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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 595 records · Page 33
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Nanoscale chemical imaging with structured X-ray illumination

High-resolution imaging with compositional and chemical sensitivity is crucial for a wide range of scientific and engineering disciplines. Although synchrotron X-ray imaging through spectromicroscopy has been tremendously successful and broadly applied, it encounters challenges in achieving enhanced detection sensitivity, satisfactory spatial resolution, and high experimental throughput simultaneously. In this work, based on structured illumination, we develop a single-pixel X-ray imaging approach coupled with a generative image reconstruction model for mapping the compositional heterogeneity with nanoscale resolvability. This method integrates a full-field transmission X-ray microscope with an X-ray fluorescence detector and eliminates the need for nanoscale X-ray focusing and raster scanning. We experimentally demonstrate the effectiveness of our approach by imaging a battery sample composed of mixed cathode materials and successfully retrieving the compositional variations of the imaged cathode particles. Bridging the gap between structural and chemical characterizations using X-rays, this technique opens up vast opportunities in the fields of biology, environmental, and materials science, especially for radiation-sensitive samples.

Li, Jizhou↗
DOE OSTI2021

A time-resolved, in-chamber x-ray pinhole imager for Z

We have commissioned a new time-resolved, x-ray imaging diagnostic for the Z facility. The primary intended application is for diagnosing the stagnation behavior of Magnetized Liner Inertial Fusion (MagLIF) and similar targets. We have a variety of imaging systems at Z, both time-integrated and time-resolved, that provide valuable x-ray imaging information, but no system at Z up to this time provides a combined high-resolution imaging with multi-frame time resolution; this new diagnostic, called TRICXI for Time Resolved In-Chamber X-ray Imager, is meant to provide time-resolved spatial imaging with high resolution. The multi-frame camera consists of a microchannel plate camera. A key component to achieving the design goals is to place the instrument inside the Z vacuum chamber within 2 m of the load, which necessitates a considerable amount of x-ray shielding as well as a specially designed, independent vacuum system. Here, a demonstration of the imaging capability for a series of MagLIF shots is presented. Predictions are given for resolution and relative image irradiance to guide experimenters in choosing the desired configuration for their experiments.

47 OTHER INSTRUMENTATION↗
DOE OSTI2021

Application of high-speed, species-specific chemiluminescence imaging for laminar flame speed and Markstein length measurements in spherically expanding flames

A high-speed chemiluminescence imaging diagnostic system has been developed and characterized for measuring species-specific properties of spherically expanding flames, with the objective of obtaining synchronized measurements of multiple flame properties from a single flame experiment. The imaging system comprises a high-speed camera coupled to a high-speed image intensifier and optical filters to isolate emission from desired excited species. Here this study validates the diagnostic scheme specifically for measuring laminar flame speed and Markstein length from chemiluminescence at three wavelength bands corresponding to OH*, CH*, and total chemiluminescence, respectively. Mixtures of methane-air and methane/ethane-air were tested at initial conditions of atmospheric pressure and room temperature. An under-utilized methodology for computing unburned Markstein length from burned Markstein length was implemented. Flame speed modeling of each mixture was conducted in Chemkin using AramcoMech 2.0. No significant differences were observed between the results derived from the three emission wavelength bands for the flame speeds nor the Markstein lengths. For both of these properties, excellent agreement was observed between the experimental results and the values reported in the literature. Because laminar flame speed and Markstein length show no dependency on the imaging wavelength, the present results imply that multiple flame properties, such as laminar flame speed, Markstein length, flame thickness, and excited-species intensity profiles, can all be acquired simultaneously for the same flame using this method.

42 ENGINEERING↗
DOE OSTI2022

Identification of a quasi-liquid phase at solid–liquid interface

Abstract An understanding of solid–liquid interfaces is of great importance for fundamental research as well as industrial applications. However, it has been very challenging to directly image solid–liquid interfaces with high resolution, thus their structure and properties are often unknown. Here, we report a quasi-liquid phase between metal (In, Sn) nanoparticle surfaces and an aqueous solution observed using liquid cell transmission electron microscopy. Our real-time high-resolution imaging reveals a thin layer of liquid-like materials at the interfaces with the frequent appearance of small In nanoclusters. Such a quasi-liquid phase serves as an intermediate for the mass transport from the metal nanoparticle to the liquid. Density functional theory-molecular dynamics simulations demonstrate that the positive charges of In ions greatly contribute to the stabilization of the quasi-liquid phase on the metal surface.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

A Systematic Interpretation of Subsurface Proppant Concentration from Drilling Mud Returns: Case Study from Hydraulic Fracturing Test Site (HFTS-2) in Delaware Basin

The aim of this study is generation and validation of a proppant log using analysis of drilling mud returns for child wells. Proppant log provides qualitative as well as quantitative insights into spatial distribution of proppant sand particles from prior stimulation of parent wells. While the basic methodology was developed and formalized during analysis of material collected from through fracture cores at Hydraulic Fracturing Test Site in Midland Basin (HFTS – 1), the test wells at HFTS – 2 in the neighboring Delaware Basin allowed the opportunity to validate the workflow on actual mud return samples from subsurface. As a child well is being drilled, periodic mud return samples are collected at the rig site and preserved for analysis. The workflow involves systematic cleaning of the samples including various steps such as washing, drying and segregation of samples into relevant size fractions of interest (< Mesh 20) based on specifications of pumped sand during stimulation of the parent well. Clean samples are imaged using high resolution transparency scanning. Scan images are then systematically analyzed for particles of interest using computer vision techniques. Sample counts are further validated using elemental analysis of smaller sub-samples at various depths of interest. This step is necessary to isolate proppant versus other naturally occurring minerals such as sulphates and carbonates which show similar optical properties. We successfully correlated proppant distribution against the existing parent well and validated propped versus relatively un-propped zones for a child well at the test site. The advantage of testing the proppant log concept at the HFTS – 2 site is the plethora of additional diagnostic data that is available to validate our primary observations. We can correlate spatial proppant distribution against variability in stimulation response based on independent observations such as image logs, microseismic attributes as well as DAS response, all of which tend to corroborate one another. One of our significant successes was being able to describe varying degrees of impact of the parent well along the lateral length of a stimulated child well. Our workflow represents a systematic and one-of-a-kind interpretation of spatial proppant distribution while drilling child wells. This provides unique opportunities to better understand the current state of the Downloaded from http://onepetro.org/URTECONF/proceedings-pdf/21URTC/2-21URTC/D021S031R003/2477415/urtec-2021-5189-ms.pdf/1 by Carol Worster on 28 February 2022 URTeC 5189 2 reservoir being targeted including zones which are likely more drained relative to others and how the planned completion of the child well can be improved. Lastly, this log can be useful is validating optimal well spacing in relatively new fields under development.

58 GEOSCIENCES↗
DOE OSTI2020

Performance of Scintillation Detectors Based on Quantum Dots in a Semiconductor Matrix (Final Technical Report)

InAs Quantum Dots (QDs) embedded into GaAs semiconductor waveguide have unique scintillation properties, valuable for nuclear security, medical imaging, and high energy physics. In this work, we developed thick (~25um) epitaxial heterostructres with high luminescence efficiency composed of self-assembled nano-engineered InAs QDs grown by molecular beam epitaxy. In this type of detector, the GaAs matrix acts as a stopping material for charged particles or photons generating electrons captured by the QDs acting as luminescence centers. The QD medium is designed to provide fast capture of electrons into QDs (few ps), high QD luminescence efficiency at room temperature (>50%), and strong red-shift of photoluminescence (PL) from the GaAs absorption edge (>250nm). Typical devices consist of a 10-25um thick GaAs layer with embedded sheets of modulation p-type doped InAs QDs and an InGaAs photodetector tuned to the QD emission wavelength. The thick GaAs layer acts also as a waveguide when layer-transferred onto a low-index substrate. Waveguiding and self-absorption (~1cm -1 ) were studied using photoluminescence with scanning laser excitation and modeled with ray optics approximation and geometrical coupling of high-index waveguide to a collection fiber. Scintillating signals from α-particles were analyzed with both an external photodiode (PD) and an integrated PD which provided an improved optical coupling. In the former case, the external InGaAs PD was air-coupled to the scintillator and had the light collection efficiency of about 1% corresponding to limited light extraction through a planar interface with air due to total internal reflection. The mean charge collected by the integrated PD was in the range of (3÷5)×10 4 photoelectrons per 1 MeV of deposited energy, or ~13-20% of the theoretically achievable light yield. Timing of the integrated device was measured by wire-bonding it to the input of an 8 GHz IC. The scintillation response shows an extremely fast 0.3-0.6 ns decay constant and about 40-70 ps time resolution, limited by the system noise. The combined light yield and decay time makes the InAs/GaAs QD heterostructures the fastest high yield scintillation material reported making it valuable for high energy physics and medical imaging applications.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
NASA NTRS1981

An algorithm for spatial heirarchy clustering

A method for utilizing both spectral and spatial redundancy in compacting and preclassifying images is presented. In multispectral satellite images, a high correlation exists between neighboring image points which tend to occupy dense and restricted regions of the feature space. The image is divided into windows of the same size where the clustering is made. The classes obtained in several neighboring windows are clustered, and then again successively clustered until only one region corresponding to the whole image is obtained. By employing this algorithm only a few points are considered in each clustering, thus reducing computational effort. The method is illustrated as applied to LANDSAT images.

Dejesusparada, N.↗
NASA NTRS1983

The X-ray morphology of Abell 1367

X-ray observations of the nearby cluster Abell 1367 were made with the Imaging Proportional Counter (IPC) and High Resolution Imager (HRI) aboard the Einstein Observatory. The IPC is used to study the diffuse cluster emission. With the HRI, eight point sources are detected above the diffuse cluster emission, three of which are apparently associated with cluster galaxies. In addition, the HRI observations have resolved 13 extended features with characteristic radii of order arcmin, eight of which are associated with cluster galaxies. These extended sources have luminosities of 1.5-6.5 x 10 to the 41st per (H0)50)-squared ergs per sec in the 0.5-4.5 keV band and constitute about 60% of the total cluster emission. The ways in which these hot galactic coronae can be maintained are discussed.

Bechtold, J.↗
NASA NTRS1983

X-ray ionization and the Orion molecular cloud

Recent observations of the Orion Nebula with the imaging proportional counter and the high resolution imager on the Einstein Observatory satellite have revealed that the presumably young stars in that region are strong X-ray emitters. The densest portion of the molecular cloud, which is also the portion with the greatest diversity of molecular species, is a few square arc minutes in size, while its conventional center (the KL Nebula) lies within an arc minute of the peak of the X-ray emission. The X-rays from the stars impinge on the neighboring molecular cloud's core with such intensity that they significantly affect its ionization equilibrium and chemistry. The present investigation has the objective to provide a quantitative account of these effects. Attention is given to simple estimates of the magnitude of X-ray ionization and its variation throughout the cloud, ionization and reaction rates, and a choice of models.

Krolik, J. H.↗
NASA NTRS1983

Optical and X-ray observations of faint quasars in an optically selected sample

The confirmation of six quasars from spectrographic observations made in 1981 using the Multiple Mirror Telescope, and the characterization of 10 quasars from 1980 Einstein-Observatory X-ray observations (using both imaging proportional counter and high-resolution imager), are reported. The candidates had been selected by Formiggini et al. (1980) in a 1.72-sq-deg region centered on 13h 6 deg, on the basis of ultraviolet excess and a limiting B magnitude of 19.20. A total sample of 10 UV-excess quasars of this magnitude has now been confirmed, for an integral surface density of 5.8 + or - 1.8 per sq deg. Confirmation of three objects from another sample with B less than 18.25 as quasars yielded a surface density of 0./59 + or - 0.13 per sq deg at that magnitude. Data from the complete samples were used to compute the number-flux relation, found to be described by a power law with a 2.25 index for quasars with B between 17.0 and 19.2. From the X-ray observations it was determined that quasars with z less than 2.2 and B less than 19.20 contribute about 15 percent to the cosmic 2-keV background.

Marshall, H. L.↗
NASA NTRS1984

The vectorization of a ray tracing program for image generation

Ray tracing is a widely used method for producing realistic computer generated images. Ray tracing involves firing an imaginary ray from a view point, through a point on an image plane, into a three dimensional scene. The intersections of the ray with the objects in the scene determines what is visible at the point on the image plane. This process must be repeated many times, once for each point (commonly called a pixel) in the image plane. A typical image contains more than a million pixels making this process computationally expensive. A traditional ray tracing program processes one ray at a time. In such a serial approach, as much as ninety percent of the execution time is spent computing the intersection of a ray with the surface in the scene. With the CYBER 205, many rays can be intersected with all the bodies im the scene with a single series of vector operations. Vectorization of this intersection process results in large decreases in computation time. The CADLAB's interest in ray tracing stems from the need to produce realistic images of mechanical parts. A high quality image of a part during the design process can increase the productivity of the designer by helping him visualize the results of his work. To be useful in the design process, these images must be produced in a reasonable amount of time. This discussion will explain how the ray tracing process was vectorized and gives examples of the images obtained.

Plunkett, D. J.↗
NASA NTRS1984

The rationale and suggested approaches for research geosynchronous satellite measurements for severe storm and mesoscale investigations

The measurements from current and planned geosynchronous satellites provide quantitative estimates of temperature and moisture profiles, surface temperature, wind, cloud properties, and precipitation. A number of significant observation characteristics remain, they include: (1) temperature and moisture profiles in cloudy areas; (2) high vertical profile resolution; (3) definitive precipitation area mapping and precipitation rate estimates on the convective cloud scale; (4) winds from low level cloud motions at night; (5) the determination of convective cloud structure; and (6) high resolution surface temperature determination. Four major new observing capabilities are proposed to overcome these deficiencies: a microwave sounder/imager, a high resolution visible and infrared imager, a high spectral resolution infrared sounder, and a total ozone mapper. It is suggested that the four sensors are flown together and used to support major mesoscale and short range forecasting field experiments.

Shenk, W. E.↗
NASA NTRS1985

The Einstein soft X-ray survey of the Pleiades

The results of a 0.1-4.5-keV X-ray survey of a 2 x 2-deg area centered on the Pleiades open cluster, performed using the imaging proportional counter and high-resolution imager of the Einstein Observatory on four days in 1980-1981, are presented in extensive tables, graphs, maps, histograms, and finding charts and characterized. A total of 61 sources are detected, and 44 of these are identified with cluster members of spectral types B-M. Findings discussed include Lx/Lbol of 10 the -7th for early-type stars; F-star mean Lx like that of F stars in the Hyades and in the field (denying time evolution of Lx); mean G-star Lx = 3.7 x 10 to the 29th erg/sec; G-star activity decay more gradual than 1/sq rt t, with sharp fall for t greater than 1 Gyr; and no evidence for X-ray-emissivity/rotational-velocity correlation in a homogeneous sample of K dwarfs or a sample of K and M stars with established V sin i data.

Caillault, J.-P.↗
NASA NTRS1987

Future U.S. ocean color missions - OCI, MODIS and HIRIS

NASA has been working to develop an Ocean Color Imager (OCI). The Earth Observing Satellite Company (EOSAT) is considering flying an ocean and land wide-field color instrument which would meet specified requirements on Landsat 6 or 7 planned for launch in 1989 and 1991, respectively. It would provide eight ocean color channels for improved atmospheric correction and in-water algorithms, global coverage and near real-time data for operational uses. In the mid 1990's NASA is planning to fly a Moderate Resolution Imaging Spectrometer (MODIS) and a High Resolution Imaging Spectrometer (HIRIS) as part of the Earth Observing System on the Polar Platform of the Space Station. These instruments are array spectrometers which would provide full spectral resolution in the visible and infrared. This opens the possibility of separating different groups of phytoplankton, suspended sediments and other substances in the water.

Davis, C. O.↗
NASA NTRS1988

Earth Observing System - A platform for imaging spectrometers

Several advanced imaging spectrometers will be deployed on the Space Station Polar Platforms as a part of the Earth Observing System (EOS) program. Two of these, the Moderate-Resolution Imaging Spectrometer (MODIS) and High-Resolution Imaging Spectrometer (HIRIS), will be provided as facility instruments, and currently are under conceptual study at the Jet Propulsion Laboratory and the Goddard Space Flight Center. Other imaging spectrometer concepts, including proposals for a thermal infrared imaging spectrometer, are expected in response to the EOS Announcement of Opportunity scheduled for release in January of 1988.

Vane, Deborah↗
NASA NTRS1990

Technology challenges for large spacecraft optical systems

The technology challenges posed by future NASA astrophysics missions in the visible region of the spectrum whose goals include making high resolution images of faint objects, and high accuracy measurements of the positions of brighter objects for dynamical studies are discussed. Concentration is on the problems associated with possible next generation great observatories in space in the post-Hubble Space Telescope, particularly those with partially filled apertures. Telescopes using interferometric techniques in the visible similar to those of radio VLBI hold the promise of providing high resolution astronomical measurements within reasonable launch constraints on mass and volume. Technology challenges in the optics, structures, and controls areas are addressed.

Synnott, S. P.↗
NASA NTRS1992

Remote sensing of surface hemispherical reflectance (albedo) using pointable multispectral imaging spectroradiometers

Remote techniques for determining albedo are examined in terms of the range of view angles required in the use of string techniques with the Moderate Resolution Imaging Spectroradiometer (MODIS) and the High Resolution Imaging Spectroradiometer (HIRIS). Ground data are used to compute full and half strings out to 15, 30, 45, and 60 degrees for various sun angles and ground cover types. A knowledge-based system is employed to evaluate both the visible and near-IR bands, and the results indicate errors of up to 7 percent for the MODIS data, HIRIS data, and the full-string +/- 60 degrees. In the cases of large extrapolations greater ranges of error are noted indicating that 60-deg systems are most effective. The error is increased in the case of sensor systems that only view in the fore or aft direction, and the MODIS full string for +/- 45 deg is also considered a good system.

Kimes, D. S.↗
NASA NTRS1998

Pixel Paradise

PixelVision, Inc., has developed a series of integrated imaging engines capable of high-resolution image capture at dynamic speeds. This technology was used originally at Jet Propulsion Laboratory in a series of imaging engines for a NASA mission to Pluto. By producing this integrated package, Charge-Coupled Device (CCD) technology has been made accessible to a wide range of users.

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