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At least 595 records · Page 33

Acousto-ultrasonic characterization of fiber reinforced composites

The acousto-ultrasonic technique combines advantageous aspects of acoustic emission and ultrasonic methodologies. Acousto-ultrasonics operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is complex, but it can be quantitized in terms of a 'stress wave factor.' The stress wave factor, which can be defined in a number of ways, is a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect appears in the stress wave factor.

Vary, A.↗

Acousto-ultrasonic characterization of fiber reinforced composites

The acousto-ultrasonic technique combines advantageous aspects of acoustic emission and ultrasonic methodologies. Acousto-ultrasonics operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is quite complex, but it can be quantitized in terms of a 'stress wave factor'. The stress wave factor, which can be defined in a number of ways, is essentially a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect will appear in the stress wave factor.

Vary, A.↗

Sub-T/g/ annealing studies of advanced epoxy-matrix graphite-fiber-reinforced composites

Annealing at temperatures below the glass transition temperature (sub-T/g/ annealing) in structural epoxy network glasses is found to affect long-term mechanical properties of symmetrically (+ or - 45 deg) reinforced 16-lamina graphite/epoxy composites. Post-cured specimens of Thornel 300 graphite/Narmco 5208 epoxy are sub-T(g) annealed at 140 C for about 10, 100, 1000, 10,000, and 100,000 min with a prior quenching above T(g). The ultimate tensile strength, strain-to-break, and static toughness of the composite materials are found to decrease as a function of sub-T(g) annealing time, while no weight loss is observed. Time-dependent changes in properties are explained by a physical aging concept based on free-volume decreases in the nonequilibrium glassy state of network epoxies, and results imply that changes in composite properties may occur with the service time.

Kong, E. S. W.↗

An inherent instability in fiber-reinforced composite laminates

Presented is a theory to predict the room-temperature shape of unsymmetric laminates. The theory is an extension of classical lamination theory and includes the effects of geometric nonlinearities. It is shown that the saddle shape predicted by the classical theory can actually be an unstable shape and a laminate will assume a cylindrical shape instead. The phenomena is coupled to the length, width, and thickness of the laminate.

Hyer, M. W.↗

Acousto-ultrasonic characterization of fiber reinforced composites

The advantageous aspects of acoustic emission and ultrasonic methodologies are combined in a technique which operates by introducing a repeating series of ultrasonic pulses into a material. The waves introduced simulate the spontaneous stress waves that would arise if the material were put under stress as in the case of acoustic emission measurements. These benign stress waves are detected by an acoustic emission sensor. The physical arrangement of the ultrasonic (input) transducer and acoustic emission (output) sensor is such that the resultant waveform carries an imprint of morphological factors that govern or contribute to material performance. The output waveform is quite complex, but it can be quantitized in terms of a "stress wave factor". The stress wave factor, which can be defined in a number of ways, is essentially a relative measure of the efficiency of energy dissipation in a material. If flaws or other material anomalies exist in the volume being examined, their combined effect will appear in the stress wave factor.

Vary, A.↗

Effect of Ionizing Radiation on the Mechanical and Structural Properties of Graphite Fiber Reinforced Composites

Graphite/epoxy (T300/5208) and graphite/polyimide composites (C6000/PMR 15) were exposed to various levels of 0.5 MeV electron radiation with the maximum dose being 10,000 Mrad. A three point bending test was used to evaluate the ultimate stress and modulus of the composites. In all composites except transverse samples of C6000/PMR 15 ultimate stress values remained approximately constant or increased slightly. The modulus values remained approximately constant for all composite types regardless of the radiation level. Interfacial aspects of composites were studied. Interlaminar shear tests were performed on T300/5208 and C6000/PMR 15 composites irradiated to 10,000 Mrad. There was an initial increase in interlaminar shear strength (up to 1,000 Mrad) followed by a sharp decrease with further radiation exposure. Using scanning electron microscopy no visual differences in the mode of fracture could be detected between ruptured control samples and those exposed to various levels of radiation. Electron spectroscopy for chemical analysis (ESCA) revealed little change in the surface elements present in control and highly irradiated T300/5208 composite samples.

Wolf, Kay Woodroof↗

Preliminary design methods for fiber reinforced composite structures employing a personal computer

The objective of this project was to develop a user-friendly interactive computer program to be used as an analytical tool by structural designers. Its intent was to do preliminary, approximate stress analysis to help select or verify sizing choices for composite structural members. The approach to the project was to provide a subroutine which uses classical lamination theory to predict an effective elastic modulus for a laminate of arbitrary material and ply orientation. This effective elastic modulus can then be used in a family of other subroutines which employ the familiar basic structural analysis methods for isotropic materials. This method is simple and convenient to use but only approximate, as is appropriate for a preliminary design tool which will be subsequently verified by more sophisticated analysis. Additional subroutines have been provided to calculate laminate coefficient of thermal expansion and to calculate ply-by-ply strains within a laminate.

Eastlake, C. N.↗

Surface generation and detection of coupled fiber-matrix mode acoustic wave propagation in fiber-reinforced composites

A technique is described that makes it possible to transmit and receive bulk ultrasonic waves launched from the same surface of a composite sheet by means of transducers mounted on variable angle blocks. A straightforward approach to measure the velocity and attenuation of this wave is presented. A bulk compressional wave of 930,000 cm/sec velocity was launched and received in this manner in an 8-ply unidirectional T-300-5208 epoxy composite. Preliminary results indicate that parameters associated with this wave might be sensitive to accumulated damage in a composite; thus, the technique has a potential for NDE in structures made from composite materials.

Yost, W. T.↗

Fatigue In Continuous-Fiber/Metal-Matrix Composites

Report describes experimental approaches to quantification of fatigue damage in metal-matrix composites (MMC's). Discusses number of examples of development of damage and failure along with associated analytical models of behavior of MMC. Objectives of report are twofold. First, present experimental procedures and techniques for conducting meaningful fatigue tests to detect and quantify fatigue damage in MMC's. Second, present examples of how fatigue damage initiated and grows in various MMC's. Report furnishes some insight into what type of fatigue damage occurs and how damage quantified.

Johnson, William S.↗

Void effects on the interlaminar shear strength of unidirectional graphite-fiber-reinforced composites

A study was conducted to evaluate the effect of voids on the interlaminar shear strength (ILSS) of a polyimide matrix composite system. The graphite/PMR-15 composite was chosen for study because of the extensive amount of experience that has been amassed in the processing of this material. Void contents were calculated and the void geometry and distribution were noted using microscope techniques such as those used in metallography. A good empirical correlation between ILSS and composite density was found. The most acceptable relationship between the ILSS and density was found to be a power equation that closely resembles theoretically derived expressions. It was found that void-free composites could be processed in matched metal die molds at pressures greater than 1.4 MPa and less than 6.9 MPa.

Bowles, Kenneth J.↗

Monitoring Loads In Fiber-Reinforced Composite Materials

In new method of determining load on specimen, direction of stress wave propagation measured by array of acoustic sensors attached to specimen. Responses of sensors analyzed by strain-energy-density calculations to calculate load. Change in anisotropy of elasticity caused by applied load and corresponding induced strain. Is means to monitor applied load corresponding to measurable shift in direction of propagation of stress wave. Monitoring device based on this method made integral part of airframe in which unidirectional section of structure, such as spar cap or longeron, carries primary load.

Prosser, William H.↗

Leveling coatings for reducing the atomic oxygen defect density in protected graphite fiber epoxy composites

Pinholes or other defect sites in a protective oxide coating provide pathways for atomic oxygen in low Earth orbit to reach underlying material. One concept for enhancing the lifetime of materials in low Earth orbits is to apply a leveling coating to the material prior to applying any reflective and protective coatings. Using a surface tension leveling coating concept, a low viscosity epoxy was applied to the surface of several composite coupons. A protective layer of 1000 A of SiO2 was deposited on top of the leveling coating, and the coupons were exposed to an atomic oxygen environment in a plasma asher. Pinhole populations per unit area were estimated by counting the number of undercut sites observed by scanning electron microscopy. Defect density values of 180,000 defects/sq cm were reduced to about 1000 defects/sq cm as a result of the applied leveling coating. These improvements occur at a mass penalty of about 2.5 mg/sq cm.

Jaworske, D. A.↗

Leveling coatings for reducing the atomic oxygen defect density in protected graphite fiber epoxy composites

Pinholes or other defect sites in a protective oxide coating provide pathways for atomic oxygen in low Earth orbit to reach underlying material. One concept of enhancing the lifetime of materials in low Earth orbit is to apply a leveling coating to the material prior to applying any reflective and protective coatings. Using a surface tension leveling coating concept, a low viscosity epoxy was applied to the surface of several composite coupons. A protective layer of 1000 A of SiO2 was deposited on top of the leveling coating, and the coupons were exposed to an atomic oxygen environment in a plasma asher. Pinhole populations per unit area were estimated by counting the number of undercut sites observed by scanning electron microscopy. Defect density values of 180,000 defects/sq cm were reduced to about 1000 defects/sq cm as a result of the applied leveling coating. These improvements occur at a mass penalty of about 2.5 mg/sq cm.

Jaworske, D. A.↗

Ceramic matrix composites (continuous fiber reinforced) thermal protection systems

Concluded remarks are: (1) advanced carbon-carbon (ACC) substrate fabrication technology in good shape; (2) ACC coating improvements satisfactory but additional work needed; (3) non-destructive test techniques to monitor hardware during operational life needed; and (4) cost reduction approaches a high priority.

Riccitiello, Salvatore R.↗

Sensor-model prediction, monitoring and in-situ control of liquid RTM advanced fiber architecture composite processing

In-situ frequency dependent electromagnetic sensors (FDEMS) and the Loos resin transfer model have been used to select and control the processing properties of an epoxy resin during liquid pressure RTM impregnation and cure. Once correlated with viscosity and degree of cure the FDEMS sensor monitors and the RTM processing model predicts the reaction advancement of the resin, viscosity and the impregnation of the fabric. This provides a direct means for predicting, monitoring, and controlling the liquid RTM process in-situ in the mold throughout the fabrication process and the effects of time, temperature, vacuum and pressure. Most importantly, the FDEMS-sensor model system has been developed to make intelligent decisions, thereby automating the liquid RTM process and removing the need for operator direction.

Kranbuehl, D.↗

Scale effects in the response and failure of fiber reinforced composite laminates loaded in tension and in flexure

The feasibility of using scale model testing for predicting the full-scale behavior of flat composite coupons loaded in tension and beam-columns loaded in flexure is examined. Classical laws of similitude are applied to fabricate and test replica model specimens to identify scaling effects in the load response, strength, and mode of failure. Experiments were performed on graphite-epoxy composite specimens having different laminate stacking sequences and a range of scaled sizes. From the experiments it was deduced that the elastic response of scaled composite specimens was independent of size. However, a significant scale effect in strength was observed. In addition, a transition in failure mode was observed among scaled specimens of certain laminate stacking sequences. A Weibull statistical model and a fracture mechanics based model were applied to predict the strength scale effect since standard failure criteria cannot account for the influence of absolute specimen size on strength.

Jackson, Karen E.↗

Dimensionally stable, graphite-fiber reinforced composite mirror technology

A research project intended to design and fabricate a dimensionally stable 2 mu spherical mirror 0.4 m in diameter, carried out by Composite Optics, Incorporated, is briefly reported. A laminate for the facesheet and the back surface that is intended to be exceptionally uniform in-plane has been designed using the P75/ERL 1999 material. The core is designed to be pseudoisotropic in all three directions.

Kulick, Shel↗