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A proposed solution to the challenges of disposal of greater than class C low-level radioactive waste - 15172

In 1982, the US Nuclear Regulatory Commission (NRC) adopted rules for the disposal of low-level radioactive waste. These rules established new standards for the siting, construction, operation and closure of low-level radioactive waste disposal facilities. The new rules also set out a classification system for low-level radioactive waste based on half-life and concentration of the radionuclides in the waste stream. The defined classes - Class A, Class B and Class C - were based on increasing toxicity with Class A being the least hazardous and Class C being relatively more hazardous. Radioactive waste that could not fit the classification scheme due to its long half-life or its high concentration of radioactive material was deemed to be greater than Class C low-level radioactive waste, with the ascribed acronym 'GTCC' low-level radioactive waste. Such waste was deemed not suitable for shallow land disposal based on the design standards for low-level radioactive waste landfills in place at that time. This resulted in a radioactive waste stream that had no disposal option. To remedy this problem, the US Congress in 1985 stipulated that the US Department of Energy would be responsible for the disposal of GTCC waste. Subsequently, the NRC amended its regulations to require GTCC low-level waste to be disposed in a geologic repository unless the Commission approved proposals for disposal in a low-level radioactive waste disposal facility. The Commission did not concurrently establish any specific technical requirements for GTCC disposal in a low-level radioactive waste disposal facility, but did infer that a site-specific performance analysis could be conducted in support of any proposal for land disposal of such waste. In light of this, Waste Control Specialists LLC (WCS) has conducted such a site-specific performance analysis that has indicated the disposal facility at Andrews Texas will perform satisfactorily as a disposal facility for certain types and quantities of GTCC waste. Concurrently with this analysis, WCS has submitted to the Texas Commission on Environmental Quality a petition for rulemaking that will permit disposal of GTCC waste in their disposal facility. This paper summarizes the technical and legal analyses that were conducted in support of the proposed rulemaking. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Development of the 3 m{sup 3} Low Level Radioactive Waste Container in Taiwan - 20037

Chinshan Nuclear Power Plant stopped its business operation in July, 2019, and Kuosheng Nuclear Power Plant will also be permanently shut down in 2023. Nuclear Reactor Facilities Regulation Act requires a nuclear facility must be dismantled in 25 years after being permanently ceased operation. According to the approved decommissioning plan of Chinshan Nuclear Power Plant and the proposed one of Kuosheng Nuclear Power Plant, the 3 m{sup 3} low level radioactive waste container is planned to store the low level radioactive wastes with higher radiation produced during the decommissioning. However, 3 m{sup 3} low level radioactive waste containers are not used or developed in Taiwan before. To meet such need, Institute of Nuclear Energy Research develops a new type of 3 m{sup 3} low level radioactive waste container and performs the corresponding analyses and tests based on Guidelines of Applying the Usage License of Low Level Radioactive Waste Containers and Regulations for the Safe Transport of Radioactive Material. In this article, it provides the information of the low level radioactive waste containers that have been approved or is under reviewing in Taiwan, and so do the design specifications of the developed 3 m{sup 3} waste container. Besides, the numerical evaluation and test results of the developed 3 m{sup 3} waste container are also included in this article. Based on the evaluation and test results, the developed 3 m{sup 3} waste container satisfies the requirements of the storage container and industrial package type 2. Institute of Nuclear Energy Research will submit the usage license applications to the authority this year, and the usage licenses would be granted in 2021, expectedly. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Understanding Contamination; Twenty Years of Simulating Radiological Contamination

A wide variety of simulated contamination methods have been developed by researchers to reproducibly test radiological decontamination methods. Some twenty years ago a method of non-radioactive contamination simulation was proposed at the Idaho National Laboratory (INL) that mimicked the character of radioactive cesium and zirconium contamination on stainless steel. It involved baking the contamination into the surface of the stainless steel in order to 'fix' it into a tenacious, tightly bound oxide layer. This type of contamination was particularly applicable to nuclear processing facilities (and nuclear reactors) where oxide growth and exchange of radioactive materials within the oxide layer became the predominant model for material/contaminant interaction. Additional simulation methods and their empirically derived basis (from a nuclear fuel reprocessing facility) are discussed. In the last ten years the INL, working with the Defense Advanced Research Projects Agency (DARPA) and the National Homeland Security Research Center (NHSRC), has continued to develop contamination simulation methodologies. The most notable of these newer methodologies was developed to compare the efficacy of different decontamination technologies against radiological dispersal device (RDD, 'dirty bomb') type of contamination. There are many different scenarios for how RDD contamination may be spread, but the most commonly used one at the INL involves the dispersal of an aqueous solution containing radioactive Cs-137. This method was chosen during the DARPA projects and has continued through the NHSRC series of decontamination trials and also gives a tenacious 'fixed' contamination. Much has been learned about the interaction of cesium contamination with building materials, particularly concrete, throughout these tests. The effects of porosity, cation-exchange capacity of the material and the amount of dirt and debris on the surface are very important factors. The interaction of the contaminant/substrate with the particular decontamination technology is also very important. Results of decontamination testing from hundreds of contaminated coupons have lead to certain conclusions about the contamination and the type of decontamination methods being deployed. A recent addition to the DARPA initiated methodology simulates the deposition of nuclear fallout. This contamination differs from previous tests in that it has been developed and validated purely to simulate a 'loose' type of contamination. This may represent the first time that a radiologically contaminated 'fallout' stimulant has been developed to reproducibly test decontamination methods. While no contaminant/methodology may serve as a complete example of all aspects that could be seen in the field, the study of this family of simulation methods provides insight into the nature of radiological contamination.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

The radium industry in France and the remediation of polluted sites - 15256

According to the French Law of 28 June 2006 relative to the management of radioactive materials and waste, Andra is in charge of a public service mission that involves the clean-up of orphan sites that have been polluted by radioactivity. Andra is currently working, or has worked in the past, on around thirty sites in mainland France. The clean-up strategy is selected after a comparative analysis of the cost and the advantages of the different scenarios based on the ALARA principle. Whenever reasonable, Andra tries to achieve total clean-up, so that the site can be re-used without any constraint. However, for certain cases, it is opted for a less ambitious scenario, which means restricting the possibilities of use of the site after clean-up. In all cases, the chosen scenarios guarantee that there will be no radiological impact on the planned new use of the site. If the site is an orphan site, a National Advisory Committee for Public Funding in the field of Radioactivity (known as CNAR) decides which scenario presents the best cost-benefit profile and whether to provide public subsidies to fund the work. The multidisciplinary composition of the CNAR, with members from public administrations and organizations, politicians, qualified personalities and non-governmental organizations, guarantees a decision that has been carefully considered from all aspects. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Lessons Learned From the Cesium Pond Soil Shipping Campaign at Whiteshell Laboratories - 18206

Whiteshell Laboratories (WL), located in Manitoba, Canada is the first major decommissioning project of a nuclear research establishment in Canada. With the focus now active remediation to return the site to green state, the majority of legacy radioactive waste and waste generated from decommissioning and demolition of nuclear facilities must be transported off site to Chalk River Laboratories (CRL), located in Ontario, Canada. No large radioactive waste shipment campaigns have been undertaken by WL until now. A newly established Waste Management Program specifically designed to support the WL Closure Project has executed its first major shipping campaign of radioactive material, making approximately one hundred shipments and reducing WL's total volume of low-level radioactive waste to transport by seven percent. The shipped waste was approximately 1800 m{sup 3} (2600 metric tons) of known Cs-137 contaminated soil material generated from the excavation of an Experimental Cesium Pond Project designed to study the distribution of dose received by organisms living at the mud-water interface from Cs-137 contamination. This paper outlines the cost benefit analysis undertaken to determine the most cost effective method for transporting the radioactively contaminated soil to CRL, storage challenges experienced by both WL and CRL, the selection of the most appropriate waste package, training of shippers, and the continual optimization of increasing the number of generated waste packages and the number of waste packages shipped and accepted at CRL. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Production of an impermeable composite of irradiated graphite and glass by hot isostatic pressing as a long term leach resistant waste form

Around 250,000 tons of irradiated graphite (i-graphite) exists worldwide and can be considered as a current waste or future waste stream. The largest national i-graphite inventory is located in UK (∼ 100,000 tons) with significant quantities also in Russia and France [5]. Most of the i-graphite remains in the cores of shutdown nuclear reactors including the MAGNOX type in UK and the UNGG in France. Whilst there are still operational power reactors with graphite cores, such as the Russian RBMKs and the AGRs in UK, all of them will reach their end of life during the next two decades. The most common reference waste management option of i-graphite is a wet or dry retrieval of the graphite blocks from the reactor core and the grouting of these blocks in a container without further conditioning. This produces large waste package volumes because the encapsulation capacity of the grout is limited and large cavities in the graphite blocks could reduce the packing densities. Packing densities from 0.5 to 1 tons per cubic meter have been assumed for grouting solutions. Furthermore the grout is permeable. This could over time allow the penetration of aqueous phases into the waste block and a potential dissolution and release of radionuclides. As a result particularly highly soluble radionuclides may not be retained by the grout. Vitrification could present an alternative, however a similar waste package volume increase may be expected since the encapsulation capacity of glass is potentially similar to or worse than that of grout. FNAG has developed a process for the production of a graphite-glass composite material called Impermeable Graphite Matrix (IGM) [3]. This process is also applicable to irradiated graphite which allows the manufacturing of an impermeable material without volume increase. Crushed i-graphite is mixed with 20 vol.% of glass and then pressed under vacuum at an elevated temperature in an axial hot vacuum press (HVP). The obtained product has zero or negligible porosity and a water impermeable structure. Structural analysis shows that the glass in the composite has replaced the pores in the graphite structure. The typical pore volume of a graphite material is in the range of 20 vol.%. Therefore no volume increase will occur in comparison with the former graphite material. This IGM material will allow the encapsulation of graphite with package densities larger than 1.5 ton per cubic meter. Therefore a huge volume saving can be achieved by such an alternative encapsulation method. Disposal performance is also enhanced since little or no leaching of radionuclides is observed due to the impermeability of the material NNL and FNAG have proved that IGM can be produced by hot isostatic pressing (HIP) which has several advantages for radioactive materials over the HVP process. - The sealed HIP container avoids the release of any radionuclides. - The outside of the waste package is not contaminated. - The HIP process time is shorter than the HVP process time. The isostatic press avoids anisotropic density distributions. - Simple filling of the HIP container has advantages over the filling of an axial die. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Space reactor assessment and validation study

The present difficulties experienced by the United States in launching payloads into space has suggested a number of problems which are associated with the handling of hazardous materials in spacecraft. The question has arisen as to the safety of launching highly radioactive material such as plutonium-238, related to the possibility of its dispersion into the atmosphere during a launch vehicle explosion. An alternative is the use of a small nuclear reactor which is not started until it is in space and contains little or no radioactivity at launch. A first order assessment of six small reactor concepts with power levels up to 100 MWe was performed. Both the nuclear feasibility of these concepts to operate at their rated power levels between 7 and 10 years and the capability of these concepts to remain subcritical both before and during launch and also in the case of water immersion during a potential launch failure or abort were investigated.

Gedeon, Stephen↗

Advancing Vision-based Feedback and Convolutional Neural Networks for Visual Outlier Detection

Machine learning has matured into a technology that has immediate applicability to the surveillance needs of nuclear material storage containers. These containers at LANL are the barrier preventing release of radioactive material to the workers, public, and environment during the storage period of the material. Annual surveillance activities can only provide coverage on a handful of containers. There is a significant need for surveillance tools to identify potential issues and precursors to containment failure that can be used during opportunistic inspections and, more generally, outside of annual surveillance activities. In this report we provide details on the advancement of our proposed embodiment that combines an automation system for taking pictures and a high-accuracy machine learning-driven object detection software. We further showcase the improvements on the software side with progress on extracting unique identification features and advances in detecting damage. The current state of the system captures subject matter expert training and a space-conscious design whose implementation is envisioned in the near future.

98 NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL P↗

Case Study of Urban Residential Remediation and Restoration in Port Hope, Canada - 13250

The Canadian Municipality of Port Hope, Ontario, is located some 100 km east of Toronto and has been the location of radium and/or uranium refining since the 1930's. Historically, these activities involved materials containing radium-226, uranium, arsenic and other contaminants generated by the refining process. In years past, properties and sites in Port Hope became contaminated from spillage during transportation, unrecorded, un-monitored or unauthorized diversion of contaminated fill and materials, wind and water erosion and spread from residue storage areas. Residential properties in Port Hope impacted by radioactive materials are being addressed by the Canadian federal government under programs administered by the Low-Level Radioactive Waste Management Office (LLRWMO) and the Port Hope Area Initiative Management Office (PHAIMO). Issues that currently arise at these properties are addressed by the LLRWMO's Interim Waste Management Program (IWM). In the future, these sites will be included in the PHAIMO's Small Scale Sites (SSS) remedial program. The LLRWMO has recently completed a remediation and restoration program at a residential property in Port Hope that has provided learnings that will be applicable to the PHAIMO's upcoming SSS remedial effort. The work scope at this property involved remediating contaminated refinery materials that had been re-used in the original construction of the residence. Following removal of the contaminated materials, the property was restored for continued residential use. This kind of property represents a relatively small, but potentially challenging subset of the portfolio of sites that will eventually be addressed by the SSS program. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Evaluation of Recent Trailer Contamination and Supersack Integrity Issues

During the period from fiscal year (FY) 2009 to FY 2011, there were a total of 21 incidents involving radioactively contaminated shipment trailers and 9 contaminated waste packages received at the Nevada National Security Site (NNSS) Area 5 Radioactive Waste Management Site (RWMS). During this time period, the EnergySolutions (ES) Clive, Utah, disposal facility had a total of 18 similar incidents involving trailer and package contamination issues. As a result of the increased occurrence of such incidents, DOE Environmental Management Headquarters (EM/HQ) Waste Management organization (EM-30) requested that the Energy Facility Contractors’ Group (EFCOG) Waste Management Working Group (WMWG) conduct a detailed review of these incidents and report back to EM-30 regarding the results of this review, including providing any recommendations formulated as a result of the evaluation of current site practices involving handling and management of radioactive material and waste shipments.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Overview of IAEA MODARIA II Program Working Group 1 on Assessment and Decision Making of Existing Exposure Situations for NORM and Nuclear Legacy Sites - 18308

The International Atomic Energy Agency (IAEA) launched the Modelling and Data for Radiological Impact Assessments (MODARIA) II Programme in October. As part of the IAEA effort to enhance the capabilities of its Member States in assessing radiological impacts of radionuclides released to the environment from sites that were not operated in accordance with current standards, and to ensure protection of the public and the environment, the MODARIA II Programme aims to: (1) test the performance of models developed for predicting the transfer of radionuclides in the environment and assessing radiological impacts to the public and the environment; (2) develop and improve models for particular environments and, where appropriate, to agree on data sets that are generally applicable for use in testing environmental transfer models; and (3) provide an international forum for the exchange of experiences, ideas and research information. The Programme will run for 3 years from 2016 to 2019. The Programme comprises seven working groups covering a wide range of topics (https://wwwns.iaea.org/projects/modaria/modaria2.asp?s=8 and l=129). MODARIA II Working Group 1 (WG1) is focused on dose assessment and decision making regarding existing exposure situations due to naturally occurring radioactive material (NORM) and nuclear legacy sites. WG1 was formed as a combination of two MODARIA I WGs: WG1 focused on application of decision-aiding tools in remediation; and WG3 focused on risk assessment for NORM and radioactively contaminated legacy sites (https://wwwns.iaea.org/projects/modaria/default.asp?s=8 and l=129). It was recognized that the decision-making needs will inform the scope of risk assessments, and the risk insights and structured decision analyses will aid in informed decision-making. Therefore, MODARIA II WG1 is focused on developing methods and toolsets for risk-informed decision-making for NORM and nuclear legacy sites, including demonstration of decision-making processes and tools through case studies. MODARIA II WG1 has 91 registered participants from 33 Member States and IAEA (as of November 2017), some 30 of whom are actively engaged in various collaborative research and development activities within WG1. Members of WG1 participated in the First Technical Meeting of MODARIA II, which was held in Vienna, Austria from 31 October to 4 November 2016. The group then held its First Interim Meeting in Brussels, Belgium from 26 to 30 June 2017, which included a field trip to the legacy Tessenderlo Chemie (TCH) Phosphate Processing Site. At this meeting, the TCH Site and the Pridneprovsky Chemical Plant (PChP) in Ukraine were selected for case studies. The Los Alamos National Laboratory (LANL) Material Disposal Area B in the USA and the Beaverlodge Uranium Mill and Mill Site in northern Canada were selected as examples for sharing of good practices and lessons learned in risk-informed decision-making for environmental remediation and land conveyance. At the Second Technical Meeting held in Vienna on 30 October to 3 November 2017, an additional NORM site for tin processing in Brazil was added to the case studies, with another NORM site in Yunnan, China included for consideration at the Second Interim Meeting of WG1. The Second Interim Meeting will be held in in early to mid-May, 2018. The group has also decided to prepare an Interim Report by October 2018 to document the WG1 discussions and analyses for the period of 2016-2018, which will be finalized at the conclusion of MODARIA II in October 2019. Initial assignments have been discussed for IM1 participants to collect data, conduct modelling and analyses, and prepare draft sections for the Interim Report. This paper will provide an overview of the work plans for WG1. It will also highlight some near-term activities that the group is currently working on. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Regulatory Treatment of Non-Core Sources of Radioactivity for Advanced Reactor Designs

The recent resurgence in advance (non-light water) reactor development has been paralleled by the development of risk-informed performance-based (RIPB) licensing pathways. Specifically, the creation of the RIPB Licensing Modernization Project (LMP) approach and subsequent endorsement by the U.S. Nuclear Regulatory Commission (NRC) now provides advanced reactor vendors with a defined RIPB method to develop an affirmative safety case for licensing. In addition, the Technology Inclusive Content of Applications Project (TICAP) has published guidance on developing a license application based on the LMP approach. To support the utilization of risk information as part of advanced reactor design and licensing efforts, the American Society of Mechanical Engineers (ASME)/American Nuclear Society (ANS) Joint Committee on Nuclear Risk Management (JCNRM) has developed a probabilistic risk assessment (PRA) standard for advanced reactors. The standard, which was formerly approved by the American National Standards Institute (ANSI) in 2021 and recently endorsed by the NRC in trial use Regulatory Guide (RG) 1.247, is an integral standard, covering from initiating events to offsite consequence. A major feature of the standard is that it permits the inclusion of any source of radioactivity material at the site within the plant PRA. Therefore, non-core sources of radioactivity, such as fuel storage, fuel processing, and purification systems, can be included within a single comprehensive plant PRA. For those advanced reactor vendors utilizing a RIPB licensing approach, there is an opportunity to include the non-core sources of radioactivity within the RIPB framework for licensing decision-making, such as the categorization of events, classification of structures, systems, and components (SSCs), and evaluation of the adequacy of defense-in-depth (DID). For advanced reactor designs that contain multiple non-core sources of radioactivity, or for monolithic plant sites that include associated fuel facilities, this approach could potentially simplify licensing applications through the use of a single, uniform, and consistent decision-making framework across all radioactive sources at the site. In addition, a RIPB approach could provide additional insights regarding plant behavior, flexibility regarding licensing decision-making, and potentially allow the use of risk information as part of the plant oversight process. Risk-informing these aspects of advanced reactor licensing would also be consistent with the NRC’s risk policy statement. However, there is diverse regulation and guidance regarding the licensing of non-core sources of radioactivity and generally limited experience using RIPB approaches for the evaluation as part of licensing.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

NUREG/CR-7239, “Review of Fissile Material Exemptions and General Licenses in 10 CFR Part 71,” and Proposed Revisions to Harmonize with IAEA SSR-6 Fissile Material Requirements

Title 10 of the United States (US) Code of Federal Regulations (CFR), Part 71, Packaging and Transportation of Radioactive Material, includes requirements for the transport of fissile material in packages. These regulations provide requirements for packaging that is certified by the US Nuclear Regulatory Commission (NRC) to transport fissile material. The regulations also include provisions that allow for shipment in packages that are not required to be certified by the NRC. These provisions include criteria for exemptions from classification as fissile material (§71.15) and permit general licenses for limited quantities of fissile material and plutonium-beryllium special form sources (§71.22 and §71.23, respectively). This paper will discuss recommendations that NRC has made on the use of the fissile material exemptions and general license provisions in a recently published NUREG/CR, and changes to these provisions proposed for an upcoming rulemaking action.NUREG/CR-7239, “Review of Fissile Material Exemptions and General Licenses in 10 CFR Part 71,” was recently developed by Oak Ridge National Laboratory (ORNL) for the NRC. This document provides technical recommendations to fissile material licensees on how to apply the fissile material exemption and general license regulations. This paper will outline this NUREG/CR, including: 1) the technical basis, intent, and anticipated usage of each of the fissile material exemption and general license provisions; 2) the recent regulatory history of the Part 71 fissile material exemptions and general licenses; and 3) example problems which illustrate how the provisions might be applied and justified.In 2012, IAEA made several significant changes to the fissile material requirements in SSR-6, including the fissile exception provisions and provisions similar to the U.S. fissile material general licenses. In 2016, the NRC began a rulemaking effort to consider these changes (among others), and to decide how to best harmonize the domestic U.S. regulations. This paper will review the 2012 changes made to SSR-6, discuss the NRC staff consideration of those changes, and detail the proposed revisions to 10 CFR Part 71 that NRC is considering for the fissile material exemptions and general licenses.

Barto, Andrew↗

Viscous Particle Breakup within a Cooling Nuclear Fireball

Following the surface detonation of a nuclear weapon, the Earth’s crust and immediate surroundings are drawn into the fireball and form melts. Fallout is formed as these melts incorporate radioactive material from the bomb vapor and cool rapidly. The resultant fallout plume and dispersion of radioactive contamination is a function of several factors including weather patterns and fallout particle shapes and size distributions. Accurate modeling of the size distributions of fallout forms an important data point for dispersion codes that calculate the aerial distribution of fallout. While morphological evidence for aggregation of molten droplets is well documented in fallout glass populations, the breakup of these molten droplets has not been similarly studied. This study documents evidence that quenched fallout populations preserve evidence of molten breakup mechanisms.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗

Development of Mini-Compact Tension Test Method for Determining Fracture Toughness Master Curves for Reactor Pressure Vessel Steels

Small specimens are playing the key role in evaluating properties of irradiated materials. The use of small specimens provides several advantages. Typically, only a small volume of material can be irradiated in a reactor at desirable conditions in terms of temperature, neutron flux, and neutron dose. A small volume of irradiated material may also allow for easier handling of specimens. Smaller specimens reduce the amount of radioactive material, minimizing personnel exposures and waste disposal. However, use of small specimens imposes a variety of challenges as well. These challenges are associated with proper accounting for size effects and transferability of small specimen data to the real structures of interest. Any fracture toughness specimen that can be made out of the broken halves of standard Charpy specimens may have exceptional utility for evaluation of reactor pressure vessels (RPVs) since it would allow one to determine and monitor directly actual fracture toughness instead of requiring indirect predictions using correlations established with impact data. The Charpy V-notch specimen is the most commonly used specimen geometry in surveillance programs. Validation of the mini compact tension specimen (mini-CT) geometry has been performed on previously well characterized Midland beltline Linde 80 (WF-70) weld in the unirradiated condition. It was shown that the fracture toughness transition temperature, To, measured by these Mini-CT specimens is almost the same as To value that was derived from various larger fracture toughness specimens. Moreover, an International collaborative program has been established to extend the assessment and validation efforts to irradiated Linde 80 weld metal. The program is underway and involves the Oak Ridge National Laboratory (ORNL), Central Research Institute for Electrical Power Industry (CRIEPI), and Electric Power Research Institute (EPRI). The irradiated Mini-CT specimens from broken halves of previously tested Charpy specimens of Midland beltline weld have been machined and just arrived to ORNL as part of this international collaboration. The ORNL will initiate tests of the irradiated Linde 80 weld in FY2017 and results of this international program will be reported in FY2018.

42 ENGINEERING↗

The Assessment and Validation of Mini-Compact Tension Test Specimen Geometry and Progress in Establishing Technique for Fracture Toughness Master Curves for Reactor Pressure Vessel Steels

Small specimens are playing the key role in evaluating properties of irradiated materials. The use of small specimens provides several advantages. Typically, only a small volume of material can be irradiated in a reactor at desirable conditions in terms of temperature, neutron flux, and neutron dose. A small volume of irradiated material may also allow for easier handling of specimens. Smaller specimens reduce the amount of radioactive material, minimizing personnel exposures and waste disposal. However, use of small specimens imposes a variety of challenges as well. These challenges are associated with proper accounting for size effects and transferability of small specimen data to the real structures of interest. Any fracture toughness specimen that can be made out of the broken halves of standard Charpy specimens may have exceptional utility for evaluation of reactor pressure vessels (RPVs) since it would allow one to determine and monitor directly actual fracture toughness instead of requiring indirect predictions using correlations established with impact data. The Charpy V-notch specimen is the most commonly used specimen geometry in surveillance programs. Assessment and validation of mini-CT specimen geometry has been performed on previously well characterized HSST Plate 13B, an A533B class 1 steel. It was shown that the fracture toughness transition temperature measured by these Mini-CT specimens is within the range of To values that were derived from various large fracture toughness specimens. Moreover, the scatter of the fracture toughness values measured by Mini-CT specimens perfectly follows the Weibull distribution function providing additional proof for validation of this geometry for the Master Curve evaluation of rector pressure vessel steels. Moreover, the International collaborative program has been developed to extend the assessment and validation efforts to irradiated weld metal. The program is underway and involves ORNL, CRIEPI, and EPRI.

36 MATERIALS SCIENCE↗