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At least 577 records · Page 32

January 2022 Semiannual Saltstone Toxicity Characteristic Leaching Procedure (TCLP) Results

The aqueous waste from Tank 50 (salt solution) is sampled semiannually for transfers to the Saltstone Production Facility (SPF). Salt solution is treated at SPF and disposed of in the Saltstone Disposal Facility (SDF). Per request of customer, X-TTR-Z-00025, Revision 0, two SDF waste form (saltstone) samples were prepared in the Savannah River National Laboratory (SRNL) from the Tank 50 Waste Acceptance Criteria (WAC) sample and Z-Area premix material for the January 2022 semiannual Toxicity Characteristic Leaching Procedure (TCLP) samples. One sample contained a Full Premix which included 10:45:45 (by weight) of cement, slag and fly ash. The second sample contained 60:40 (by weight) of slag and fly ash only referred to as the “Cement-Free grout sample.” Results from this technical report support Task 2: ‘Grout Leaching Analyses’ of the Task Technical Request (TTR) prepared by Savannah River Mission Completion (SRMC). After at least 28 days cured, a sample of each of the SDF waste forms was collected and shipped to a certified laboratory for analysis using the Toxicity Characteristic Leaching Procedure (TCLP). The January 2022 semiannual saltstone (Full Premix) and the Cement-Free grout samples met the South Carolina (SC) Code of Regulations for Hazardous Waste Management Regulations (HWMR) 61-79.261.24 and 61-79-268.48 requirements for a non-hazardous waste form with respect to Resource Conservation and Recovery Act (RCRA) metals and Underlying Hazardous Constituents (UHCs), and also met the SPF WAC that was in effect at the time of the tank sampling.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

July 2022 Semiannual Saltstone Toxicity Characteristic Leaching Procedure (TCLP) Results

The aqueous waste from Tank 50 (salt solution) is sampled semiannually for transfers to the Saltstone Production Facility (SPF). Salt solution is treated at SPF and disposed of in the Salstone Disposal Facility (SDF). Per request of customer, X-TTR-Z-00025, Revision 0, two SDF waste form (salstone) samples were prepared in the Savannah River National Laboratory (SRNL) from the Tank 50 Waste Acceptance Criteria (WAC) sample and Z-Area premix material for the July 2022 Semiannual Toxicity Characteristic Leaching Procedure (TCLP) samples. One sample contained a Full Premix which included 10:45:45 (by weight) of cement, slag and fly ash. The second sample contained 60:40 (by weight) of slag and fly ash only referred to as the "Cement-Free grout sample." Results from this technical report support Task 2: 'Grout Leaching Analyses' of the Task Technical Request (TTR) prepared by Savannah River Mission Completion (SRMC). After at least 28 days cured, a sample of each of the SDF waste forms was collected and shipped to a certified laboratory for analysis using Toxicity Characteristic Leaching Procedure (TCLP). The July 2022 semiannual salstone (Full Premix) and the Cement-Free grout samples met the South Carolina (SC) Code of Regulations for Hazardous Waste Management Regulations (HWMR) 61-79.261.24 and 61-79-268.48 requirements for the non-hazardous waste form with respect to Resource Conservation and Recovery Act (RCRA) metals and Underlying Hazardous Constituents (UHCs), and also met the SPF WAC that was in effect at the time of the tank sampling.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Conduct of Engineering Project Engineer Qualification Standard

This document describes the training and qualification requirements for the Project Engineer (PE) position at the Los Alamos National Laboratory (LANL). Analysis indicates that the Project Engineer position is not required to meet the requirements of DOE Order 426.2, Personnel Selection, Training, Qualification, and Certification Requirements for DOE Nuclear Facilities for “Technical Staff” positions. However, Engineering Services Division (ESD) has decided to hold their Project Engineers to a higher professional standard by developing a qualification program for the PEs.

42 ENGINEERING↗

January 2023 Semiannual Saltstone Toxicity Characteristic Leaching Procedure (TCLP) Results

The aqueous waste from Tank 50 (salt solution) is sampled semiannually for transfers to the Saltstone Production Facility (SPF). Salt solution is treated at SPF and disposed of in the Saltstone Disposal Facility (SDF). Per request of customer, X-TTR-Z-00027, Revision 0, two SDF waste form (saltstone) samples were prepared in the Savannah River National Laboratory (SRNL) from the Tank 50 Waste Acceptance Criteria (WAC) sample and Z-area premix material for January 2023 semiannual Toxicity Characteristic Leaching Procedure (TCLP) samples. One sample contained a Full Premix which included 10:45:45 (by weight) of cement, slag, and fly ash. The second sample contained 60:40 (by weight) of slag and fly ash only referred to as the “Cement-Free grout sample.” Results from the technical report support Task 2: ‘Grout Leaching Analyses’ of the Task Technical Request (TTR) prepared by Savannah River Mission Completion (SRMC). After at least 28 days cured, a sample of each of the SDF waste forms was collected and shipped to a certified laboratory for analysis using the Toxicity Characteristic Leaching Procedure (TCLP). The January 2023 semiannual saltstone (Full Premix) and the Cement-Free grout samples met the South Carolina (SC) Code of Regulations for Hazardous Waste Management Regulations (HWMR) 61-79.261.24 and 61-79.268.48 requirements for a non-hazardous waste form with respect to the Resource Conservation and Recovery Act (RCRA) metals and Underlying Hazardous Constituents (UHCs), and also met the SPF WAC that was in effect at the time of the tank sampling.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Investigating Similarity Differences for Light-water-Moderated and Polyethylene-Moderated Systems

Oak Ridge National Laboratory has performed validation studies in support of Pacific Northwest National Laboratory’s analysis of the Sum-of-Fractions method. Work in a companion paper examines the validation methods and results for various mixtures of fissile isotopes in various concentrations moderated and reflected by water and polyethylene. Those results indicate a greater coverage of critical experiments for validating water moderated and reflected systems versus those moderated and reflected with polyethylene.

07 ISOTOPE AND RADIATION SOURCES↗

OGO-6 gas-surface energy transfer experiment

The kinetic energy flux of the upper atmosphere was analyzed using OGO-6 data. Energy transfer between 10 microwatts/sq cm and 0.1 W/sq cm was measured by short-term frequency changes of temperature-sensitive quartz crystals used in the energy transfer probe. The condition of the surfaces was continuously monitored by a quartz crystal microbalance to determine the effect surface contamination had on energy accommodation. Results are given on the computer analysis and laboratory tests performed to optimize the operation of the energy transfer probe. Data are also given on the bombardment of OGO-6 surfaces by high energy particles. The thermoelectrically-cooled quartz crystal microbalance is described in terms of its development and applications.

Mckeown, D.↗

Fabrication of neurophysiological monitoring systems

A system designed to collect electroencephalographic, electro-oculographic, electromyographic, and head motion data is described. The portable instrumentation provides a rapid and simple means by which neurophysiological data can be obtained by the patient in his home and the taped data returned to the laboratory for analysis. The system was designed primarily for the study of sleep.

Frost, J. D., Jr.↗

Shuttle LOX loading transient study. Task 2 milestone report. National space and technology laboratories (NSTL) LOX loading facility analysis

Transient thermodynamic analyses were made of the LOX loading system proposed for the space shuttle main propulsion test article (MPTA). This system is made up of a LOX replenish system and a main LOX line which include the barge tank, the lines, pumps, and valves between the barge and the orbiter (ORB) ground service equipment (GSE) interface, the MPTA fill system, the space shuttle main engine (SSME) chilldown bleed system, and the GSE vent system. System analyses include predictions of system performance sensitivity to operating sequence and LOX flowrate, temperature, and quality at the ORB/GSE interface. The transient thermodynamic conditions at the SSME feed line entrance, ET entrance (tank bottom), and the SSME bleed/GSE vent TEE are also included. The analyses are based on continuous SSME bleed flow during GSE facility chilldown.

Glasgow, V. L.↗

Soil-moisture ground truth, Hand County, South Dakota

Soil samples were taken in the field and carefully preserved in taped metal containers for later laboratory gravimetric analysis to determine soil-moisture content. The typical sampling pattern used in this mission is illustrated, and the soil types encountered on the soil-moisture lines are summarized. The actual soil-moisture data were tabulated by range, township and section. Soil-moisture data obtained in fields of winter wheat and spring wheat are briefly summarized.

Jones, E. B.↗

System measurements of a CO2 laser communications link

Measurements were made under simulated operating conditions to establish the capability of a CO2 laser transmitting heterodyne receiver link to acquire weak laser transmitter beams and maintain spatial tracking during communications. For the case of a synchronous satellite-to-earth station link, analysis and laboratory measurements indicate that the infrared heterodyne receiver subsystem is capable of performing the acquisition, acquisition confirm, and spatial tracking functions at IF signal-to-noise ratio of -17 dB. For the case of a low-altitude satellite-to-earth station link, the laser transmit signal is Doppler-shifted due to the difference in relative velocity of the two stations. The resultant Doppler frequency shift varies with time and must be spectrally acquired and tracked.

Peyton, B. J.↗

Development of CO2 laser Doppler instrumentation for detection of clear air turbulence, volume 1

Modification, construction, test and operation of an advanced airborne carbon dioxide laser Doppler system for detecting clear air turbulence are described. The second generation CAT program and those auxiliary activities required to support and verify such a first-of-a-kind system are detailed: aircraft interface; ground and flight verification tests; data analysis; and laboratory examinations.

Harris, C. E.↗

The rings of Saturn - New near-infrared reflectance measurements and a 0.326-4.08 micron summary

A new high-photometric-precision reflectance spectrum of Saturn's rings covering the spectral region 0.65 to 2.5 microns is presented and three previously unreported absorption features at 1.25, 0.85, and probably 1.04 microns are identified. The 1.25- and 1.04 micron absorptions are due to water ice. The 0.85 microns feature may be due to a combination of 0.81- and 0.90 micron ice absorptions but this feature appears too strong relative to the 1.04 micron band to be completely explained by water ice. Another possibility is that the 0.85 micron band is due to Fe(3+)-bearing minerals in an ice-mineral mixture. This explanation could also account for the drop in the visible and ultraviolet reflectance and the rise in reflectance around 3.6 microns. Finally, a composite spectrum from 0.325 to 4.08 is presented which will be useful for future analysis and laboratory studies.

Clark, R. N.↗

Exceedance statistics of accelerations resulting from thruster firings on the Apollo-Soyuz mission

Spacecraft acceleration resulting from firings of vernier control system thrusters is an important consideration in the design, planning, execution and post-flight analysis of laboratory experiments in space. In particular, scientists and technologists involved with the development of experiments to be performed in space in many instances required statistical information on the magnitude and rate of occurrence of spacecraft accelerations. Typically, these accelerations are stochastic in nature, so that it is useful to characterize these accelerations in statistical terms. Statistics of spacecraft accelerations are summarized.

Fichtl, G. H.↗

Release of volatiles from possible Martian analogs

Viking data suggest the presence of volatile-rich materials in the Martian regolith. The thermal stabilities of mineral phases and their volatile release profiles were studied in detail in our laboratory. Thermal analysis, combined with mass spectrometry, was applied to the study of the behavior of carbonates, sulfates, hydrates, and clays. The results indicate that these techniques are useful in the preliminary mineralogical characterizations of volatile-rich minerals. However, our results also indicate that great care must be taken in the incorporation into planetary probes of such methods as hearing rates, pressure, composition of atmospheres, grain size, etc., because these factors effect volatile release.

Kotra, R. K.↗

Exceedance statistics of accelerations resulting from thruster firings on the Apollo-Soyuz mission

Spacecraft acceleration resulting from firings of vernier control system thrusters is an important consideration in the design, planning, execution and post-flight analysis of laboratory experiments in space. In particular, scientists and technologists involved with the development of experiments to be performed in space in many instances required statistical information on the magnitude and rate of occurrence of spacecraft accelerations. Typically, these accelerations are stochastic in nature, so that it is useful to characterize these accelerations in statistical terms. Statistics of spacecraft accelerations are summarized. Previously announced in STAR as N82-12127

Fichtl, G. H.↗

Multijunction cells for concentrators: Technology prospects

Development of high-efficiency multijunction solar cells for concentrator applications is a key step in achieving the goals of the U.S. Department of Energy National Photovoltaics Program. This report summarizes findings of an issue study conducted by the Jet Propulsion Laboratory Photovoltaic Analysis and Integration Center, with the assistance of the Solar Energy Research Institute and Sandia National laboratoies, which surveyed multijunction cell research for concentrators undertaken by federal agencies and by private industry. The team evaluated the potentials of research activities sponsored by DOE and by corporate funding to achieve projected high-efficiency goals and developed summary statements regarding industry expectations. Recommendations are made for the direction of future work to address specific unresolved aspects of multijunction cell technology.

Ferber, R. R.↗

Microwave analog fiber-optic link for use in the deep space network

A novel fiber-optic system with dynamic range of up to 150 dB-Hz for transmission of microwave analog signals is described. The design, analysis, and laboratory evaluations of this system are reported, and potential applications in the NASA/JPL Deep Space Network are discussed.

Logan, R. T., Jr.↗