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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 595 records · Page 33
All sourcesNASA NTRSDOE OSTI
NASA NTRS2012

Carbon Nanotube Bonding Strength Enhancement Using Metal "Wicking" Process

Carbon nanotubes grown from a surface typically have poor bonding strength at the interface. A process has been developed for adding a metal coat to the surface of carbon nano tubes (CNTs) through a wicking process, which could lead to an enhanced bonding strength at the interface. This process involves merging CNTs with indium as a bump-bonding enhancement. Classical capillary theory would not normally allow materials that do not wet carbon or graphite to be drawn into the spacings by capillary action because the contact angle is greater than 90 degrees. However, capillary action can be induced through JPL's ability to fabricate oriented CNT bundles to desired spacings, and through the use of deposition techniques and temperature to control the size and mobility of the liquid metal streams and associated reservoirs. A reflow and plasma cleaning process has also been developed and demonstrated to remove indium oxide, and to obtain smooth coatings on the CNT bundles.

Lamb, James L.↗
NASA NTRS1979

The magnetic anomaly model of the Jovian magnetosphere - Predictions for Voyager

The magnetic anomaly model, in which the anomalously weak magnetic field region in the northern hemisphere of Jupiter influences the outer Jovian magnetosphere by one or more plasma interaction processes, has been put forth to account for the various observed Jovian magnetospheric phenomena that show evidence of Jovian longitudinal asymmetry or planetary spin periodicity. From this model, normalized by empirical fitting to Pioneer 10 and 11 flyby data and to ground-based radio data, a series of predictions are made that are subject to test by the forthcoming flybys of Jupiter by Voyagers 1 and 2. These predictions cover: (1) the longitude range and time intervals of enhanced interaction between Io (and possibly Europa) and Jupiter's ionosphere, (2) plasma, energetic particle, and magnetic field periodicities in the outer magnetosphere, and (3) the sub-spacecraft System III longitude and the time, modulo 10 hours, of the first and subsequent magnetopause crossings.

Dessler, A. J.↗
NASA NTRS1997

The Tethered Satellite System: Scientific and Technological Results

The bi-national, US-Italian, Tethered Satellite System (TSS) program was designed to provide a unique opportunity to explore certain space plasma- electrodynamic processes and the orbital mechanics of a gravity-gradient stabilized system of two satellites linked by a long conducting tether. The second flight, TSS-LR, was launched February 22, 1996 on STS-75 and satellite deployment began at MET 3/00:27. A unique data set was obtained over the next five hours as the tether was deployed to a length of 19695 meters, which has allowed significant science to be accomplished. This presentation will focus on results from the TSS-LR mission that are most important to the future technological applications of electrodynamic tethers in space - in particular, the current collection process. Of particular significance is an apparent transition of the physics of current collection when the potential of the collecting body becomes greater than the ram energy of the ionospheric atomic oxygen ions. Previous theoretical models of current collection were electro- static - assuming that the orbital motion of the system, which is highly sub-sonic with respect to electron thermal motion, was unimportant. This may still be acceptable for the case of relatively slow-moving sounding rockets. However, the TSS-LR results show that motion relative to the plasma must be accounted for in orbiting systems.

Stone, Nobie H.↗
NASA NTRS1995

Some remarks on waves in the solar wind

Waves are significant to the solar wind in two ways as modifiers of the particle distribution functions, and as diagnostics. In addition, the solar wind serves as an important laboratory for the study of plasma wave processes, as it is possible to make detailed measurements of phenomena which are too small to be easily measured by laboratory sized sensors. There are two areas where waves (we include discontinuities under this heading) must make important modifications of the distribution functions: in accelerating the alpha particles to higher speeds than the protons (Marsch et al.) and in accelerating the solar wind itself. A third area is possibly in maintaining the relative isotropy of the solar wind ion distribution in the solar wind rest frame. As the solar wind is nearly collisionless, the ions should conserve magnetic moment in rushing out from the sun, and therefore Tperp/B should be relatively constant, but it is obviously not. This has not received much attention. The waves, both electromagnetic and electrostatic, which are pan of the solar Type 111 burst phenomenon, have been extensively studied as examples of nonlinear plasma phenomena, and also used as remote sensors to trace the solar magnetic field. The observations made by Ulysses show that the field can be traced in this way out to perhaps a little more than an A.U., but then the electromagnetic pan of the type 111 burst fades out. Nevertheless, sometimes Langmuir waves appear at Ulysses at an appropriate extrapolated time. This seems to support the picture in which the electromagnetic waves at the fundamental plasma frequency are trapped in density fluctuations. Langmuir waves in the solar wind are usually in quasi-thermal equilibrium quasi because the solar wind itself is not isothermal. The Observatory of Paris group (Steinberg. Meyer-Vernet, Hoang) has exploited this with an experiment on WIND which is capable of providing density and temperature on a faster time scale than hitherto. Recently it has been found that Langmuir waves are associated with magnetic holes. This may help to elucidate the nature of magnetic holes. Nonlinear processes are important in the transformation of wave energy to panicle energy. Some recent examples from WIND data will be shown.

Kellogg, Paul J.↗
DOE OSTI2024

An octahedral Mach B-dot probe for 3D flows and magnetic fields in the edge of reversed field pinches

Measurements and simulations show that plasma relaxation processes in the reversed field pinch drive and redistribute both magnetic flux and momentum. To examine this relaxation process, a new 3D Mach B-dot probe has been constructed. This probe collects ion saturation currents through six molybdenum electrodes arranged on the flattened vertices of an octahedron made of boron nitride (BN). The ion saturation current flows through configurable voltage dividers for measurement and returns through one of six selectable return electrodes equally spaced along the 12 cm BN probe arm. In addition, the probe arm houses three B-dot magnetic pickup coils in the BN stalk immediately below to the octahedron, to measure the local magnetic field. Inserted in the Madison Symmetric Torus (MST) during deuterium discharges with 220 kA plasma current, density of 0.8 × 10 13 cm –3 , the probe collects ion saturation currents with sawtooth-like peaks correlated with relaxation events. This compact octahedral design fitting six Mach electrode surfaces within a 1 cm3 cube will enable future multi-point, multi-field probes compatible with the 1.5 in. ports of MST. Such probes will allow for flow circulation, current, and canonical vorticity to be calculated in the center of the finite difference stencil formed by the measurement locations.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2022

Experimental observations of multiple modes of filamentary structures in the magnetized dusty plasma experiment (MDPX) device

Due to the small charge-to-mass ratio of dust particles, it is often necessary to use large magnetic fields of B ≥ 1 T, in order to observe the influence of magnetic forces in laboratory dusty plasmas. However, when experiments are performed at high magnetic fields in capacitively coupled, radio frequency discharges used for these dusty plasma experiments, the plasma is often observed to form filamentary structures between the electrodes that are aligned to the external magnetic field which disrupt the uniformity of the plasma and adversely impact some of our dusty plasma experiments. Recent experiments performed in the Magnetized Dusty Plasma Experiment device seek to identify and characterize these filamentary structures. This paper discusses the morphology of several distinct filamentary modes that are formed in low temperature argon plasmas. Three different spatial modes of filaments that appear to be strongly dependent on the magnetic field and neutral pressure are identified. There is strong evidence that each spatial mode has a threshold condition that is dependent on the ion Hall parameter. The criteria for the formation of the filaments are shown to be consistent with predictions of recent numerical simulations.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2022

Electron Modulational Instability in the Strong Turbulent Regime for an Electron Beam Propagating in a Background Plasma

We study collective processes for an electron beam propagating through a background plasma using simulations and analytical theory. A new regime where the instability of a Langmuir wave packet can grow locally much faster than ion frequency is clearly identified. The key feature of this new regime is an electron modulational instability that rapidly creates a local Langmuir wave packet, which in its turn produces local charge separation and strong ion density perturbations because of the action of the ponderomotive force, such that the beam-plasma wave interaction stops being resonant. Three evolution stages of the process and observed periodic burst features are discussed. In conclusion, different physical regimes in the plasma and beam parameter space are demonstrated for the first time.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1979

Investigation of the magnetospheric boundary plasma and magnetic field data from Explorers 33, 43, and 50

Understanding of the plasma depletion process in the dayside magnetosheath, the nature of magnetotail boundary motion, and the geometry of the magnetospheric boundary layers was examined. A model of the dayside boundary layers, based on the hypothesis that merging occurs only for strictly anitparallel fields was developed which provides a qualitative solution to the problem of the half-wave rectifier response of the magnetosphere to the solar wind electric field. Regarding magnetotail boundary motion, consideration of the data led to the conclusion that at lunar distance, substorms are associated with very large amplitude compressional wave motion of the sausage type. A study of IMF orientation for depletion and nondepletion cases suggests that depletion is most likely to occur for angles between the IMF and the normal to the magnetopause at the measurement location near 90 deg, in agreement with predictions. Observations of the heat flux in the dayside magnetosheath plasma suggest that the energized plasma ions have their source along a given flux tube at that intersection with the bow shock where the magnetic field is most compressed.

Siscoe, G. L.↗
DOE OSTI2020

Tutorial on forming through-silicon vias

Through-silicon vias (TSVs) are a critical technology for three-dimensional integrated circuit technology. These through-substrate interconnects allow electronic devices to be stacked vertically for a broad range of applications and performance improvements such as increased bandwidth, reduced signal delay, improved power management, and smaller form-factors. There are many interdependent processing steps involved in the successful integration of TSVs. This article provides a tutorial style review of the following semiconductor fabrication process steps that are commonly used in forming TSVs: deep etching of silicon to form the via, thin film deposition to provide insulation, barrier, and seed layers, electroplating of copper for the conductive metal, and wafer thinning to reveal the TSVs. Recent work in copper electrochemical deposition is highlighted, analyzing the effect of accelerator and suppressor additives in the electrolyte to enable void-free bottom-up filling from a conformally lined seed metal.

42 ENGINEERING↗
NASA NTRS1983

Evidence for temporal variations in polar plumes

The variability of the O VI and Mg X emissions from four plumes is studied in order to place empirical constraints on possible plasma heating processes and acceleration mechanisms for mass flows in polar plumes. The observations comprise a 40 min seqeunce of spectroheliograms acquired with a temporal resolution of approximately 2 min. It is found that the Mg X emission from each plume has a strong 'dc' component and that any variations occurred at approximately the 10 percent (of the mean) level or less. This means that temporal variations in the density and/or temperature were 5 percent or less. Some statistically significant variations in the measured Mg X signals are seen. It is noted that two of the plumes decreased in brightness by approximately 10 percent during the 40 min period of the observations. Besides this, two plumes exhibited short-term (few minute) variations that are seen as statistically significant at a confidence level of more than 90 percent. The latter variations (if real) are thought to be due to small (approximately 20,000 K) fluctuations in temperature caused by fluctuations in the local plasma heating rate.

Withbroe, G. L.↗
DOE OSTI2026

A tutorial on high-order harmonic generation in atoms, molecules, and condensed matter

This tutorial introduces strong-field-driven high-order harmonics, their experimental generation and characterization techniques, and their main applications including attosecond pulse generation and ultrafast spectroscopy of the target material. We begin from the use of atomic targets, where the first high-order harmonic generation (HHG) experiments were realized in the late 1980s. Then, we briefly discuss the basics of the microscopic generation mechanism and how various steps of the mechanism were exploited in applications such as generating isolated attosecond pulses and probing molecular orbitals. We introduce and describe the standard experimental approaches for condensed phase HHG, where we discuss unique technical challenges of the use of solid-state materials, such as the mitigation of plasma formation and laser damage. We cover the fundamentals of high-harmonic spectroscopy in condensed matter systems, such as wide bandgap dielectrics, semiconductors, liquid media, and 2D-crystals. We provide some examples of rapidly emerging spectroscopic capabilities, such as for probing crystal symmetries, Berry phases, and associated non-trivial topological properties of the source material. Finally, we provide an overview of the research field, including some of the challenges, opportunities, and open questions.

Attosecond pulses↗
DOE OSTI2024

Magnetic Reconnection

Magnetic reconnection is a fundamental plasma physics process ubiquitous in astrophysics, and important in both magnetic confinement fusion and space weather. The MARZ fundamental science program was recently established on Z to enable the first laboratory astrophysics platform able to access and study the strongly radiatively cooled magnetic reconnection regime. Simulations of this system have successfully used a resistive-MHD approach, but in some regions of parameter space Hall physics has the potential to be important. We describe implementation of a Hall method on a staggered grid resistive-MHD method (compatible with the approach used to model MARZ experiments. We then present a different Hall method based on cell-centered field quantities. Both approaches have been implemented in the Sandia KRAKEN code, to enable us to contrast different numerical Hall-MHD methods within the same HED code.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1967

Potassium plasma cell facilitates thermionic energy conversion process

Thermionic energy converter converts nuclear generated heat directly into high frequency and direct current output. It consists of a potassium plasma cell, a tantalum emitter, and a silver plated copper collector. This conversion process eliminates the steam interface usually required between the atomic heat source and the electrical conversion system.

Richards, H. K.↗
DOE OSTI2021

Erosion of focus rings in capacitively coupled plasma etching reactors

In plasma etching reactors, the structure surrounding the wafer, often called a focus ring (FR), plays an important role in maintaining uniform fluxes of reactants across the wafer. The FR is typically made of dielectric materials. During the plasma etching process, the sheath that forms over the wafer to accelerate ions anisotropically into the surface extends over the FR. Electrical charging of the FR modifies the sheath relative to that over the wafer. On the one hand, one wants the sheath to be uniform across the wafer-FR boundary to enable uniform fluxes to the edge of the wafer. On the other hand, maintaining a high voltage sheath over the FR will erode the FR, which is undesirable as the FR is a consumable component that must be periodically replaced in high volume manufacturing. In this work, we computationally investigated the consequences of dielectric constant ε of the FR materials on erosion of the FR. The series capacitance of the FR and its underlying structure is typically smaller than that of the wafer and its underlying structure. As a result, the FR charges quickly relative to the wafer, which then reduces the voltage across the sheath on top of the FR. The ion energy and angular distributions (IEADs) striking the FR are, therefore, generally lower in energy with a broader angular distribution. With ε = 2, the ion energies striking the middle to the outer edge of the FR are 30–180 eV, whereas for ε = 100, the ion energies are 120–380 eV. At the transition between the wafer and the FR, there is a skew in the IEAD as large as 15° that results from the difference in sheath thickness above the wafer and the FR. This skew and the erosion rate across the FR are functions of the dielectric constant of the FR material. With low ε, the FR charges quickly, less plasma is produced above the FR, and there is less voltage across the sheath that results in less FR erosion. Increasing ε of the FR produces a higher sheath voltage as well as higher ion fluxes over the FR, which increases erosion, while the skew at the edge of the wafer is less severe. Further, the material of the subsurface portion of the FR, which dominates its capacitance, is an important consideration in the design of the substrate assembly.

36 MATERIALS SCIENCE↗
DOE OSTI2024

Deuterium Permeation Through a Self-Supported Palladium-Silver Membrane in Helium Gas Mixtures

Palladium membranes and membrane reactors can separate and purify tritium from impurities in the plasma exhaust processing system for the fusion energy fuel cycle. Membranes can also act as a continuous separation method to remove tritium from helium streams in the breeder blanket tritium extraction system, such as from the purge gas of solid breeders. To investigate the potential of these membranes for these applications, we performed a deuterium permeation campaign with a self-supported palladium-silver (Pd-25Ag wt%) tube of 0.15 m length, 76 µ m wall thickness, and 3.0 mm inner diameter. A gas mixture of 3.95% D 2 and a balance of He was delivered to the inside of the tube and D permeated radially outwards through the membrane into a vacuum chamber. Permeation experiments were conducted at 300 ° C, 350 ° C, 400° C, and 450°C, from 100 to 1000 sccm total flow rate, and with total pressures of 90, 150, 190, and 250 kPa. Further, deuterium permeation was consistently lower than predicted from diffusion-limited permeation models, thus we developed a transport model that included gas-phase mass transfer and surface reactions to model experimental results. The dissociation constant was optimized to fit the developed model to experimental data.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2025

Microstructure, mechanical, and thermal properties of compositionally complex (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 ceramics

Novel compositionally complex borides, (Hf,Zr,Nb,Ti)B 2 and (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 , were fabricated using spark plasma sintering process. (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 exhibits a dual-phase microstructure, in which (Hf,Zr,Nb,Ti)B 2 is a primary phase with the hexagonal structure and LaB 6 is a secondary phase with a cubic structure. The mechanical properties of both (Hf,Zr,Nb,Ti)B 2 and (Hf,Zr,Nb,Ti)B 2 ‒LaB 6 are comparable, with a combination of high hardness and moderate fracture toughness. Thermal diffusivity and conductivity of (Hf,Zr,Nb,Ti)B 2 are much lower than the individual transition metal borides but are significantly increased by the addition of LaB 6 . Herein, it is implied that the thermal properties of boride ceramics can be controlled through the appropriate design of principal metal element compositions.

borides↗
NASA NTRS1992

Studies of dynamic processes related to active experiments in space plasmas

This is the final report for grant NAGw-2055, 'Studies of Dynamic Processes Related to Active Experiments in Space Plasmas', covering research performed at the University of Michigan. The grant was awarded to study: (1) theoretical and data analysis of data from the CHARGE-2 rocket experiment (1keV; 1-46 mA electron beam ejections) and the Spacelab-2 shuttle experiment (1keV; 100 mA); (2) studies of the interaction of an electron beam, emitted from an ionospheric platform, with the ambient neutral atmosphere and plasma by means of a newly developed computer simulation model, relating model predictions with CHARGE-2 observations of return currents observed during electron beam emissions; and (3) development of a self-consistent model for the charge distribution on a moving conducting tether in a magnetized plasma and for the potential structure in the plasma surrounding the tether. Our main results include: (1) the computer code developed for the interaction of electrons beams with the neutral atmosphere and plasma is able to model observed return fluxes to the CHARGE-2 sounding rocket payload; and (2) a 3-D electromagnetic and relativistic particle simulation code was developed.

Banks, Peter M.↗
DOE OSTI2021

Effect of CMAS viscosity on the infiltration depth in thermal barrier coatings of different microstructures

Calcium magnesium aluminum silicate (CMAS) is one of the leading concerns for the gas turbine industry. The effects of CMAS viscosity and the coating microstructure on CMAS infiltration depth were explored by conducting a time dependent interaction study. Three CMAS compositions were used from literature, and their viscosities predicted through FactSage viscosity module were drastically different. The interaction was carried out on three different TBCs synthesized using the solution precursor plasma spray process (SPPS): two of the TBCs were made of yttrium aluminum garnet (YAG) having different microstructures that promote different modes of CMAS infiltration, and one TBC was made of gadolinium zirconate (GZO). All samples had stress relieving vertical cracks and different intensities of horizontally banded porosity, (inter pass boundaries IPBs). A concentration of 100 mg/cm 2 of CMAS was applied on the TBCs which were then subjected to a 5-minute interaction at 1300 °C. Samples were analyzed using scanning electron microscopy (SEM), electron dispersive X-ray spectroscopy (EDXS), and transmission electron microscopy (TEM). Low viscosity CMAS readily penetrated the TBCs while more viscous CMAS showed less penetration. The depth of CMAS infiltration depended on the coating microstructure. In the YAG with IPBs, the CMAS spread horizontally in the IPBs before infiltrating deeper, resulting in reduced infiltration depth compared to other samples in spite of having wider vertical cracks. TEM and EDXS analysis were performed to investigate the phases present in the CMAS-TBC interaction region in YAG. Two regions were chosen, the top TBC surface in direct contact with the sea of CMAS, and the region at the CMAS penetration ended within the coating. Finally, the results showed that no secondary phases like apatite were observed in YAG, thus it can be concluded that the arrest of CMAS happened solely because of CMAS viscosity and the short infiltration time.

36 MATERIALS SCIENCE↗