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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 595 records · Page 33
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Reservoir Response to Thermal and High-Pressure Well Stimulation Efforts at Raft River, Idaho

An injection stimulation test begun at the Raft River geothermal reservoir in June, 2013 has produced a wealth of data describing well and reservoir response via high-resolution temperature logging and distributed temperature sensing, seismic monitoring, periodic borehole televiewer logging, periodic stepped flow rate tests and tracer injections before and after stimulation efforts. The hydraulic response demonstrates continually increasing injectivity, reflected in varying flow rate response to nearly constant injection pressure, but features of the hydraulic response provide information about different characteristics of the reservoir. Changes in injectivity immediately following high-flow rate tests suggest that hydro shearing has altered the near-well permeability structure, while pressure response during those tests indicates that near-well permeability is relatively homogeneous and low but that the well is near, but not well connected to, a zone of higher transmissivity. Long-term changes in injectivity are believed to reflect propagation of the injection cooling front through low permeability zones. Two dimensional flow and heat transport simulations are used to demonstrate how the timescale of pressure response may relate to length scales of permeability distribution.

Well stimulation, injectivity, enhanced geothermal↗
NASA NTRS2018

Boeing: Arc Jet Exposure of Ablative Non-Oxide CMC TPS for Planetary Probe and Sample Return Applications

NASA Game Changing Development (GCD) provided Boeing support under a Space Act Agreement (SAA) for arc jet sample design, CFD support and arc jet test time of stagnation and shear models for 3 Boeing TPS materials: BLA (Boeing Lightweight Ablator, 18, 21 and 22 densities), BPA (Boeing Phenolic Ablator, standard, graded density, or without reinforcement) and Non-oxide high temperature ceramic composite for structurally integrated TPS (SITPS). Results: For BLA, tested successfully to 500 W/cm² heat flux and heat loads up to 12 kJ/cm² with shear loads up to 370 Pa. The BPA 2017 formulation tested successfully to 1500 W/cm² and 80 kJ/cm², with shear loads up to 250 Pa. For SITIPS, Boeing fabricated C/SiC laminate materials survived testing in shear.

commercial space↗
NASA NTRS1995

Analytical investigation of the hygrothermal effects and parametric study of the Edge Crack Torsion (ECT) mode 3 test lay-ups

A shear deformation theory including residual thermal and moisture effects is developed for the analysis of either symmetric or unsymmetric laminates with mid-plane edge delamination under torsion loading. The theory is based on an assumed displacement field which includes shear deformation. The governing equations and boundary conditions are obtained from the principle of virtual work. The analysis of the (90/(+/- 45)(n)/(-/+ 45)(n)/90)(s) ECT mode 3 test lay-up indicates that there are no hygrothermal effects on the mode 3 strain energy release rate because the laminate, and both sublaminates above and below the delamination, are symmetric lay-ups. A further parametric study reveals that some other lay-ups can have negligible hygrothermal effects even when the sublaminates above and below the delamination are not symmetric about their own mid-planes. However, these lay-ups may suffer from distortion after the curing process. Another Interesting set of lay-ups investigated is a class of antisymmetric laminates with (+/-(theta/(theta -90)(2)/theta))(n) lay-ups. It is observed that when n takes on even numbers (2 and 4), both hygrothermal and mode 1 effects can be neglected. From this point of view, these lay-ups provide a way to determine the mode 3 toughness between two dissimilar layers. However, when n takes on odd numbers (1 and 3), both hygrothermal and mode 1 effects may be strong in these lay-ups. In particular, when theta equals 45 deg, the lay-ups are free from both hygrothermal and mode 1 effects irrespective of n.

Li, Jian↗
NASA NTRS1973

Shear strength of lunar soil from Oceanus Procellarum.

Soil from the scoop of Surveyor 3, returned to earth by Apollo 12 astronauts, has been tested in a miniature shear box at five bulk densities, from 0.99 to 1.87 g/cu cm. Cohesion increased with bulk density from .03 to .3 N/sq cm; internal friction angle increased from 13 to 56 deg. Shear stress vs normal stress data fit a logarithmic relationship better than a linear one, at normal stresses of .003 to 3 N/sq cm. Results of these tests, in air, show no systematic differences from those for tests made elsewhere in vacuum and nitrogen. Results agree with those obtained in remotely controlled lunar surface operations with Surveyor 3 and other spacecraft provided that the bulk density was slightly underestimated for the on-surface measurements.

Jaffe, L. D.↗
NASA NTRS2001

ZBLAN Viscosity Instrumentation

The past year's contribution from Dr. Kaukler's experimental effort consists of these 5 parts: a) Construction and proof-of-concept testing of a novel shearing plate viscometer designed to produce small shear rates and operate at elevated temperatures; b) Preparing nonlinear polymeric materials to serve as standards of nonlinear Theological behavior; c) Measurements and evaluation of above materials for nonlinear rheometric behavior at room temperature using commercial spinning cone and plate viscometers available in the lab; d) Preparing specimens from various forms of pitch for quantitative comparative testing in a Dynamic Mechanical Analyzer, Thermal Mechanical Analyzer; and Archeological Analyzer; e) Arranging to have sets of pitch specimens tested using the various instruments listed above, from different manufacturers, to form a baseline of the viscosity variation with temperature using the different test modes offered by these instruments by compiling the data collected from the various test results. Our focus in this project is the shear thinning behavior of ZBLAN glass over a wide range of temperature. Experimentally, there are no standard techniques to perform such measurements on glasses, particularly at elevated temperatures. Literature reviews to date have shown that shear thinning in certain glasses appears to occur, but no data is available for ZBLAN glass. The best techniques to find shear thinning behavior require the application of very low rates of shear. In addition, because the onset of the thinning behavior occurs at an unknown elevated temperature, the instruments used in this study must provide controlled low rates of shear and do so for temperatures approaching 600 C. In this regard, a novel shearing parallel plate viscometer was designed and a prototype built and tested.

Kaukler, William↗
DOE OSTI2020

Ion-Conducting Dynamic Solid Polymer Electrolyte Adhesives

Cross-linked polymer electrolytes containing structurally dynamic disulfide bonds have been synthesized to investigate their combined ion transport and adhesive properties. Dynamic network polymers of varying cross-link densities are synthesized via thiol oxidation of a bisthiol monomer, 2,2'-(ethylenedioxy)diethanethiol, and tetrathiol cross-linker, pentaerythritol tetrakis(3-mercaptopropionate). At optimal loading of lithium bis(trifluoromethane-sulfonyl-imide) (LiTFSI) salt, the ionic conductivities (σ) at 90 °C are about 1 × 10–4 and 1 × 10–5 S/cm at the lowest and highest cross-linking, respectively. Notably, in comparison to the equivalent nondynamic network, the dynamic network shows a positive deviation in σ above 90 °C, which suggests the enhancement of ion transport occurs from the difference in structural relaxation on account of the dissociation of disulfide bonds. Lap shear adhesion and conductivity tests on ITO-coated glass substrates reveal the dynamic network exhibits a higher adhesive shear strength of 0.2 MPa (vs 0.03 MPa for the nondynamic network) and higher σ after the application of external stimulus (UV light or heat). The adhesive strength and σ are stable over multiple debonding/rebonding cycles and, thus, demonstrating the utility of these structurally dynamic networks as solid polymer electrolyte adhesives.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1982

Test and analysis of Celion 3000/PMR-15, graphite/polyimide bonded composite joints: Data report

Standard single lap, double lap and symmetric step lap bonded joints of Celion 3000/PMR-15 graphite/polyimide composite were evaluated. Composite to composite and composite to titanium joints were tested at 116 K (-250 F), 294 K (70 F) and 561 K (550 F). Joint parameters evaluated are lap length, adherend thickness, adherend axial stiffness, lamina stacking sequence and adherend tapering. Advanced joint concepts were examined to establish the change in performance of preformed adherends, scalloped adherends and hybrid systems. The material properties of the high temperature adhesive, designated A7F, used for bonding were established. The bonded joint tests resulted in interlaminar shear or peel failures of the composite and there were very few adhesive failures. Average test results agree with expected performance trends for the various test parameters. Results of finite element analyses and of test/analysis correlations are also presented.

Cushman, J. B.↗
DOE OSTI2022

Extracting single fiber transverse and shear moduli from off-axis misalignment fiber tensile testing

Small diameter (<100 μm) fibers (e.g. carbon fibers, Kevlar, and fiberglass) and wires (e.g. ultrafine copper and aluminum wires) are frequently used in many different engineering applications, such as for light weighting structures, electromagnetic shielding for aircraft/infrastructure/EVs, vibration damping, biological sensors, aerospace electrical devices, and electric windings just to name a few. Due to the manufacturing process, the fibers and wires are pulled and stretched to produce a preferential alignment. Therefore, thin fibers and wires typically display different properties along the length of the fiber as opposed to their cross section and many fibers/wires are considered transversely isotropic. The axial properties of fibers/wires can be ascertained via tensile testing of single-filaments or fiber tows, but the radial properties require much more effort to measure. Knowing these properties is important for the accurate prediction of micromechanical models and manipulation of fibers during micromanufacturing. In this paper, a new technique was developed to determine the transverse/shear moduli and strength of a material by conducting tensile tests of the material at increasing misalignment angles from the tensile axis. Due to the transversely isotropic nature of the material, the transverse/shear moduli and strength influence the experimental results recorded by the test machine to different degrees based on the amount of misalignment in the test setup. An equation was derived to determine the influence of each of the material properties based on the misalignment angle by manipulating the stiffness matrix for transversely isotropic materials using the transformation matrices. Then, curve fitted coefficients were used to identify the material properties. Here, the strengths were similarly determined by curve fitting an off-axis Tsai-Hill failure criteria to determine the influence of transverse, shear, and tensile strengths based on the complex loading condition provided by the off-axis tensile test. Zoltek Panex 35 carbon fibers were used to demonstrate this new technique and the determined properties were then compared to those obtained from nanoindentation and from literature. Fracture surfaces provide insight into the different failure mechanisms at various misalignment angles.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Viscous flow properties and hydrodynamic diameter of phenothiazine-based redox-active molecules in different supporting salt environments

We report viscous flow properties of a redox-active organic molecule, N-(2-(2-methoxyethoxy)ethyl)phenothiazine (MEEPT), a candidate for non-aqueous redox flow batteries, and two of its radical cation salts. A microfluidic viscometer enabled the use of small sample volumes in determining viscosity as a function of shear rate and concentration in the non-aqueous solvent, acetonitrile, both with and without supporting salts. All solutions tested show Newtonian behavior over shear rates of up to 30 000 s−1, which was rationalized by scaling arguments for the diffusion-based relaxation time of a single MEEPT molecule without aggregation. Neat MEEPT is flowable but with a large viscosity (412 mPa⋅s at room temperature), which is ∼1000 times larger than that of acetonitrile. MEEPT solutions in acetonitrile have low viscosities; at concentrations up to 0.5 M, the viscosity increases by less than a factor of two. From concentration-dependent viscosity measurements, molecular information was inferred from intrinsic viscosity (hydrodynamic diameter) and the Huggins coefficient (interactions). Model fit credibility was assessed using the Bayesian Information Criterion. It is found that the MEEPT and its charged cations are “flowable” and do not flocculate at concentrations up to 0.5 M. MEEPT has a hydrodynamic diameter of around 8.5 Å, which is almost insensitive to supporting salt and state of charge. This size is comparable to molecular dimensions of single molecules obtained from optimized structures using density functional theory calculations. The results suggest that MEEPT is a promising candidate for redox flow batteries in terms of its viscous flow properties.

Wang, Yilin (ORCID:0000000316102995)↗
NASA NTRS1991

High strain rate properties of unidirectional composites, part 1

Experimental methods were developed for testing and characterization of composite materials at strain rates ranging from quasi-static to over 500 s(sup -1). Three materials were characterized, two graphite/epoxies and a graphite/S-glass/epoxy. Properties were obtained by testing thin rings 10.16 cm (4 in.) in diameter, 2.54 cm (1 in.) wide, and six to eight plies thick under internal pressure. Unidirectional 0 degree, 90 degree, and 10 degree off-axis rings were tested to obtain longitudinal, transverse, and in-plane shear properties. In the dynamic tests internal pressure was applied explosively through a liquid and the pressure was measured with a calibrated steel ring. Strains in the calibration and specimen rings were recorded with a digital processing oscilloscope. The data were processed and the equation of motion solved numerically by the mini-computer attached to the oscilloscope. Results were obtained and plotted in the form of dynamic stress-strain curves. Longitudinal properties which are governed by the fibers do not vary much with strain rate with only a moderate (up to 20 percent) increase in modulus. Transverse modulus and strength increase sharply with strain rate reaching values up to three times the static values. The in-plane shear modulus and shear strength increase noticeably with strain rate by up to approximately 65 percent. In all cases ultimate strains do not vary significantly with strain rates.

Daniel, I. M.↗
DOE OSTI2017

Structure/property relationships in copolymers comprising renewable isosorbide, glucarodilactone, and 2,5-bis(hydroxymethyl)furan subunits

Carbohydrates and their derivatives have great potential as building blocks for the development of renewable materials that are cost and performance competitive with conventional petroleum-based materials. To this end, the rigid carbohydrate-derived diols, glucarodilactone and isosorbide were functionalized with a castor oil derivative, 10-undecenoic acid, forming α,ω-dienes suitable for acyclic diene metathesis (ADMET) polymerization. Equimolar copolymerizations of these two monomers, glucarodilactone undecenoate (GDLU) and isosorbide undecenoate (GDLU), transform brittle homopolymers into elastic materials with shape memory capabilities. To understand the source of these properties, a series of copolymers consisting of a range of GDLU and IU compositions (100:0, 77:23, 76:24, 52:48, 48:52, 18:82, 0:100 mol percent GDLU to IU) was synthesized. The material and chemical properties were characterized by uniaxial tensile testing, small-amplitude oscillatory shear rheology, X-ray scattering and hydrolytic degradation testing. Small compositional changes in this family were shown to have a drastic impact on the observed mechanical performance and degradability of these materials. Rheological measurements of GDLU-containing copolymers found evidence for the presence of transient networking within these materials. We posit that the transient network within this material is responsible for the elasticity and shape memory abilities of the GDL-containing materials. In confirmation of these properties, a novel α,ω-diene 2,5-bis(hydroxymethylfuran) undecenoate (BHMFU) was developed and served as a direct replacement for either GDLU or IU in copolymerizations. The replacement of GDLU resulted in a total loss of the elasticity and shape memory of the copolymers, supporting the role of GDLU in the mechanical performance.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2024

KiDS-1000 cosmology: Combined second- and third-order shear statistics

Aims.In this work, we perform the first cosmological parameter analysis of the fourth release of Kilo Degree Survey (KiDS-1000) data with second- and third-order shear statistics. This paper builds on a series of studies aimed at describing the roadmap to third-order shear statistics. Methods.We derived and tested a combined model of the second-order shear statistic, namely, the COSEBIs and the third-order aperture mass statistics 〈ℳ ap 3 〉 in a tomographic set-up. We validated our pipeline withN-body mock simulations of the KiDS-1000 data release. To model the second- and third-order statistics, we used the latest version of HMCODE2020 for the power spectrum and BIHALOFITfor the bispectrum. Furthermore, we used an analytic description to model intrinsic alignments and hydro-dynamical simulations to model the effect of baryonic feedback processes. Lastly, we decreased the dimension of the data vector significantly by considering only equal smoothing radii for the 〈ℳ ap 3 〉 part of the data vector. This makes it possible to carry out a data analysis of the KiDS-1000 data release using a combined analysis of COSEBIs and third-order shear statistics. Results.We first validated the accuracy of our modelling by analysing a noise-free mock data vector, assuming the KiDS-1000 error budget, finding a shift in the maximum of the posterior distribution of the matter density parameter, ΔΩ m < 0.02 σ Ω m , and of the structure growth parameter, ΔS 8 < 0.05 σ S 8 . Lastly, we performed the first KiDS-1000 cosmological analysis using a combined analysis of second- and third-order shear statistics, where we constrained Ω m = 0.248 −0.055 +0.062 andS 8 = σ 8 √(Ω m /0.3 )= 0.772 ± 0.022. The geometric average on the errors of Ω m andS 8 of the combined statistics decreases, compared to the second-order statistic, by a factor of 2.2.

Astronomy & Astrophysics↗
NASA NTRS1981

The Joint Airport Weather Studies Project

A block diagram of the joint airport weather studies program is presented. Background leading to the development of the program is reviewed. Basic studies, aircraft performance, and detection and warning techniques used to develop fine scale structure of thunderstorm dynamics and kinematics in the vicinity of a major airport; effect of thunderstorm low level wind shear on aircraft performance; and development of real time testing of flow level wind shear detection and warning techniques and displays are described.

Mccarthy, J.↗
NASA NTRS1983

The Joint Airport Weather Studies (JAWS) project

A block diagram of the joint airport weather studies program is presented. Background leading to the development of the program is reviewed. Basic studies, aircraft performance, and detection and warning techniques used to develop fine scale structure of thunderstorm dynamics and kinematics in the vicinity of a major airport; effect of thunderstorm low level wind shear on aircraft performance; and development of real time testing of flow level wind shear detection and warning techniques and displays are described.

Mccarthy, J.↗
NASA NTRS2010

Performance and Stability Analyses of Rocket Combustion Devices Using Liquid Oxygen/Liquid Methane Propellants

Liquid rocket engines using oxygen and methane propellants are being considered by the National Aeronautics and Space Administration (NASA) for in-space vehicles. This propellant combination has not been previously used in flight-qualified engine systems, so limited test data and analysis results are available at this stage of early development. NASA has funded several hardware-oriented programs with oxygen and methane propellants over the past several years with the Propulsion and Cryogenic Advanced Development (PCAD) project, under the Exploration Technology Development Program. As part of this effort, NASA Marshall Space Flight Center has conducted combustion, performance, and combustion stability analyses of several of the configurations on these programs. This paper summarizes these analyses. Test and analysis results of impinging and coaxial element injectors using liquid oxygen and liquid methane propellants are included. Several cases with gaseous methane are included for reference. Several different thrust chamber configurations have been modeled, including thrust chambers with multi-element like-on-like and swirl coax element injectors tested at NASA MSFC, and a unielement chamber with shear and swirl coax injectors tested at The Pennsylvania State University. Configurations were modeled with two one-dimensional liquid rocket combustion analysis codes, the Rocket Combustor Interaction Design and Analysis (ROCCID), and the Coaxial Injector Combustion Model (CICM). Significant effort was applied to show how these codes can be used to model combustion and performance with oxygen/methane propellants a priori, and what anchoring or calibrating features need to be applied or developed in the future. This paper describes the test hardware configurations, presents the results of all the analyses, and compares the results from the two analytical methods.

Hulka, James R.↗
NASA NTRS1992

Experimental investigation of cyclic thermomechanical deformation in torsion

An investigation of thermomechanical testing and deformation behavior of tubular specimens under torsional loading is described. Experimental issues concerning test accuracy and control specific to thermomechanical loadings under a torsional regime are discussed. A series of shear strain-controlled tests involving the nickel-base superalloy Hastelloy X were performed with various temperature excursions and compared to similar thermomechanical uniaxial tests. The concept and use of second invariants of the deviatoric stress and strain tensors as a means of comparing uniaxial and torsional specimens is also briefly presented and discussed in light of previous thermomechanical tests conducted under uniaxial conditions.

Ellis, John R.↗