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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 595 records · Page 33
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Oxygen Reduction Reaction Measurements on Platinum Electrocatalysts Utilizing Rotating Disk Electrode Technique: I. Impact of Impurities, Measurement Protocols and Applied Corrections

The rotating disk electrode (RDE) technique is being extensively used as a screening tool to estimate the activity of novel PEMFC electrocatalysts synthesized in lab-scale (mg) quantities. Discrepancies in measured activity attributable to glassware and electrolyte impurity levels, as well as conditioning, protocols and corrections are prevalent in the literature. Moreover, the electrochemical response to a broad spectrum of commercially sourced perchloric acid and the effect of acid molarity on impurity levels and solution resistance were also assessed. Our findings reveal that an area specific activity (SA) exceeding 2.0 mA/cm 2 (20 mV/s, 25°C, 100 kPa, 0.1 M HClO 4 ) for polished poly-Pt is an indicator of impurity levels that do not impede the accurate measurement of the ORR activity of Pt based catalysts. After exploring various conditioning protocols to approach maximum utilization of the electrochemical area (ECA) and peak ORR activity without introducing catalyst degradation, an investigation of measurement protocols for ECA and ORR activity was conducted. Down-selected protocols were based on the criteria of reproducibility, duration of experiments, impurity effects and magnitude of pseudo-capacitive background correction. In sum, statistical reproducibility of ORR activity for poly-Pt and Pt supported on high surface area carbon was demonstrated.

14 SOLAR ENERGY↗
DOE OSTI2013

Algorithm for Screening Phasor Measurement Unit Data for Power System Events and Categories and Common Characteristics for Events Seen in Phasor Measurement Unit Relative Phase-Angle Differences and Frequency Signals

A network of multiple phasor measurement units (PMU) was created, set up, and maintained at the University of Texas at Austin to obtain actual power system measurements for power system analysis. Power system analysis in this report covers a variety of time ranges, such as short- term analysis for power system disturbances and their effects on power system behavior and long- term power system behavior using modal analysis. The first objective of this report is to screen the PMU data for events. The second objective of the report is to identify and describe common characteristics extracted from power system events as measured by PMUs. The numerical characteristics for each category and how these characteristics are used to create selection rules for the algorithm are also described. Trends in PMU data related to different levels and fluctuations in wind power output are also examined.

17 WIND ENERGY↗
DOE OSTI2017

Modeled Martian subsurface elemental composition measurements with the Probing In situ with Neutron and Gamma ray instrument: Gamma and Neutron Measurements on Mars

Here, the Probing In situ with Neutrons and Gamma rays (PING) instrument is an innovative application of active neutron-induced gamma-ray technology. The objective of PING is to measure the elemental composition of the Martian regolith. As part 2 of a two-part submission, this manuscript presents PING's sensitivities as a function of the Martian regolith depth and PING's uncertainties in the measurements as a function of observation time in passive and active mode. Part 1 of our submission models the associated regolith types. The modeled sensitivities show that in PING's active mode, where both a Pulsed Neutron Generator (PNG) and a Gamma-Ray Spectrometer (GRS) are used, PING can interrogate the material below the rover to about 20 cm due to the penetrating nature of the high-energy neutrons and the resulting secondary gamma rays observed with the GRS. PING is capable of identifying most major and minor rock-forming elements, including H, O, Na, Mn, Mg, Al, Si, P, S, Cl, Cr, K, Ca, Ti, Fe and Th. The modeled uncertainties show that PING's use of a PNG reduces the required observation times by an order of magnitude over a passive operating mode where the PNG is turned off. While the active mode allows for more complete elemental inventories with higher sensitivity, the gamma-ray signatures of some elements are strong enough to detect in passive mode. We show that PING can detect changes in key marker elements and make thermal neutron measurements in about 1 minute that are sensitive to H and Cl.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2018

Rates of Ligand Exchange around the Bis-Oxalato Complex [NpO 2 (C 2 O 4 ) 2 ] 3- Measured by Using Multinuclear NMR Spectroscopy under Neutral to Semi-Alkaline Conditions [Rates of ligand exchange around the bis-oxalato complex NpO2(C2O4)23- measured using multinuclear NMR at neutral to semi-alkaline conditions]

The kinetics of ligand exchange between the free oxalate ion, C 2 O 4 2- , and the bis-oxalato Np V complex, [NpO 2 (C 2 O 4 ) 2 ] 3- , in aqueous solution are reported by using 13 C and 17 O NMR spectroscopy methods. Rates of exchange were measured in the pH regime of 6.5–9.0, at which speciation is shown to be suitably simple. Because the neptunium(V) complex is paramagnetic, the rates of ligand exchange were estimated by following the width of the 13 C and 17 O signals assigned to the free oxalate ion in solution and by applying the Swift–Connick method for measuring rates of exchange. A set of experiments were conducted in which pH and total oxalate concentration were varied, and the linear dependence of the rate on these parameters was demonstrated. Variable-temperature NMR spectroscopy was also performed to measure activation parameters of complexation. Finally, at pH<8.0, ΔH ≠ =16.9 ±4.9 kJ mol -1 and ΔS≠=-116.3 ±17.1kJ mol -1 K -1 , whereas at pH>8.0 there is almost no dependence on temperature, which is interpreted to indicate that hydrolysis is coupled to ligand exchange under these conditions.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2017

Measurements of ψ(2S) and X(3872) → J/ψπ + π - production in pp collisions at $\sqrt{s} = 8$ TeV with the ATLAS detector

Differential cross sections are presented for the prompt and non-prompt production of the hidden-charm states X(3872) and ψ(2S), in the decay mode J/ψπ + π – , measured using 11.4 fb –1 of pp collisions at √s = 8 TeV by the ATLAS detector at the LHC. The ratio of cross-sections X(3872)/ψ(2S) is also given, separately for prompt and non-prompt components, as well as the non-prompt fractions of X(3872) and ψ(2S). Assuming independent single effective lifetimes for non-prompt X(3872) and ψ(2S) production gives R B = B(B→X(3872)+any)B(X(3872)→J/ψπ+π–)/B(B→ψ(2S)+any)B(ψ(2S)→J/ψπ+π–)=(3.95±0.32(stat)±0.08(sys))×10 –2 separating short- and long-lived contributions, assuming that the short-lived component is due to B c decays, gives R B = (3.57 ± 0.33(stat) ± 0.11(sys)) × 10 –2 , with the fraction of non-prompt X(3872) produced via B c decays for p T (X(3872)) > 10 GeV being (25 ± 13(stat) ± 2(sys) ± 5(spin))%. The distributions of the dipion invariant mass in the X(3872) and ψ(2S) decays are also measured and compared to theoretical predictions.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2015

Measurement of the inclusive jet cross-section in proton-proton collisions at $ \sqrt{s}=7 $ TeV using 4.5 fb -1 of data with the ATLAS detector

The inclusive jet cross-section is measured in proton-proton collisions at a centre-of-mass energy of 7 TeV using a data set corresponding to an integrated luminosity of 4.5 fb -1 collected with the ATLAS detector at the Large Hadron Collider in 2011. Jets are identified using the anti-k t algorithm with radius parameter values of 0.4 and 0.6. The double-differential cross-sections are presented as a function of the jet transverse momentum and the jet rapidity, covering jet transverse momenta from 100 GeV to 2 TeV. Next-to-leading-order QCD calculations corrected for non-perturbative effects and electroweak effects, as well as Monte Carlo simulations with next-to-leading-order matrix elements interfaced to parton showering, are compared to the measured cross-sections. A quantitative comparison of the measured cross-sections to the QCD calculations using several sets of parton distribution functions is performed.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2014

Measurement of dijet cross-sections in pp collisions at 7 TeV centre-of-mass energy using the ATLAS detector

Double-differential dijet cross-sections measured in pp collisions at the LHC with a 7 TeV centre-of-mass energy are presented as functions of dijet mass and half the rapidity separation of the two highest-p T jets. These measurements are obtained using data corresponding to an integrated luminosity of 4.5 fb -1 , recorded by the ATLAS detector in 2011. The data are corrected for detector effects so that cross-sections are presented at the particle level. Cross-sections are measured up to 5TeV dijet mass using jets reconstructed with the anti- k t algorithm for values of the jet radius parameter of 0.4 and 0.6. The cross-sections are compared with next-to-leading-order perturbative QCD calculations by NLOJet++ corrected to account for non-perturbative effects. Comparisons with POWHEG predictions, using a next-to-leading-order matrix element calculation interfaced to a partonshower Monte Carlo simulation, are also shown. Electroweak effects are accounted for in both cases. The quantitative comparison of data and theoretical predictions obtained using various parameterizations of the parton distribution functions is performed using a frequentist method. In general, good agreement with data is observed for the NLOJet++ theoretical predictions when using the CT10, NNPDF2.1 and MSTW 2008 PDF sets. Disagreement is observed when using the ABM11 and HERAPDF1.5 PDF sets for some ranges of dijet mass and half the rapidity separation. An example setting a lower limit on the compositeness scale for a model of contact interactions is presented, showing that the unfolded results can be used to constrain contributions to dijet production beyond that predicted by the Standard Model.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2015

Measurement of the charge asymmetry in dileptonic decays of top quark pairs in pp collisions at $ \sqrt{s}=7 $ TeV using the ATLAS detector

A measurement of the top-antitop (t$\bar{t}$) charge asymmetry is presented using data corresponding to an integrated luminosity of 4.6 fb -1 of LHC pp collisions at a centreof-mass energy of 7 TeV collected by the ATLAS detector. Events with two charged leptons, at least two jets and large missing transverse momentum are selected. Two observables are studied: A C ℓℓ based on the identified charged leptons, and A$t\bar{t}\atop{C}$, based on the reconstructed tt final state. The asymmetries are measured to be A $ℓℓ\atop{C}$ =0.024 ± 0.015 (stat.) ± 0.009 (syst.), A $t\bar{t}\atop{C}$ = 0.021 ± 0.025 (stat.) ± 0.017 (syst.). The measured values are in agreement with the Standard Model predictions.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2019

Measurement of VH, H → $b\bar{b}$ production as a function of the vector-boson transverse momentum in 13 TeV pp collisions with the ATLAS detector

Cross-sections of associated production of a Higgs boson decaying into bottomquark pairs and an electroweak gauge boson, W or Z , decaying into leptons are measured as a function of the gauge boson transverse momentum. The measurements are performed in kinematic fiducial volumes defined in the ‘simplified template cross-section’ framework. The results are found using 79.8 fb ₋1 of proton-proton collisions recorded by the ATLAS detector at the Large Hadron Collider at a centre-of-mass energy of 13 TeV. All measurements are found to be in agreement with the Standard Model predictions, and limits are set on the parameters of an effective Lagrangian sensitive to modifications of the Higgs boson couplings to the electroweak gauge bosons.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2016

Measurement of the angular coefficients in Z-boson events using electron and muon pairs from data taken at $ \sqrt{s}=8 $ TeV with the ATLAS detector

The angular distributions of Drell-Yan charged lepton pairs in the vicinity of the Z-boson mass peak probe the underlying QCD dynamics of Z-boson production. This paper presents a measurement of the complete set of angular coefficients A 0–7 describing these distributions in the Z-boson Collins-Soper frame. The data analysed correspond to 20.3 fb –1 of pp collisions at √s = 8 TeV, collected by the ATLAS detector at the CERN LHC. The measurements are compared to the most precise fixed-order calculations currently available (O(α2s)) and with theoretical predictions embedded in Monte Carlo generators. The measurements are precise enough to probe QCD corrections beyond the formal accuracy of these calculations and to provide discrimination between different parton-shower models. A significant deviation from the (O(α 2 s )) predictions is observed for A 0 – A 2 . In conclusion, evidence is found for non-zero A 5,6,7 , consistent with expectations.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2017

Measurement of the inclusive jet cross-sections in proton-proton collisions at $\sqrt{s}=8$ TeV with the ATLAS detector

Inclusive jet production cross-sections are measured in proton-proton collisions at a centre-of-mass energy of √s=8 TeV recorded by the ATLAS experiment at the Large Hadron Collider at CERN. The total integrated luminosity of the analysed data set amounts to 20.2 fb -1 . Double-differential cross-sections are measured for jets defined by the anti-k t jet clustering algorithm with radius parameters of R = 0.4 and R = 0.6 and are presented as a function of the jet transverse momentum, in the range between 70 GeV and 2.5 TeV and in six bins of the absolute jet rapidity, between 0 and 3.0. The measured cross-sections are compared to predictions of quantum chromodynamics, calculated at next-to-leading order in perturbation theory, and corrected for non-perturbative and electroweak effects. The level of agreement with predictions, using a selection of different parton distribution functions for the proton, is quantified. Tensions between the data and the theory predictions are observed.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2021

Quantitative concentration measurements in a turbulent helium jet using rainbow schlieren deflectometry

Rainbow schlieren deflectometry (RSD) is applied to acquire quantitative concentration measurements in a turbulent environment for the first time. RSD methodology is developed and validated using Rayleigh scattering data available in the literature. Experiments were performed in an initially laminar, momentum-driven helium jet injected into ambient air. Full-field measurements are acquired that span the laminar, transition, and fully turbulent regions of the jet. Furthermore, the RSD results are shown to provide accurate measurements in each region and also confirm the self-similar nature of the fully turbulent jet. Analysis shows that the transition from laminar to turbulent flow occurs across an axial span that decreases with increasing Reynolds number. Experiments with a long exposure time were conducted to evaluate the limitations of hardware averaging of the RSD signal in comparison with software averaging.

02 PETROLEUM↗
DOE OSTI2022

Speed of Sound Measurements of Binary Mixtures of Difluoromethane (R-32) with 2,3,3,3-Tetrafluoropropene (R-1234yf) or trans-1,3,3,3-Tetrafluoropropene (R-1234ze(E)) Refrigerants

In this article, sound speed data measured using a dual-path pulse-echo instrument are reported for binary mixtures of difluoromethane (R-32) with 2,3,3,3-tetrafluoropropene (R-1234yf) or trans-1,3,3,3-tetrafluoropropene (R-1234ze(E)). The sound speed is reported at two compositions for each binary mixture of approximately (0.33/67) and (0.67/0.33) mole fraction at temperatures between 230 K and 345 K. Data are reported from pressures slightly above the bubble point to 12 MPa for R-32/1234yf mixtures to avoid potential polymerization reactions and to 53 MPa for the R-32/1234ze(E) mixtures. The mean uncertainty of the sound speed data are less than 0.1% of the measured value where uncertainties at individual state points range from 0.04% to 0.5% of the measured value as the conditions approach the mixture critical region. The reported data are compared to available Helmholtz-energy-explicit EOS included in REFPROP and all systems studied have average absolute deviations greater than 2%. The comparisons show that further adjustments to the mixture models are needed to provide a reasonable representation of the data within its experimental uncertainty.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗