plasma nitriding developments, and a comparative study of the pulsed and dc ion-nitriding behavior in specimens with blind holes. Also discussed are the influence of heating method on ion nitriding, surface hardening of marage steels by ion nitriding without core hardness reduction, plasma nitriding of nodular cast iron sput gears, NbN composites for superconductors, the carburization of tungsten in a glow discharge methane plasma, economic considerations concerning plasma nitriding, and the corrosion properties obtained by ion nitriding.

Spalvins, T.↗

NASA NTRS1989

Orienting Superconductive Crystals For High Current Density

Proposed technique for controlled distortion of crystal grains in newly discoverd superconductor YBa2Cu3O7-x increases current-carrying capacity. Helps to ensure grains in this and other anisotropic materials all oriented in same direction so charge carriers transferred readily from one grain to another. Specimen of YBa2Cu3O7-x heated in oxygen atmosphere compressed in one direction as slowly cooled below transition temperature. Under these conditions, oxygen atoms tend to rearrange so as to relieve stress created by compression.

Shlichta, Paul J.↗

NASA NTRS1989

Making Excited Oxygen Molecules And Atoms

Oxidation of semiconductors and high-temperature superconductors achieved at lower temperatures by use of oxygen molecules or atoms raised into specific excited states. Use of excited oxygen (or other species) of interest in research on kinetics and mechanisms of chemical reactions. Used in ultra-high-vacuum chamber also equipped for such surface-analytical techniques as x-ray photoelectron spectroscopy.

Vasquez, Richard P.↗