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At least 577 records · Page 32
All sourcesNASA NTRSDOE OSTI
DOE OSTI2023

Aculeaxanthones A–E, new xanthones from the marine-derived fungus Aspergillus aculeatinus WHUF0198

Introduction Dimeric natural products are widespread in plants and microorganisms, which usually have complex structures and exhibit greater bioactivities than their corresponding monomers. In this study, we report five new dimeric tetrahydroxanthones, aculeaxanthones A−E ( 4−8 ), along with the homodimeric tetrahydroxanthone secalonic acid D ( 1 ), chrysoxanthones B and C ( 2 and 3 ), and 4−4’-secalonic acid D ( 9 ), from different fermentation batches of the title fungus. Methods A part of the culture was added to a total of 60 flasks containing 300 ml each of number II fungus liquid medium and culture 4 weeks in a static state at 28˚C. The liquid phase (18 L) and mycelia was separated from the fungal culture by filtering. A crude extract was obtained from the mycelia by ultrasound using acetone. To obtain a dry extract (18 g), the liquid phase combined with the crude extract were further extracted by EtOAc and concentrated in vacuo. The MIC of anaerobic bacteria was examined by a broth microdilution assay. To obtain MICs for aerobic bacteria, the agar dilution streak method recommended in Clinical and Laboratory Standards Institute document (CLSI) M07-A10 was used. Compounds 1−9 was tested against the Bel-7402, A-549 and HCT-116 cell lines according to MTT assay. Results and Discussion The structures of these compounds were elucidated on the base of 1D and 2D NMR and HR-ESIMS data, and the absolute configurations of the new xanthones 4−8 were determined by conformational analysis and time-dependent density functional theory-electronic circular dichroism (TDDFT-ECD) calculations. Compounds 1–9 were tested for cytotoxicity against the Bel-7402, A549, and HCT-116 cancer cell lines. Of the dimeric tetrahydroxanthone derivatives, only compound 6 provided cytotoxicity effect against Bel-7402 cell line (IC50, 1.96 µM). Additionally, antimicrobial activity was evaluated for all dimeric tetrahydroxanthones, including four Gram-positive bacteria including Enterococcus faecium ATCC 19434, Bacillus subtilis 168, Staphylococcus aureus ATCC 25923 and MRSA USA300; four Gram-negative bacteria, including Helicobacter pylori 129, G27, as well as 26,695, and multi drug-resistant strain H. pylori 159, and one Mycobacterium M. smegmatis ATCC 607. However, only compound 1 performed activities against H. pylori G27, H. pylori 26695, H. pylori 129, H. pylori 159, S. aureus USA300, and B. subtilis 168 with MIC values of 4.0, 4.0, 2.0, 2.0, 2.0 and 1.0 μg/mL, respectively.

Wu, Jun↗
DOE OSTI2022

Conversion Kinetics and Ionic Conductivity in Na-β”-Alumina + YSZ (Naβ”AY) Sodium Solid Electrolyte via Vapor Phase Conversion Process

Sodium ion batteries have been receiving increasing attention and may see potential revival in the near future, particularly in large-scale grid energy storage coupling with wind and solar power generation, due to the abundant sodium resources, low cost, and sufficiently high energy density. Among the known sodium ion conductors, the Na-β”-alumina electrolyte remains highly attractive because of its high ionic conductivity. This study focuses on the vapor phase synthesis of a Na-β”-Alumina + YSZ (Naβ”AY) composite sodium electrolyte, which has higher mechanical strength and stability than conventional single phase β”-Alumina. The objectives are the measurement of conversion kinetics through a newly developed weight-gain based model and the determination of sodium ionic conductivity in the composite electrolyte. Starting samples contained ~70 vol% α-Alumina and ~30 vol% YSZ (3 mol% Y 2 O 3 stabilized Zirconia) with and without a thin alumina surface layer made by sintering in air at 1600 °C. The sintered samples were placed in a powder of Na-β”-alumina and heat-treated at 1250 °C for various periods. Sample dimensions and weight were measured as a function of heat treatment time. The conversion of α-Alumina in the α-Alumina + YSZ composite into Naβ”AY occurred by coupled diffusion of sodium ions through Na-β”-alumina and of oxygen ions through YSZ, effectively diffusing Na2O. From the analysis of the time dependence of sample mass and dimensions, the effective diffusion coefficient of Na 2 O through the sample, D eff , was estimated to be 1.74 x 10 -7 cm2 s -1 , and the effective interface transfer parameter, k eff , was estimated as 2.33 x 10 -6 cm s -1 . By depositing a thin alumina coating layer on top of the bulk composite, the chemical diffusion coefficient of oxygen through single phase Na-β”-alumina was estimated as 4.35 x 10 -10 cm 2 s -1 . An AC impedance measurement was performed on a fully converted Naβ”AY composite, and the conductivity of the composite electrolyte was 1.3 x 10 -1 S cm -1 at 300 °C and 1.6 x 10 -3 S cm -1 at 25 °C, indicating promising applications in solid state or molten salt batteries at low to intermediate temperatures.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Lorentz Symmetry Group, Retardation and Energy Transformations in a Relativistic Engine

In a previous paper, we have shown that Newton’s third law cannot strictly hold in a distributed system of which the different parts are at a finite distance from each other. This is due to the finite speed of signal propagation which cannot exceed the speed of light in vacuum, which in turn means that when summing the total force in the system the force does not add up to zero. This was demonstrated in a specific example of two current loops with time dependent currents, the above analysis led to suggestion of a relativistic engine. Since the system is effected by a total force for a finite period of time this means that the system acquires mechanical momentum and energy, the question then arises how can we accommodate the law of momentum and energy conservation. The subject of momentum conservation was discussed in a pervious paper, while preliminary results regarding energy conservation where discussed in some additional papers. Here we give a complete analysis of the exchange of energy between the mechanical part of the relativistic engine and the field part, the energy radiated from the relativistic engine is also discussed. We show that the relativistic engine effect on the energy is 4th-order in 1c and no lower order relativistic engine effect on the energy exists.

42 ENGINEERING↗
DOE OSTI2025

SIDM Concerto: Compilation and Data Release of Self-interacting Dark Matter Zoom-in Simulations

We present SIDM Concerto: 14 cosmological zoom-in simulations in cold dark matter (CDM) and self-interacting dark matter (SIDM) models based on the Symphony and Milky Way-est suites. SIDM Concerto includes one Large Magellanic Cloud– (LMC-) mass system (host mass ∼10 11 M ⊙ ), two Milky Way (MW) analogs (∼10 12 M ⊙ ), two group-mass hosts (∼10 13 M ⊙ ), and one low-mass cluster (∼10 14 M ⊙ ). Each host contains ≈2 × 10 7 particles and is run in CDM and one or more strong, velocity-dependent SIDM models. Our analysis of SIDM (sub)halo populations over seven subhalo mass decades reveals that (1) the fraction of core-collapsed isolated halos and subhalos peaks at a maximum circular velocity corresponding to the transition of the SIDM cross section from a v −4 to v 0 scaling; (2) SIDM subhalo mass functions are suppressed by ≈50% relative to CDM in LMC, MW, and group-mass hosts but are consistent with CDM in the low-mass cluster host; (3) subhalos’ inner density profile slopes, which are more diverse in SIDM than in CDM, are sensitive to both the amplitude and shape of the SIDM cross section. Our simulations provide a benchmark for testing SIDM predictions with astrophysical observations of field and satellite galaxies, strong lensing systems, and stellar streams. Data products are publicly available at doi:10.5281/zenodo.14933624.

dark matter↗
NASA NTRS1971

NASA multidisciplinary research grant

Research is discussed in the multidisciplinary areas of space and planetary science; materials and radiation; systems, instrumentation, and structures; and technology and man. Highlights are identified as an alpha-recoil track method of archeological dating; infrared astronomical telescope; reaction rates data, semiconductor radiation detectors, and analysis of time-dependent systems; Gunn effect devices for microwave generation and detection, mode-locked lasers, and radiation theory; and the application of a satellite communication system to educational development. Detectors to be flown on Apollo 16 to measure heavy particle flux in the solar wind and to be part of the HEAO-A experiment on extremely heavy nuclei in cosmic rays were developed. The impact of the multidisciplinary research on university activities is described, and individual departmental reports are included.

Source record↗
NASA NTRS1972

Positive ion chemistry of the D and E regions.

A comparison of ion-molecule reaction rates implied by E- and F-region chemistry and measured in the laboratory shows on the whole good agreement except that the ionospheric analysis demands stronger temperature dependences. In the daytime D region, it is claimed that the reconciliation of positive ion densities with production rates and laboratory rate constants would best be achieved if (1) ionization of O2(1 delta g) and hydration of O4(+) in competition with the reduction of O4(+) to O2(+) by O were the dominant source of hydrates between 85 and 77 km, (2) ionization of NO by solar Lyman alpha followed by hydration was the dominant source of hydrates below 77 km, and (3) for some reason, Lyman alpha did not ionize NO effectively at pressures below those prevailing at 75 km.

Donahue, T. M.↗
NASA NTRS1973

Determination of the temperature of gas mixtures by using laser Raman scattering

A theoretical model for the Raman rotational spectrum of air was formulated, yielding the spectral temperature dependence; and an error analysis of temperature measurement accuracies was performed. The theoretical spectra and the predicted temperature measurement error of + or - 20 K (7 percent) compared well with experimental data. These experimental data consisted of Raman spectra of air obtained for temperatures ranging from 243 to 313 K at a pressure of 1 atmosphere. The use of selected lines resulted in an experimental accuracy of + or - 13 K (-5 percent).

Coney, T. A.↗
NASA NTRS1973

Analysis of shape of porous cooled medium for an imposed surface heat flux and temperature

The surface of a porous cooled medium is to be maintained at a specified design temperature while being subjected to uniform heating by an external source. An analytical method is given for determining the shape of the medium surface that will satisfy these boundary conditions. The analysis accounts for temperature dependent variations of fluid density and viscosity and for temperature dependent matrix thermal conductivity. The energy equation is combined with Darcy's law in such a way that a potential can be defined that satisfies Laplace's equation. All of the heat-transfer and flow quantities are expressed in terms of this potential. The determination of the shape of the porous cooled region is thereby reduced to a free-boundary problem such as in inviscid free jet theory. Two illustrative examples are carried out: a porous leading edge with coolant supplied through a slot and a porous cooled duct with a rectangular outer boundary.

Siegel, R.↗
NASA NTRS1973

Study of resonance light scattering for remote optical probing

Enhanced scattering and fluorescence processes in the visible and UV were investigated which will enable improved remote measurements of gas properties. The theoretical relationship between scattering and fluorescence from an isolated molecule in the approach to resonance is examined through analysis of the time dependence of re-emitted light following excitation of pulsed incident light. Quantitative estimates are developed for the relative and absolute intensities of fluorescence and resonance scattering. New results are obtained for depolarization of scattering excited by light at wavelengths within a dissociative continuum. The experimental work was performed in two separate facilities. One of these utilizes argon and krypton lasers, single moded by a tilted etalon, and a 3/4 meter double monochromator. This facility was used to determine properties of the re-emission from NO2, I2 and O3 excited by visible light. The second facility involves a narrow-line dye laser, and a 3/4 meter single monochromator. The dye laser produces pulsed light with 5 nsec pulse duration and 0.005 nm spectral width.

Penney, C. M.↗
NASA NTRS1975

Coal refuse site inventories

Small-scale color-infrared aerial photography at 1:120,000 scale is used to carry out an operational survey of coal refuse sites. Site analyses and reclamation cost estimates are completed in less than 90 days by using remote sensing techniques. Analysis of photographs provided dependable and accurate data for the location and environmental assessment of nearly 200 coal refuse banks and slurry ponds. The inventory constitutes a comprehensive reference for establishing priorities for coal refuse site reclamation and for complementing future field surveys.

Wobber, F. J.↗
NASA NTRS1976

TAP 1: A Finite Element Program for Steady-State Thermal Analysis of Convectively Cooled Structures

The program has a finite element library of six elements: two conduction/convection elements to model heat transfer in a solid, two convection elements to model heat transfer in a fluid, and two integrated conduction/convection elements to represent combined heat transfer in tubular and plate/fin fluid passages. Nonlinear thermal analysis due to temperature dependent thermal parameters is performed using the Newton-Raphson iteration method. Program output includes nodal temperatures and element heat fluxes. Pressure drops in fluid passages may be computed as an option. A companion plotting program for displaying the finite element model and predicted temperature distributions is presented. User instructions and sample problems are presented in appendixes.

Thornton, E. A.↗
NASA NTRS1979

Reduction of particulate carryover from a pressurized fluidized bed

A bench scale fluidized bed combustor was constructed with a conical shape so that the enlarged upper part of the combustor would also serve as a granular bed filter. The combustor was fed coal and limestone. Ninety-nine tests of about four hours each were conducted over a range of conditions. Coal-to-air ratio varied from 0.033 to 0.098 (all lean). Limestone-to-coal ratio varied from 0.06 to 0.36. Bed depth varied from 3.66 to 8.07 feet. Temperature varied from 1447 to 1905 F. Pressure varied from 40 to 82 psia. Heat transfer area had the range zero to 2.72 ft squared. Two cone angles were used. The average particulate carry over of 2.5 grains/SCF was appreciably less than cylindrical fluidized bed combustors. The carry over was correlated by multiple regression analysis to yield the dependence on bed depth and hence the collection efficiency, which was 20%. A comparison with a model indicated that the exhaust port may be below the transport disengaging height for most of the tests, indicating that further reduction in carry over and increase in collection efficiency could be affected by increasing the freeboard and height of the exhaust port above the bed.

Patch, R. W.↗
NASA NTRS1979

Application of the superposition principle to solar-cell analysis

The superposition principle of differential-equation theory - which applies if and only if the relevant boundary-value problems are linear - is used to derive the widely used shifting approximation that the current-voltage characteristic of an illuminated solar cell is the dark current-voltage characteristic shifted by the short-circuit photocurrent. Analytical methods are presented to treat cases where shifting is not strictly valid. Well-defined conditions necessary for superposition to apply are established. For high injection in the base region, the method of analysis accurately yields the dependence of the open-circuit voltage on the short-circuit current (or the illumination level).

Lindholm, F. A.↗
NASA NTRS1979

Reduction of particulate carryover from a pressurized fluidized bed

A bench-scale pressurized fluidized bed combustor (PFBC) constructed with a conical shape to reduce the particulate carryover is examined. The combustor was fed coal and limestone with the coal to air ratio varying from 0.033 to 0.098 (all lean) and the coal to limestone ratio varying from 0.06 to 0.36. Two cone angles were used and it is shown that the average particulate carryover of 2.5 grains/SCF is appreciably less than cylindrical fluidized bed combustors. In addition the carryover was correlated by multiple regression analysis to yield the dependence on bed depth and hence the collection efficiency, which was 20%. Finally, a comparison with a model indicated that the exhaust port may be below the transport disengaging height for most of the tests showing that further improvements could be achieved by increasing the freeboard height of the exhaust port above the bed.

Patch, R. W.↗
NASA NTRS1980

Investigations of eddy coherence in jet flows

In turbulent shear flow the term coherent structures refers to eddies which are both spatially coherent, i.e., large eddies, aand also temporally coherent, i.e., they retain their identities for times which are long compared with their time scales in fixed point measurements. In transitional flows, the existence of such structures is evident from flow visualizations. In many other flows, such structures are not so evident. The reasons for the existence of these two classes of flows are discussed and attention is focused upon the more difficult flows, where coherent structures are not so evident. Techniques by which the existence (or nonexistence) of such structures in these flows can be established from point measurements, are also discussed. A major problem is shown to be the need to discriminate between real losses in eddy coherence and apparent losses in coherence introduced by phase scrambling effects which 'smear' multipoint correlations. The analysis of multiprobe time dependent data in cold and reacting round turbulent jets is described and it is shown how evidence of strong eddy coherence can be extracted from data.

Yule, A. J.↗
NASA NTRS1980

Energetic particle penetrations into the inner magnetosphere

The nose structures observed on 90-deg pitch angle ion spectrograms characteristic of energetic particle injection into the ring current region of the inner magnetosphere in the afternoon to midnight sector are examined in detail on the basis of Explorer 45 data. A statistical analysis of the time dependence of nose structures yields a highest probability of occurrence at around 2000 MLT, and most events are found to occur on successive passes. The appearance of nose events is also related to an enhancement or change in configuration of the geoelectric field which alters magnetospheric convection patterns to drive an ion front close to the earth, where it can be observed by Explorer 45. The observed characteristics of nose structures are interpreted in terms of adiabatic charged particle motions in the magnetosphere in a Volland-Stern convection electric field model, which is also applied to explain the energy spectra and dispersion in penetration distances of electrons and ions observed in the postmidnight to morning sectors.

Ejiri, M.↗
NASA NTRS1979

TF34 engine compression system computer study

The stability of the fan and the compressor components was examined individually using linearized and time dependent, one dimensional stability analysis techniques. The stability of the fan core integrated compression system was investigated using a two dimensional compression system model. The analytical equations on which this model was based satisfied the mass, axial momentum, radial momentum, and energy conservation equations for flow through a finite control volume. The results gave an accurate simulation of the flow through the compression system. The speed lines of the components were reproduced; the points of instability were accurately predicted; the locations where the instability was initiated in the fan and the core were indicated; and the variation of the bypass ratio during flow throttling was calculated. The validity of the analytical techniques was then established by comparing these results with test data and with results obtained from the steady state cycle deck.

Hosny, W. M.↗