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All sourcesNASA NTRSDOE OSTI
NASA NTRS2010

History of Space Shuttle Main Engine Turbopump Bearing Testing at the Marshall Space Flight Center

The Space Shuttle is propelled into orbit by two solid rocket motors and three liquid fed main engines. After the solid motors fall away, the shuttle engines continue to run for a total time of 8 minutes. These engines are fed propellants by low and high pressure turbopumps. A critical part of the turbopump is the main shaft that supports the drive turbine and the pump inducer and impeller. Rolling element bearings hold the shaft in place during rotation. If the bearings were to fail, the shaft would move, allowing components to rub in a liquid oxygen or hydrogen environment, which could have catastrophic results. These bearings are required to spin at very high speeds, support radial and axial loads, and have high wear resistance without the benefit of a conventional means of lubrication. The Rocketdyne built Shuttle turbopumps demonstrated their capability to perform during launches; however, the seven hour life requirement was not being met. One of the limiting factors was the bearings. In the late 1970's, an engineering team was formed at the Marshall Space Flight Center (MSFC), to develop a test rig and plan for testing the Shuttle s main engine high pressure oxygen turbopump (HPOTP) bearings. The goals of the program were to better understand the operation of bearings in a cryogenic environment and to further develop and refine existing computer models used to predict the operational limits of these bearings. In 1982, testing began in a rig named the Bearing and Seal Material Tester or BSMT as it was commonly called. The first testing investigated the thermal margin and thermal runaway limits of the HPOTP bearings. The test rig was later used to explore potential bearing improvements in the area of increased race curvatures, new cage materials for better lubrication, new wear resistant rolling element materials, and other ideas to improve wear life. The most notable improvements during this tester s time was the incorporation of silicon nitride balls and bronze filled polytetrafluoroethylene (PTFE) cage inserts into the bearings and the anchoring of the SHABERTH bearing model and SINDA thermal computer model for cryogenic bearing analysis. In the mid 1990's, Pratt and Whitney (P&W) won the contract to deliver new high pressure turbopumps for the Shuttle s engines. P&W used two new bearing materials for the rings, Cronidur 30 and AISI 9310 steel and testing was needed on these new materials. A test rig had been designed and delivered to MSFC for testing hydrostatic bearings but with the need by Pratt to validate their bearings, the rig was reconfigured for testing of two ball bearings or a ball bearing and a roller bearing. The P&W bearings are larger than the Rocketdyne bearings and could not be installed in the BSMT. This new test rig was called the LH2 test rig and began operation in 1995. The LH2 test rig accumulated 75,000 seconds of run time in hydrogen. This test rig was valuable in two areas: validating the use of silicon nitride balls and rollers in Alternate Turbopump Development (ATD) bearings, which Pratt eventually used, and in proving the robustness of the balls and rollers after river marks appeared on the surface of the rolling elements. Individual test reports have been presented at conferences and symposiums throughout the years. This paper is a comprehensive report of all the bearing testing done at Marshall. It represents thousands of hours of dedication and labor in all engineering and technical fields that made this program a success.

Gibson, Howard↗
DOE OSTI2023

Transactive Emergency Power Allocation

The devastating impacts of extreme weather events, many of which are climate-change related, are increasingly evident through the frequency and duration of outages on power grids, especially the distribution systems. One of the major modern-day concerns of utilities is dealing with such extreme supply outages where operators have used rolling blackouts as a contingency plan balance supply and demand while serving critical loads. Such events have significant repercussions social and economic costs. Such blackouts practices are a blunt instrument, depriving customers with low-capacity high-priority loads (i.e. refrigeration, water, telecommunication, etc.) that provide high marginal amenity. Our contribution presented in this work is a transactive emergency allocation mechanism that would provide some minimum level of service to all of the customers while enabling preference-based trading of this initial allocation. This is in contrast to the state-of-art TE mechanisms that allocate resources to customers solely based on their willingness-to-pay. The effectiveness of the proposed mechanism is demonstrated through simulation-based evaluation on a prototypical distribution system experiencing 12-hour scarcity-based emergency event due to extreme operating conditions. Simulation results clearly demonstrate the capability of the proposed transactive emergency allocation mechanism in effectively utilizing the available energy and providing some level of service to all customers to operate their high-priority loads throughout the extreme scarcity event while being economically efficient in allowing trading of allocation based on customer preferences.

transactive energy, power system economics, emerge↗
DOE OSTI2025

Coherency-Constrained Spectral Clustering for Power Network Reduction

This paper presents a methodology for reducing the complexity of large-scale power network models using spectral clustering, aggregation of electrical components, and cost function approximation. Two approaches are explored using unconstrained and constrained spectral clustering to determine areas for effective system reduction. Once the system areas are determined, both loads and generators by type are aggregated, and their new cost function is approximated through polynomial curve-fitting or statistical methods. The performance of reduced networks is evaluated in terms of their ability to follow the true daily cost of the original system over a 24-hour period considering a set of several days. Two test systems are taken as test beds. Application of the methodology to a modified version of the IEEE 39-bus system reduces it from 17 generators to a 4-bus system and 9 generators with about 93% of accuracy. Similarly, the IEEE 118-bus system is reduced from 19 generators to a 3-bus system with three aggregated units achieving over 99% of accuracy. These findings address scalability challenges and enhance accuracy for high and mid-loading level conditions, and by aggregating thermal units with similar cost functions.

42 ENGINEERING↗
DOE OSTI2024

Side-by-Side Comparison of Subhourly Clipping Models

Over the past several years there have been numerous attempts at quantifying the inherent power clipping of inverters due to sub-hourly irradiance variability that is not captured in hourly PV performance models. Different models have been proposed to correct for these clipping losses in PV performance estimates, including matrix lookup models, distribution modeling of the PV power performance within a given hour, and machine learning methods. To date, there have been few comprehensive quantitative comparisons of these inverter clipping correction modeling approaches to evaluate the effectiveness of these approaches in predicting the actual behavior of PV system inverter clipping. In this study, we perform such a comparison, evaluating the Allen and Walker correction loss modeling approaches recently implemented in the System Advisor Model (SAM) against clipping losses modeled with 1-minute climate data. These comparisons were performed across a variety of climate locations and inverter loading ratios to thoroughly analyze the effectiveness of these modeling approaches relative to each other. Results from this analysis reveal that both clipping correction approaches improve annual energy accuracy to within 2% of 1-minute modeled energy yield. The two models predict annual clipping loss more accurately than simple hourly power limit clipping, with the Allen method typically being slightly more accurate at typical ILR values and the Walker method often being slightly more accurate at high ILR values The models can improve accuracy over the status quo clipping approach up to 3 percentage points in systems with ILR of 2.0, showing the importance of this modeling factor in energy yield estimates.

ENERGY PLANNING, POLICY, AND ECONOMY,MATHEMATICS A↗
DOE OSTI2022

Stable, high-performing bifunctional electrodes for anion exchange membrane-based unitized regenerative fuel cells

Anion exchange membrane unitized regenerative fuel cells (AEM-URFCs) are a promising technology for energy storage and electricity production; however, their efficiency is limited by the kinetics of the bifunctional oxygen electrode (BOE) where the oxygen evolution reaction (OER) and oxygen reduction reaction (ORR) occur. A particular concern when designing the BOE is that the OER and ORR have differing catalytic requirements, which make it challenging to develop effective bifunctional electrocatalysts with single active sites. In this study, we focus on advancing the BOE performance using Pt-IrO x and Pt-NiCoO x electrocatalysts. Here, single-layer and dual-layer Pt-IrO x BOEs were made, with the dual-layer electrode leading to improved performance due to efficient catalyst utilization in both modes. Using the dual-layer oxygen electrode paired with a PtRu/C hydrogen electrode, a round trip efficiency (RTE) as high as 50% (62 %iR-free) was achieved at 500 mA/cm 2 and operation for more than 24 h, which included five one-hour-long H 2 generation and consumption cycles followed by one eight-hour-long cycle. To the best of our knowledge, this is the highest performance for AEM-URFCs reported to date. Lastly, the approach is extended to electrodes with a Pt loading of 0.5 mg/cm 2 and the IrO x substituted by NiCoO x .

25 ENERGY STORAGE↗
DOE OSTI2021

Photoelectrochemically Self Improving Si/GaN Photocathode: Figure 1d Raw Data

Fig1d results were obtained using a 3-electrode configuration with IrOx as the counter electrode and saturated calomel electrode as the reference electrode. Two Si/GaN photocathodes were compared. Sample #1 (named as S#1) was the as-received sample, and sample #2 (named as S#2) was CA tested for 4 hours under same testing conditions described in Fig.1a. The PEC performance (J-V curve) was recorded for both samples. Then a photodeposition of Pt was performed on both samples, each loading time was set to be 5 minutes, then the J-V curve was recorded to track the changes of the performance. The Pt photodeposition was stopped until the J-V curve won't shift (the maximum onset potential was achieved). The results show that, S#1 needs at least 20 minutes of Pt photodeposition to achieve its best PEC performance while S#2, which is after CA testing, only needs 5 minutes of Pt photodeposition to achieve its best PEC performance.

photocathode↗
DOE OSTI2023

Durable Fuel Cell MEA through Immobilization of Catalyst Particle and Membrane Chemical Stabilizer

For hydrogen-based fuel cell electric vehicle to be cost competitive with the incumbent diesel-powered internal combustion engine heavy-duty vehicle, the total cost of ownership of the truck must be decreased via both capital cost and the operating cost (H 2 fuel expense) reduction. This puts the emphasis on the decrease of fuel cell stack cost via use of low platinum catalyst material usage to decrease capital cost, high H 2 fuel efficiency and high stack durability to decrease the operating cost. US DOE has set a target of ≤ 0.25 mgPt/cm 2 total loading in the membrane electrode assembly, high fuel efficiency of > 68% and a HD-combined target of ≥ 2.5 kW/gPGM after running an accelerated stress test (AST) equivalent to 30,000 hours of heavy-duty fuel cell operation.

08 HYDROGEN↗
NASA NTRS2012

Large Scale Flutter Data for Design of Rotating Blades Using Navier-Stokes Equations

A procedure to compute flutter boundaries of rotating blades is presented; a) Navier-Stokes equations. b) Frequency domain method compatible with industry practice. Procedure is initially validated: a) Unsteady loads with flapping wing experiment. b) Flutter boundary with fixed wing experiment. Large scale flutter computation is demonstrated for rotating blade: a) Single job submission script. b) Flutter boundary in 24 hour wall clock time with 100 cores. c) Linearly scalable with number of cores. Tested with 1000 cores that produced data in 25 hrs for 10 flutter boundaries. Further wall-clock speed-up is possible by performing parallel computations within each case.

Guruswamy, Guru P.↗
DOE OSTI2022

Economic Dispatch Optimization of Multi-Unit SMR Site

With the increase of integration of variable renewable into the grid, grid resilience can be compromised without flexible electricity suppliers. Flexible operation of NPP can expand the scope of integration of new nuclear power plants in regions with high share of renewables. It also provides opportunity to increase profits through participation in ancillary services. In this research, NuScale modules are used as the case study. NuScale is an integrated pressurized water reactor with thermal power of 250 MWth. Having multiple units can provide higher flexibility in changing power levels and supplying the grid with electricity all year long. Additionally, load-following might perturbate the ordered sequence of refueling (every 24 months for NuScale). To maintain the 2 year refueling cycles, the loading patterns will need to be adjusted in a year-to-year basis, resulting in additional unnecessary costs. Another solution is to find the optimal outage schedule. This will also shift the focus of the planned outage to a more optimized predictive outages and maintenance. Results from short-term optimization (i.e., daily participation in energy and ancillary services markets) shows that average commitment to regulation down ancillary service markets during late night and early morning hours can increase revenues. Participating in upward reserves during pre-work commuting hours and early evening hours can also generate additional revenues due to high ramp up of electricity demand. Having multiple units at a single site can also help operate flexibly. Results from long-term optimization show that daily fluctuation in electric power is usually handled by few units while other units operate on base-load profile. It is possible to combine base-load operation with flexible operation to extend component remaining useful life in some units and find optimal outage schedule for the units.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗
DOE OSTI2026

Estimating Flexibility Envelopes for Residential Customers From Utility Smart Meter Data: Preprint

Demand response from residential customers has significant potential to support power system operations, but accurate flexibility estimation is challenging due to the limited resolution of advanced metering infrastructure (AMI) data. Most utility AMI measurements are recorded at hourly intervals, with only a small portion at higher resolutions, and even fewer households have appliance-level energy usage data. To address this issue, this paper proposes a two-stage long short-term memory (LSTM) framework for estimating household flexibility envelopes from low-resolution AMI data. In the first stage, the heating, ventilating, and air-conditioning (HVAC) load and non-HVAC loads are estimated by using a model trained on a small set of households with appliance-level profiles. These estimated data are then used to compute the upper- and lower-flexibility bounds, which are subsequently down-sampled to lower-resolution data. In the second stage, these flexibility bounds serve as training inputs for another LSTM model, enabling direct prediction of flexibility envelopes for households with only hourly AMI data. This method is validated using Pecan Street data from two different areas, and the results demonstrate its applicability and effectiveness.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2023

Automated Air Sealing Demonstration: Denver Federal Center Building 40

This project aimed to demonstrate building airtightness achieved by automated air sealing in a commercial building setting. The automated air sealing demonstrated in this project uses a modified blower door to pressurize and distribute the sealing aerosol to achieve the required building airtightness. To demonstrate this technology, Building 40 at the Denver Federal Center, a federally owned campus under the jurisdiction, custody and control of the U.S. General Services Administration (GSA), was selected for testing (Figure 2). This building is currently undergoing several retrofit projects, including increasing insulation, installing high-performance windows, and adding advanced equipment, control systems, and automated air sealing. This demonstration project involved installing automated air sealing and measuring the improvements in the building's airtightness. The automated air sealing was installed over two days by AeroBarrier, the vendor. An external blower door test contractor measured the airtightness of the demonstration space before and after air sealing. The new airtightness value and the percentage increase in airtightness were used to evaluate the energy savings potential of automated air sealing. These airtightness values were used to compute the energy savings and CO 2 emissions reduction for different climate zones, building types, and initial airtightness conditions. In addition, the heating, ventilation and air conditioning (HVAC) load reduction attributable to the reduced building air leakage was studied. This study included research to determine the cost and time reduction of automated air sealing. Finally, the automated air sealing performance was evaluated qualitatively using a focus group discussion that included GSA and Bristol, the general contractor. The installation has shown the demonstration site, with a floor size of 4,462 ft 2 , air leakage has reduced by more than 50% in less than 7 hours, including preparation, site sealing, and cleanup. The performance objectives were classified as quantitative or qualitative based on the evaluation metrics used to assess the project’s success. The key performance objectives for this project were the level of airtightness achieved, the time and cost required to perform the sealing, and the HVAC load reduction attributable to air sealing. Table 1 shows the quantitative performance objectives.

42 ENGINEERING↗
NASA NTRS2012

Advanced Lithium Ion Venus Explorer (ALIVE)

The COncurrent Multidisciplinary Preliminary Assessment of Space Systems (COMPASS) Team partnered with the Applied Research Laboratory to perform a NASA Innovative Advanced Concepts (NIAC) Program study to evaluate chemical based power systems for keeping a Venus lander alive (power and cooling) and functional for a period of days. The mission class targeted was either a Discovery ($500M) or New Frontiers ($750M to $780M) class mission. Historic Soviet Venus landers have only lasted on the order of 2 hours in the extreme Venus environment:temperatures of 460 degrees Centigrade and pressures of 93 bar. Longer duration missions have been studied using plutonium powered systems to operate and cool landers for up to a year. However, the plutonium load is very large. This NIAC study sought to still provide power and cooling but without the plutonium. Batteries are far too heavy but a system which uses the atmosphere (primarily carbon dioxide) and on on-board fuel to power a power generation and cooling system was sought. The resuling design was the Advanced Long-Life Lander Investigating the Venus Environment (ALIVE) Spacecraft (S/C) which burns lithium (Li) with the CO2 atmosphere to heat a Duplex Stirling to power and cool the lander for a 5-day duration (until the Li is exhausted). While it does not last years a chemical powered system surviving days eliminates the cost associated with utilizing a flyby relay S/C and allows a continuous low data rate direct to earth (DTE) link in this instance from the Ovda Regio of Venus. The five-day collection time provided by the chemical power systems also enables science personnel on earth to interact and retarget science - something not possible with an approximately 2-hour spacecraft lifetime. It also allows for contingency operations directed by the ground (reduced risk). The science package was based on that envisioned by the Venus Intrepid Tessera Lander (VITaL) Decadal Survey Study. The Li Burner within the long duration power system creates approximately 14000 W of heat. This 1300 degree Centigrade heat using Li in the bottom "ballast" tank is melted to liquid by the Venus temperature, drawn into a furnace by a wick and burned with atmospheric CO2. The Li carbonate exhaust is liquid at 1300 degrees Centigrade and being denser than Li drains into the the Li tank and solidifies. Since the exhaust product is a dense liquid no "chimney" is required which conserves the heat for the stirling power convertor. The Duplex Stirling provides about 300 W of power and removes about 300 W of heat from the avionics and heat that leaks into the 1-bar-insulated payload pressure vessel kept at 25 degrees Centigrade. The Na K radiator is run to the top of the drag flap.The ALIVE vehicle is carried to Venus via an Atlas 411 launch vehicle (LV) with a C3 of 7 km2/s2. An Aeroshell, derived from the Genesis mission, enables a direct entry into the atmosphere of Venus (-10 degrees Centigrade, 40 g max) and 6 m/s for landing (44 g) using a drag ring. For surface science and communication, a 100 WRF (WebEx Recording Format), X-Band 0.6-meter pointable DTE (Direct-to-Earth) antenna provides 2 kbps (kilobits per second) to DSN (Deep-Space Network) 34-meter antenna clusters.Table 1.1 summarizes the top-level details of each subsystem that was incorporated into the design. Cost estimates of the ALIVE mission show it at approximately $760M which puts it into the New Frontiers class.The ALIVE landed duration is only limited by the amount of Li which can be carried by the lander. Further studies are needed to investigate how additional mass can be carried, perhaps by a larger launcher and larger aeroshell.

Exploration↗
DOE OSTI2021

Heterogeneous photo-Fenton-like degradation of emerging pharmaceutical contaminants in wastewater using Cu-doped MgO nanoparticles

In this study, a facile thermal decomposition method was utilized to synthesize Cu-doped MgO nanoparticles possessing mesoporosity. These mesoporous Cu doped MgO nanoparticles were shown to be efficient photo-Fenton-like catalysts for the degradation of emerging pharmaceutical contaminants in wastewater and were able to completely oxidize salicylic acid within 1 hour under optimized conditions. Tetracycline was shown to be converted to other intermediates with a large portion of it undergoing full mineralization. Batch experiments were conducted to demonstrate the effects of Cu loading on MgO, overall catalyst loading, and H 2 O 2 concentration on the salicylic acid and tetracycline conversion and rate constants. Quenching experiments revealed that both •OH radicals or HO 2 •/•O 2 - radicals were involved in the reaction, with the latter showing a higher contribution. The surface dissolution of MgO was shown to facilitate a high pH environment which completely prevented Cu from leaching out of the catalyst while retaining high activity. The catalyst reusability was shown to be satisfactory with high activity and conversion being preserved over five cycles.

04 OIL SHALES AND TAR SANDS↗
DOE OSTI2022

Regenerable solvents mediate accelerated low temperature CO 2 capture and carbon mineralization of ash and nano-scale calcium carbonate formation

The dual need to remove CO 2 from our emissions and treat alkaline industrial residues such as ash materials motivate the design of innovative pathways to simultaneously capture and convert CO 2 into mineralized carbonates. Direct carbon mineralization is one approach that addresses the need to simultaneously treat alkaline industrial residues and mineralize CO 2 emissions. Low CO 2 solubility in water and slow kinetics at ambient temperature have challenged the direct carbon mineralization of alkaline industrial residues. Here, to address these challenges, the use of CO 2 capture solvents that enhance CO 2 solubility and facilitate accelerated carbon mineralization of fly ash at temperatures below 90 °C is investigated. Calcium carbonate formation results in the inherent regeneration of the solvent. The carbon mineralization extents of non-calcium carbonate content in fly ash were 50% and 51% and in waste ash were 58% and 62% in 2.5 M sodium glycinate and 30 wt% MEA solutions, respectively. The experiments were performed at 50 °C for 3 hours with CO 2 partial pressure of 1 atm in a continuously stirred slurry environment with 15 wt.% solid. Furthermore, nanoscale CaCO 3 is successfully synthesized from dissolved calcium using CO 2 -loaded sodium glycinate and surfactants such as CTAB (Cetyl Trimethyl Ammonium Bromide). Surfactants such as CTAB bind to the calcium carbonate surface and regulate the growth of calcium carbonate particles. These innovative approaches demonstrate the feasibility of directly storing CO 2 in fly ash and waste ash as calcium carbonate and producing nanoscale calcium carbonate using regenerable CO 2 capture solvents.

42 ENGINEERING↗
DOE OSTI2022

Universal Solvent Viscosity Reduction via Hydrogen Bonding Disruptors

Liquid Ion Solutions LLC (DBA RoCo Global) in partnership with Carnegie Mellon University and Carbon Capture Scientific LLC, has performed lab-scale development and evaluation of novel additives that lower the viscosity of water-lean amine solvents for post-combustion carbon dioxide capture. This project focuses on developing additives that minimize the formation of long-range electrostatic and hydrogen bonding (HB) networks, decreasing the solvent viscosity, improving diffusion, and improving the process economics. The project objectives included: 1) performing computer simulation to understand the molecular interactions of the additive molecules in water-lean CO 2 capture solvents, 2) design and synthesis of HB disruptors additives, 3) performance testing with additive molecules on model amine solvents, and 4) demonstration of the effectiveness of the optimized additives in the presence of synthetic flue gas. To meet the abovementioned objectives, the project team utilized a holistic approach that combines molecular simulation, experimental testing, and economic analysis studies. The project team developed ab initio molecular model and then perform computer simulation to develop relationship between hydrogen bonding, viscosity, and performed quantitative analysis of additive on the viscosity of the solvent. The team completed computational comparative study on a range of organic functional groups such as ethers, esters, cyclic carbonates, alkanes, and ammonium salts for their effect on viscosity gaining key insights into molecular interactions and the impact of various functional groups and molecular shapes on viscosity. Assisted with molecular simulation insights, the project team conducted additive synthesis and testing, including a proof-of-concept study, additive screening, optimization, and synthetic flue gas testing. The experimental proof-of-concept study proved that the hydrogen bonding acceptors result in significant decrease of viscosities. Detailed additive screening (exploring various functionalities and molecular structures) has been performed. Several promising additives showed excellent reduction in viscosity (30-41%) at 5% additive loading, and over 50% viscosity reduction at 10% additive loading for the model solvents. The team also performed complex screening studies on additive loadings and mixing effect among additives using the design of experiments. Based on multiple screening experiments, one additive-solvent candidate was down-selected for synthetic flue gas testing. A 100-hour continuous absorption/desorption study was conducted under simulated flue gas using a lab-scale continuous capture and separation system. No degradation (for both solvent and additive) was observed based on the GC results of the solvent samples collected from the continuous study. The team conducted preliminary engineering analyses and cost-benefit analyses to quantify the potential economic benefits of the additive approach for solvent viscosity reduction. Based on the experimental data, CO 2 capture cost savings from the capital and operating cost savings are estimated at $\$$4.7/tonne and $\$$0.3/tonne CO 2 captured, respectively. Considering the additive cost, the net benefit is estimated to be between $\$$4.32~$\$$4.86/tonne CO 2 captured.

20 FOSSIL-FUELED POWER PLANTS↗
DOE OSTI2024

Lignin content of Populus trichocarpa residues after CELF pretreatment and CBP fermentation

Here we present a dataset of lignin content from a woody energy crop (Populus trichocarpa) residues after a series of co-solvent enhanced lignocellulosic fractionation (CELF) pretreatment and consolidated bioprocessing (CBP) process. The natural poplar variant GW-9947 from the Center for Bioenergy Innovation (CBI) was used. The poplar was knife milled and passed through a 1 mm sieve and CELF pretreatment was performed in a Parr autoclave reactor with 7.5 wt % solids loading, 0.5 wt% H2SO4 as catalyst at 150°C with 5, 15, 25 and 30 minutes, respectively. Tetrahydrofuran was added in a 1:1 mass ratio with water as the pretreatment solvent. The residues from CELF pretreatment were then subjected to CBP using the bacterium C. thermocellum DSM 1313. CBP fermentations were performed at 60 °C in a shaker at 50, 75, and 100 grams/L solids loadings. The Klason lignin was measured using a two-step acid hydrolysis process. In brief, the poplar samples were first hydrolyzed by 72 wt% sulfuric acid at 30 oC for an hour. The hydrolysates were then diluted to 4 wt% sulfuric acid using deionized water and subsequently autoclaved at 121 oC for 1 h. Upon the completion of the two-step hydrolysis, the resulting solution was cooled to room temperature and the precipitate was then filtered through a G8 glass fiber filter through a crucible, dried at oven for overnight, and weighed to get the Klason lignin content. The lignin data provides information about lignin content changes after CELF and C. thermocellum CBP process.

Lignin Populus trichocarpa CELF pretreatment CBP f↗
NASA NTRS1977

Accelerated life tests of specimen heat pipe from Communication Technology Satellite (CTS) project

A gas-loaded variable conductance heat pipe of stainless steel with methanol working fluid identical to one now on the CTS satellite was life tested in the laboratory at accelerated conditions for 14 200 hours, equivalent to about 70 000 hours at flight conditions. The noncondensible gas inventory increased about 20 percent over the original charge. The observed gas increase is estimated to increase operating temperature by about 2.2 C, insufficient to harm the electronic gear cooled by the heat pipes in the satellite. Tests of maximum heat input against evaporator elevation agree well with the manufacturer's predictions.

Tower, L. K.↗
NASA NTRS1985

Bonding and nondestructive evaluation of graphite/PEEK composite and titanium adherends with thermoplastic adhesives

Bonded single overlap shear specimens were fabricated from Graphite/PEEK (Polyetheretherketone) composite adherends and titanium adherends. Six advanced thermoplastic adhesives were used for the bonding. The specimens were bonded by an electromagnetic induction technique producing high heating rates and high-strength bonds in a few minutes. This contrasts with conventionally heated presses or autoclaves that take hours to process comparable quality bonds. The Graphite/PEEK composites were highly resistant to delamination during the testing. This allowed the specimen to fail exclusively through the bondline, even at very high shear loads. Nondestructive evaluation of bonded specimens was performed ultrasonically by energizing the entire thickness of the material through the bondline and measuring acoustic impedance parameters. Destructive testing confirmed the unique ultrasonic profiles of strong and weak bonds, establishing a standard for predicting relative bond strength in subsequent specimens.

Hodges, W. T.↗