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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 595 records · Page 33

Space Shuttle Columbia Aging Wiring Failure Analysis

A Space Shuttle Columbia main engine controller 14 AWG wire short circuited during the launch of STS-93. Post-flight examination divulged that the wire had electrically arced against the head of a nearby bolt. More extensive inspection revealed additional damage to the subject wire, and to other wires as well from the mid-body of Columbia. The shorted wire was to have been constructed from nickel-plated copper conductors surrounded by the polyimide insulation Kapton, top-coated with an aromatic polyimide resin. The wires were analyzed via scanning electron microscope (SEM), energy dispersive X-Ray spectroscopy (EDX), and electron spectroscopy for chemical analysis (ESCA); differential scanning calorimetry (DSC) and thermal gravimetric analysis (TGA) were performed on the polyimide. Exemplar testing under laboratory conditions was performed to replicate the mechanical damage characteristics evident on the failed wires. The exemplar testing included a step test, where, as the name implies, a person stepped on a simulated wire bundle that rested upon a bolt head. Likewise, a shear test that forced a bolt head and a torque tip against a wire was performed to attempt to damage the insulation and conductor. Additionally, a vibration test was performed to determine if a wire bundle would abrade when vibrated against the head of a bolt. Also, an abrasion test was undertaken to determine if the polyimide of the wire could be damaged by rubbing against convolex helical tubing. Finally, an impact test was performed to ascertain if the use of the tubing would protect the wire from the strike of a foreign object.

McDaniels, Steven J.↗

Development of energy-absorbing reaction-sintered Si3N4 surface layers on hot-pressed Si3N4

Energy-absorbing Si3N4 surface layers on dense Si3N4 substrates were formed by in-place nitridation of fine-grained silicon powder. Ballistic impact tests performed on samples with 1-mm thick layers at room temperature and 1370 C showed up to an eightfold increase in the energy necessary to fracture the substrate. For maximum impact resistance, a small amount (about 20 vol %) of residual Si must be present in the reaction-sintered Si3N4 surface layer. Thermal cycling to 1370 C did not affect impact resistance, even though a considerable amount of SiO2 formed within the reaction-sintered Si3N4 layer during cycling. Erosion testing of samples in a Mach 0.8 burner rig at 1370 C resulted in minimal surface recession of the surface layer. Chemically vapor-deposited SiC-coated material similarly tested exhibited no surface recession.

Brennan, J. J.↗

Impact Modeling and Testing of Pouch and Prismatic Cells

Understanding battery response under impact is critical to improve the safety of electrified vehicles. Nevertheless, predicting the impact behaviors of batteries is not straightforward since a battery cell usually contains hundreds of thin layers with dramatically different material properties and multiple physical processes occur simultaneously during cell deformation. Here we utilized both empirical tests and numerical models to capture the failure process of pouch and prismatic cells in various impact scenarios. In each test, a cell was hit once by an indenter dropped from a certain height. During which the cell penetration, loading force, voltage and temperature were monitored to characterize the cell’s response. Meanwhile, numerical models were developed to capture the coupled mechanical, electrical, electrochemical and thermal responses of batteries. In these models, the cell bulk was treated as a homogeneous part to achieve computational efficiency required by large-scale simulations, and it was represented by the geologic cap model that allows both shear and compaction deformation. Simulation results showed agreement with experimental data in essential features of cell behaviors during impact. Details of the test setup, model development and cell failure behaviors are presented in this paper. Additionally, capabilities, limitations and future improvement of the battery safety modeling are discussed.

25 ENERGY STORAGE↗

Grain refinement of high strength steels to improve cryogenic toughness

Grain-refining techniques using multistep heat treatments to reduce the grain size of five commercial high-strength steels were investigated. The goal of this investigation was to improve the low-temperature toughness as measured by Charpy V-notch impact test without a significant loss in tensile strength. The grain size of four of five alloys investigated was successfully reduced up to 1/10 of original size or smaller with increases in Charpy impact energy of 50 to 180 percent at -320 F. Tensile properties were reduced from 0 to 25 percent for the various alloys tested. An unexpected but highly beneficial side effect from grain refining was improved machinability.

Rush, H. F.↗

A novel drop weight impact setup for testing reinforced concrete beams

A novel method of testing reinforced concrete beams under impact using a drop tower is described. The method consists of configuring the support conditions and instrumenting both the loading end of the hammer and support points in such a way that a proper dynamic analysis of the impact event can be performed and rational data can be derived.

42 ENGINEERING↗

Polyimide aerogels for ballistic impact protection

The ballistic performance of edge-clamped monolithic polyimide aerogel blocks (12 mm thickness) has been studied through a series of impact tests using a helium-filled gas gun connected to a vacuum chamber and a spherical steel projectile (approximately 3 mm diameter) with an impact velocity range of 150–1300 m s -1 . The aerogels had an average bulk density of 0.17 g cm -3 with high porosity of approximately 88%. The ballistic limit velocity of the aerogels was estimated to be in the range of 175–179 m s -1 . Moreover, the aerogels showed a robust ballistic energy absorption performance (e.g., at the impact velocity of 1283 m s -1 at least 18% of the impact energy was absorbed). At low impact velocities, the aerogels failed by ductile hole enlargement followed by a tensile failure. By contrast, at high impact velocities, the aerogels failed through an adiabatic shearing process. Given the substantially robust ballistic performance, the polyimide aerogels have a potential to combat multiple constraints such as cost, weight, and volume restrictions in aeronautical and aerospace applications with high blast resistance and ballistic performance requirements such as in stuffed Whipple shields for orbital debris containment application.

42 ENGINEERING↗

Development and modeling for a small-scale, rapidly heated high explosives initiation time (HEIT) experiment

Most small-scale assessments of explosive sensitivity, including the popular drop-weight impact test, convolute thermal and mechanical phenomena to the extent that it has been extremely challenging to decipher how an explosive ignites and propagates reactions. For instance, an impact generates heat through a range of dissipation mechanisms, which can in turn, depending on the reaction rates of the explosive, lead to chemical decomposition. To deconvolute the various contributions to the sub-shock initiation and propagation of explosive reactions, we describe the development and modeling of the High Explosives Initiation Time (HEIT) test - a new, small-scale, high-throughput experiment designed to rapidly heat milligram quantities of energetic materials confined within small diameter steel needles. Specifically, we have modeled and designed a 250 joule pulsed power system capable of rapidly delivering electrical current to the needles, resulting in rapid heat delivery to the sample. In conclusion, the energy deposition rate into the sample is controlled by different transmission line topologies. Modeling in COMSOL is performed to understand the energy required to heat up the explosive sample.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Impact damage resistance of carbon/epoxy composite tubes for the DC-XA liquid hydrogen feedline

Low-velocity impacts were inflicted upon two elbow sections of carbon/epoxy feedline that are to be a part of the Delta Clipper-XA flight vehicle. A soap-based liquid leak detector solution was used to inspect the impact sites for leaks of pressurized gas that was pumped into the tube. Visual surface damage was noted and recorded for each impact site. After impact testing of each of the two sections of tubes was completed, the damage zones were disected from the tube and cross sectioned through the impact site. These specimens were polished after potting them in epoxy and were examined for microcracking using a fluorescent dye penetrant technique. The results showed that nonvisible damage could cause microcracking, thereby resulting in leaks through the tube wall.

Nettles, A. T.↗

Characterization of Low-Velocity Impact Damage in Toughened Non-Crimp Fabric Laminates

The damage response of resin-infused composites was investigated using quasi-static indentation (QSI) and instrumented drop-weight impact testing. The test specimens were composed of six layers of non-crimp fabrics where each layer contained +45°, 90°, −45°, and 0° plies. The goals of the testing were to identify damage responses that may differ from traditional thermoset materials and provide damage characterization data to evaluate current damage prediction analyses and aid improvements to current damage models. The damage was characterized using X-ray computed tomography (CT) and ultrasonic testing (UT). Incremental QSI loading was used on a single specimen to investigate damage growth in nine steps at progressively higher loads. Realtime acoustic emission data were used to determine the unloading points. Unlike typical thermoset composites, the force-displacement was smooth and showed no obvious indications of damage. The primary damage consisted of large lines of fiber fracture on the plies near the impact surface and delaminations through the thickness. Nine specimens were impacted at nominal impact energies of 25 ft-lbs, 30 ft-lbs, and 35 ft-lbs. The force histories at each energy followed nearly identical paths. Again, no obvious signs of damage were observed in any of the force histories. The general damage response in the dynamic tests was similar to the QSI-loaded specimens. However, repeat specimens impacted with a given impact energy showed variations in the damage. Some characteristics of the damage response were different than those typically observed in thermoset composites and will need to be evaluated using current analysis methods.

Composite Materials↗

Characterization of Low-Velocity Impact Damage in Toughened Non-Crimp Fabric Laminates

The damage response of resin-infused composites was investigated using quasi-static indentation (QSI) and instrumented drop-weight impact testing. The test specimens were composed of six layers of non-crimp fabrics where each layer contained +45°, 90°, −45°, and 0° plies. The goals of the testing were to identify damage responses that may differ from traditional thermoset materials and provide damage characterization data to evaluate current damage prediction analyses and aid improvements to current damage models. The damage was characterized using X-ray computed tomography (CT) and ultrasonic testing (UT). Incremental QSI loading was used on a single specimen to investigate damage growth in nine steps at progressively higher loads. Realtime acoustic emission data were used to determine the unloading points. Unlike typical thermoset composites, the force-displacement was smooth and showed no obvious indications of damage. The primary damage consisted of large lines of fiber fracture on the plies near the impact surface and delaminations through the thickness. Nine specimens were impacted at nominal impact energies of 25 ft-lbs, 30 ft-lbs, and 35 ft-lbs. The force histories at each energy followed nearly identical paths. Again, no obvious signs of damage were observed in any of the force histories. The general damage response in the dynamic tests was similar to the QSI-loaded specimens. However, repeat specimens impacted with a given impact energy showed variations in the damage. Some characteristics of the damage response were different than those typically observed in thermoset composites and will need to be evaluated using current analysis methods.

Composite Materials↗

Characteristics of Whipple Shield Performance in the Shatter Regime

Between the onset of projectile fragmentation and the assumption of rear wall failure due to an impulsive load, multi-wall ballistic limit equations are linearly interpolated to provide reasonable yet conservative predictions of perforation thresholds with conveniently simple mathematics. Although low velocity and hypervelocity regime predictions are based on analytical expressions, there is no such scientific foundation for predictions in the intermediate (or shatter) regime. As the debris flux in low earth orbit (LEO) becomes increasingly dominated by manmade pollution, the profile of micrometeoroid and orbital debris (MMOD) risk shifts continually towards lower velocities. For the International Space Station (ISS), encounter velocities below 7 km/s now constitute approximately 50% of the penetration risk. Considering that the transition velocity from shatter to hypervelocity impact regimes described by common ballistic limit equations (e.g. new non-optimum Whipple shield equation [1]) occurs at 7 km/s, 50% of station risk is now calculated based on failure limit equations with little analytical foundation. To investigate projectile and shield behavior for impact conditions leading to projectile fragmentation and melt, a series of hypervelocity impact tests have been performed on aluminum Whipple shields. In the experiments projectile diameter, bumper thickness, and shield spacing were kept constant, while rear wall thickness was adjusted to determine spallation and perforation limits at various impact velocities and angles. The results, shown in Figure 1 for normal and 45 impacts, demonstrated behavior that was not sufficiently described by the simplified linear interpolation of the NNO equation (also shown in Figure 1). Hopkins et al. [2] investigated the performance of a nominally-identical aluminum Whipple shield, identifying the effects of phase change in the shatter regime. The results (conceptually represented in Figure 2) were found to agree well with those obtained in this study at normal incidence, suggesting that shielding performance in the shatter regime could be well described by considering more complex phase conditions than currently implemented in most BLEs. Furthermore, evidence of these phase effects were found in the oblique test results, providing the basis for an empirical description of these effects that can be applied in MMOD risk assessment software. In this paper, results of the impact experiments are presented, and characteristics of target damage are evaluated. A comparison of intermediate velocity impact failure mechanisms in current BLEs are discussed and compared to the findings of the experimental study. Risk assessment calculations have been made on a simplified structure using currently implemented penetration equations and predicted limits from the experimental program, and the variation in perceived mission risk is discussed. It was found that ballistic limit curves that explicitly incorporated phase change effects within the intermediate regime lead to a decrease in predicted MMOD risk for ISS-representative orbits. When considered for all Whipple-based shielding configurations onboard the ISS, intermediate phase change effects could lead to significant variations in predicted mission risk.

Ryan, Shannon↗

Impact damage in small diameter graphite/epoxy composite struts

An investigation was performed to study impact induced damage in small-diameter struts made of a composite material with a brittle matrix system. The major focus is on characterizing the impact behavior associated with the barely visible damage. An experimental procedure including ultrasonic inspection, instrumented impact testing, and delamination buckling and residual strength measurements is presented. From the ultrasonic inspection, it is found that for the strut specimens under investigation, the impact energy level for barely visible damage threshold is above that of the internal damage threshold. A 60- to 65-percent reduction in compressive strength was typical for struts subjected to the barely visible impact damage threshold.

Chen, G.-S.↗

Correlation of Microstructure and Mechanical Properties of Metal Big Area Additive Manufacturing

Metal Big Area Additive Manufacturing (MBAAM) is a novel wire-arc additive manufacturing method that uses a correction-based approach developed at the Oak Ridge National Laboratory (ORNL). This approach is an integrated software method that minimizes the dynamic nature of welding and compensates for build height. The MBAAM process is used to fabricate simple geometry thin walled specimens, using a C-Mn steel weld wire, to investigate the scatter in mechanical properties and correlate them to the underlying microstructure. The uni-axial tensile tests show isotropic tensile and yield properties with respect to building directions, although some scatter in elongation is observed. Large scatter is observed in the Charpy Impact tests. The microstructure characterization reveals mostly homogenous ferrite grains with some pearlite, except for some changes in morphology and grain size at the interface between the build and the base plate. The measured properties and microstructure are compared with the toughness and strength values reported in the literature, and a hypothesis is developed to rationalize the differences. Overall, the MBAAM process creates stable, isotropic, and weld-like mechanical properties in the deposit, while achieving a precise geometry obtained through a real-time feedback sensing, closed loop control system.

36 MATERIALS SCIENCE↗

Properties of largest fragment produced by hypervelocity impact of aluminum spheres with thin aluminum sheets

Results are presented from hypervelocity impact tests in which 1.275 g spheres of 2017-T4 Al alloy were fired at normal incidence at eight thicknesses of 6061-T6 Al alloy sheets, with impact velocity of about 6.7 km/sec; additional data are presented for smaller and larger spheres than these, in the cases of other Al alloy impact bumpers. A large fragment of the projectile is observable at the center of the debris clouds generated upon impact. The velocity of these large fragments decreased continuously with increasing bumper thickness/projectile diameter ratio, from 99 percent to less than 80 percent of impact velocity; there is a linear increase in the size of the central projectile fragment with decreasing shock-induced stress in the projectile.

Piekutowski, Andrew J.↗

Observing system simulation experiments at NASA. Goddard Space Flight Center

A series of realistic simulation studies is being conducted as a cooperative effort between the European Centre for Medium Range Weather Forecasts (ECMWF), the National Meteorological Center (NMC), and the Goddard Laboratory for Atmospheres (GLA), to provide a quantitative assessment of the potential impact of future observing systems on large scale numerical weather prediction. A special objective is to avoid the unrealistic character of earlier simulation studies. Following a brief review of previous simulation studies and real data impact tests, the methodology for the current simulation system will be described. Results from an assessment of the realism of the simulation system and of the potential impact of advanced observing systems on numerical weather prediction and preliminary results utilizing this system will be presented at the conference.

Atlas, R.↗

The White Sands Test Facility

This is an overview of the White Sands Test Facility's role in ensuring the safety and reliability of materials and hardware slated for launch aboard the Space Shuttle. Engine firings, orbital flights debris impact tests, and propulsion tests are featured as well as illustrating how they provide flight safety testing for the Johnson Space Center, other NASA centers, and various government agencies. It also contains a historical perspective and highlights of major programs that have been participated in as part of NASA.

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