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At least 577 records · Page 32

All sources NASA NTRS DOE OSTI

NASA NTRSDate not supplied

ISS Wastewater Pretreatment via DNA Pattern Picofilter Using Inorganic Brine Stimulant

Astronauts in the International Space Station (ISS) need as much water as they can access, whether it comes from people's breath, sweat or urine, recycled shower water or hand washing. It is of vital importance that any type of water is recycled and filtrated through different methods so it can be re-used. Recently, Cerahelix Inc. offered a ceramic tubular membrane element that uses DNA strands as a pattern in a sol-gel process that allows the sintered product to have a pore size in the picometer scale and claims to achieve ten times higher purity than other commercially available ceramic filters. This should allow higher purities and yields at reduced energy costs and theoretically allow near total dewatering of the reject stream and greater than 80% removal of polyvalent ions. Trials were performed with Cerahelix Inc. filters using an inorganic brine simulant at two pHs to test the efficiency of Pico Helix TM membranes and determine their feasibility for spacecraft wastewater treatment processes. Emphasis was placed on the polyvalent ions: SO42-, PO43-, Mg2+, and Ca2+. These ions should be rejected almost entirely from the feed solution and, not permeate through the filter. Results show that at a pH of 4.2, permeation of the polyvalent ions varied from 59% to 74% and at pH of 8.0, permeation varied from 72% to 87%. An Extended Nernst Planck (ENP) approach that describes the mass transfer process for a pico-filtration membrane was used to construct a model to inform the experimental expectations and outcome.

Carolina Franco↗

NASA NTRSDate not supplied

Particle Loading Tests on HEPA Flat Sheet Media at Sub-Ambient Pressures Using a Lunar Dust Simulant

When humans return to the moon under the NASA Artemis program, their activities on the lunar surface will inevitably lead to the intrusion of some level of lunar dust into the lander cabin. Therein the crew would be exposed to the potential hazards of lunar dust and the possibility of subsequent transfer into orbiting segments after docking. The spacecraft’s cabin filtration system will need to be effective at removing the airborne lunar dust to properly purify the breathable cabin air and minimize the spreading of the dust throughout the vehicle and orbital segments through the mission duration. The fine nature of the lunar dust will require high efficiency filtration, such as HEPA. A series of tests were performed in a specially designed recirculating sealed flow loop, for testing filter media and filter elements at the NASA Glenn Research Center. The flow loop was used to assess the performance and capacity of flat sheet filter media at representative cabin pressures using JSC-1AF lunar he filter media was measured as a function of accumulated particle mdust simulant and at high rates of particle loading. The pressure drop across tass load at ambient pressure and at two sub-ambient pressures, 0.0703MPa and 0.0565MPa, and at a media velocity that was scaled relative to its pleated configuration. The challenge particle flows were generated by a custom designed particle generator that introduces dispersed particles of the lunar simulant at high concentrations. An optical particle counting instrument provided filter efficiency measurements within the sealed environment. The pressure drop was found to increase linearly with the amount of dust load on the media, for all test conditions, while the starting pressure drop was found to be lower at the lowest sub-ambient pressure case. High filter efficiency was maintained after high particle loads on the media

Sub-ambient↗

NASA NTRSDate not supplied

Flight Environment HEPA Filter Testing for Lunar Dust Removal Capability

Lunar dust is an abrasive regolith that can cause critical damage to hardware and crew. Its morphology and chemical makeup differs from typical earth dust due to space weathering effects. Current space missions require extensive air filtration of lunar dust to ensure mission success; as such filtration testing is paramount in verifying the dust-removal capabilities of the system. Previous testing at NASA GRC consisted of two stages: testing a flat high efficiency particulate air (HEPA) media sheet at various pressure ranges (Stage 1) and testing a pleated HEPA filter at different humidity and dust levels (Stage 2). This testing was done to buy-down risk when testing the flight-qualification HEPA filter for the proposed Stage 3 test. Stage 3 testing used a flight-ready HEPA filter to measure its performance characteristics to verify programmatic requirements. This included measuring lunar dust loading versus pressure drop performance and establishing a maximum capacity based on the allowable pressure drop, determining the HEPA filter efficiency utilizing two separate methodologies, and assessing if the lunar dust caused the HEPA filter to experience any damage. Additionally, dust removal from the HEPA filter was performed using a vacuum to ascertain if the filter life can be prolonged. These test results will aid the program in verifying programmatic requirements and ensuring risk buydown before this HEPA filter takes flight.

HEPA↗

NASA NTRSDate not supplied

Testing of the ISS’s Charcoal HEPA Integrated Particle Scrubber (CHIPS) Filters to Ascertain an Efficiency Curve and Most Penetrating Particle Size

High air quality is a top priority in hermetically sealed environments, such as the International Space Station (ISS). Aerosol particulate filtration on the ISS is achieved via 21 HEPA filters. Traditional HEPA filters have an efficiency of 99.97%, but HEPA filters aboard the ISS have been found to achieve 99.99% efficiency. This may be due to the flight-grade HEPA filters chosen or, less likely, that they are combined with activated charcoal filters for siloxane removal in a combination referred to as Charcoal HEPA Integrated Particle Scrubbers (CHIPS) filters. All filters have a Most Penetrating Particle Size (MPPS), but, until now, the MPPS and efficiency curve of the CHIPS filters was not known. The efficiency curve of the CHIPS filters was ascertained at NASA Glenn Research Center through standard salt crystal aerosolization. This method was selected over aerosolized oil droplets due to a desire to preserve the filter’s function for further testing. The CHIPS filters were tested as they are oriented on the ISS (activated charcoal filter followed by a flight-grade HEPA filter), with the HEPA portion alone, and with the activated charcoal portion alone. The results of this experiment are generally useful but can be especially useful for the microbiology and Environmental Control and Life Support Systems (ECLSS). This is due to microbial contamination being a potential concern in the air revitalization systems on the ISS. Knowing the MMPS of the CHIPS filters, in conjunction with levels of airborne microbes, is useful for predicting which and how many microbes are likely to get through the HEPA filters that sit in the beginning of the ISS airstream. It may also be useful to other groups at NASA to know how many particulates are able to pass through high-efficiency filtration, and even for healthcare cleanrooms and other air purification pursuits.

A Nicolas Whitlock↗

NASA NTRS2024

Evaluation of the Accumulation of Foreign Object Debris in the International Space Station Ventilation Systems and Resulting Impacts to Systems

A challenge for the International Space Station (ISS) is accumulation of Foreign Object Debris (FOD) and the impacts to crew, equipment, and experiments. One function of the temperature and humidity control system is to capture FOD with various methods of filtration to minimize these impacts. ISS filtration has been augmented by charcoal filters and screens. A qualitative comparison of the quantity of FOD found over the years and the current levels are evaluated. Impacts to FOD are crew time for cleaning, reduction of equipment life, and component damage and examples are provided. Recommendations for further improvements to reduce the accumulation of FOD on ISS is provided.

ISS↗

NASA NTRSDate not supplied

Evaluation of the Accumulation of Foreign Object Debris in the International Space Station Ventilation Systems and Resulting Impacts to Systems

A challenge for the International Space Station (ISS) is accumulation of foreign object debris (FOD) in the ventilation systems and the impacts to crew, equipment, and experiments. One function of the temperature and humidity control system is to capture FOD with various methods of filtration to minimize these impacts. ISS filtration has been augmented by charcoal and High Efficiency Particulate Air (HEPA) filters and screens. A qualitative comparison of the quantity of FOD found since 2012 study and the current levels are evaluated. Impacts due to FOD are reduced air circulation, increased crew time for cleaning, reduction of equipment life, and component damage; examples are provided. Recommendations for further improvements to reduce the accumulation of FOD on ISS are provided.

ISS↗

DOE OSTI2014

Development and Testing of an Americium/Lanthanide Separation Flowsheet Using Sodium Bismuthate

The separation of Am from the lanthanides and curium is a key step in proposed advanced fuel cycle scenarios. The partitioning and transmutation of Am is desirable to minimize the long-term heat load of material interred in a future high-level waste repository. A separation process amenable to process scale-up remains elusive. Given only subtle chemistry differences within and between the ions of the trivalent actinide and lanthanide series this separation is challenging ; however, higher oxidation states of americium can be prepared using sodium bismuthate and separated via solvent extraction using diamylamylphosphonate (DAAP) extraction. Among the other trivalent metals only Ce is also oxidized and extracted. Due to the long-term instability of Am(VI) , the loaded organic phase is readily selectively stripped to partition the actinide to a new acidic aqueous phase. Batch extraction distribution ratio measurements were used to design a flowsheet to accomplish this separation. Additionally, crossflow filtration was investigated as a method to filter the bismuthate solids from the feed solution prior to extraction. Results of the filtration studies, flowsheet development work and flowsheet performance testing using a centrifugal contactor are detailed.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

DOE OSTI2014

Optimization of Ventilation Energy Demands and Indoor Air Quality in High-Performance Homes

High-performance homes require that ventilation energy demands and indoor air quality (IAQ) be simultaneously optimized. We attempted to bridge these two areas by conducting tests in a research house located in Oak Ridge, TN, that was 20 months old, energy-efficient (i.e., expected to consume 50% less energy than a house built per the 2006 IRC), tightly-built (i.e., natural ventilation rate ~0.02 h-1), unoccupied, and unfurnished. We identified air pollutants of concern in the test home that could generally serve as indicators of IAQ, and conduced field experiments and computer simulations to determine the effectiveness and energy required by various techniques that lessened the concentration of these contaminants. Formaldehyde was selected as the main pollutant of concern among the contaminants that were sampled in the initial survey because it was the only compound that showed concentrations that were greater than the recommended exposure levels. Field data indicate that concentrations were higher during the summer primarily because emissions from sources rise with increases in temperature. Furthermore, supply ventilation and gas-phase filtration were effective means to reduce formaldehyde concentrations; however, exhaust ventilation had minimal influence on this pollutant. Results from simulations suggest that formaldehyde concentrations obtained while ventilating per ASHRAE 62.2-2010 could be decreased by about 20% from May through September through three strategies: 1) increasing ASHRAE supply ventilation by a factor of two, 2) reducing the thermostat setpoint from 76 to 74 F, or 3) running a gas-phase filtration system while decreasing supply ventilation per ASHRAE by half. In the mixed-humid climate of Oak Ridge, these strategies caused increases in electricity cost of ~$5 to ~$15/month depending on outdoor conditions.

Hun, Diana E↗

DOE OSTI2014

Method for reducing pressure drop through filters, and filter exhibiting reduced pressure drop

Methods for generating and applying coatings to filters with porous material in order to reduce large pressure drop increases as material accumulates in a filter, as well as the filter exhibiting reduced and/or more uniform pressure drop. The filter can be a diesel particulate trap for removing particulate matter such as soot from the exhaust of a diesel engine. Porous material such as ash is loaded on the surface of the substrate or filter walls, such as by coating, depositing, distributing or layering the porous material along the channel walls of the filter in an amount effective for minimizing or preventing depth filtration during use of the filter. Efficient filtration at acceptable flow rates is achieved.

36 MATERIALS SCIENCE↗

DOE OSTI2015

Technology Solutions Case Study: Ventilation System Effectiveness and Tested Indoor Air Quality Impacts

Ventilation system effectiveness testing was conducted at two unoccupied, single-family, detached lab homes at the University of Texas - Tyler. Five ventilation system tests were conducted with various whole-building ventilation systems. Multizone fan pressurization testing characterized building and zone enclosure leakage. PFT testing showed multizone air change rates and interzonal airflow filtration. Indoor air recirculation by a central air distribution system can help improve the exhaust ventilation system by way of air mixing and filtration. In contrast, the supply and balanced ventilation systems showed that there is a significant benefit to drawing outside air from a known outside location, and filtering and distributing that air. Compared to the Exhaust systems, the CFIS and ERV systems showed better ventilation air distribution and lower concentrations of particulates, formaldehyde and other VOCs.

Airborne particles↗

DOE OSTI2016

High and rapid hydrogen release from thermolysis of ammonia borane near PEM fuel cell operating temperature

A system for generating and purifying hydrogen. To generate hydrogen, the system includes inlets configured to receive a hydrogen carrier and an inert insulator, a mixing chamber configured to combine the hydrogen carrier and the inert insulator, a heat exchanger configured to apply heat to the mixture of hydrogen carrier and the inert insulator, wherein the applied heat results in the generation of hydrogen from the hydrogen carrier, and an outlet configured to release the generated hydrogen. To purify hydrogen, the system includes a primary inlet to receive a starting material and an ammonia filtration subassembly, which may include an absorption column configured to absorb the ammonia into water for providing purified hydrogen at a first purity level. The ammonia filtration subassembly may also include an adsorbent member configured to adsorb ammonia from the starting material into an adsorbent for providing purified hydrogen at a second purity level.

08 HYDROGEN↗

DOE OSTI2018

Hydrogen purification systems for PEM fuel cells

08 HYDROGEN↗

DOE OSTI2018

DIRECT SIMULTANEOUS MEASUREMENT OF PARTICULATE MATTER AND AMMONIA STORAGE ON COMBINED SELECTIVE CATALYTIC REDUCTION FILTER SYSTEMS USING RADIO FREQUENCY SENSORS

Tightening global emissions regulations are motivating interest in the development and implementation of Selective Catalytic Reduction + Filtration (SCRF) systems, which are designed to reduce the concentration of tailpipe particulate matter (PM) and NO x emissions. These systems allow designers to combine the NO x reduction capability of an SCR with the filtration capability of a particulate filter on a single unit. Practical implementation of these systems requires reliable measurement and diagnosis of their state – both with respect to trapped particulate matter as well as adsorbed ammonia. Currently, these systems rely on a variety of gas sensors, mounted upstream or downstream of the system, that only provide an indirect inference of the operation state. In this study, a single radio frequency (RF) sensor was used to perform simultaneous measurements of soot loading and ammonia inventory on an SCRF. Several SCRF core samples were tested at varying soot and ash loads in a catalyst reactor bench. Soot levels were measured by monitoring changes in the bulk dielectric properties within the catalyst using the sensor, while ammonia levels were determined by feeding selected regions of the RF spectrum into a pretrained generalized regression neural network model. Results show the RF sensor is able to directly measure the instantaneous ammonia inventory, while simultaneously providing soot loading measurements within 0.5 g/L. These results confirm that simultaneous measurements of both the PM and ammonia loading state of an SCRF are possible using a single RF sensor via analysis of specific features in the full RF spectrum. The results indicate significant potential to remove the control barriers typically associated with the implementation of advanced SCRF systems.

Ragaller, Paul↗

DOE OSTI2020

Measuring Neutrino Oscillations in the NOvA and CHIPS Detectors.

NOvA is a long baseline neutrino experiment which uses muon neutrinos produced by the NuMI beam at the Fermi National Accelerator Laboratory to measure muon neutrino disappearance and electron neutrino appearance, among other analyses. The Far/Near Extrapolation analysis framework (FNEX) was used to measure muon neutrino disappearance using the events observed by NOvA while the NuMI beam was in Forward Horn Current configuration (i.e. this analysis uses neutrino data, not antineutrino data). The values of the parameters measured in this analysis are sin 2 θ 23 - 0.499$^{+0.098}_{-0.069}$ and Δm$^2_{32}$ - 2.454$^{+0.108}_{0.119}$ × 10 -3 eV, which is consistent with the results of NOvA’s main muon neutrino disappearance analysis using the experiment’s usual framework, known as CAF. The CHIPS detector is a water Cherenkov detector currently in construction. It will also use the NuMI beam to perform muon neutrino disappearance and electron neutrino appearance analyses. The necessary water clarity for a detector with a diameter of 25 m and a height of 6 m is discussed, as well as the results of testing water filtration systems. The filtration that will be used for the detector is a 10 µm carbon block filter and a 0.5 µm filter in series, with no reverse osmosis or ultraviolet sterilisation being used. This provides an attenuation length of 16.63 ± 0.25 m for light of 532 nm wavelength (green), so light with a wavelength of 405 nm (violet) would have an attenuation length of 133±2 m. The greatest possible distance between a PMT and any point in the detector’s volume is approximately 26 m, so 133 m is sufficient for the detector to measure Cherenkov light produced anywhere in the detector.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

Durable graphene oxide membranes

Embodiments described herein relate generally to durable graphene oxide membranes for fluid filtration. For example, the graphene oxide membranes can be durable under high temperatures non-neutral pH, and/or high pressures. One aspect of the present disclosure relates to a filtration apparatus comprising: a support substrate, and a graphene oxide membrane disposed on the support substrate. The graphene oxide membrane has a first lactose rejection rate of at least 50% with a first 1 wt % lactose solution at room temperature. The graphene oxide membrane has a second lactose rejection rate of at least 50% with a second 1 wt % lactose solution at room temperature after the graphene oxide membrane is contacted with a solution that is at least 80° C. for a period of time.

Frayne, Stephen↗

DOE OSTI2022

Durable graphene oxide membranes

Frayne, Stephen↗

DOE OSTI2012

Near-Tank Treatment of Hanford Tank Waste: Pilot-Scale Testing - 12107

In order to reduce the number of high level waste canisters that will have to be produced by the Hanford Tank Waste Treatment and Immobilization Plant, supplemental waste treatment technologies are being investigated. One such technology is the Near-Tank Treatment System, which uses continuous sludge leaching, filtration, and ion exchange to process the waste in a simple, compact system. The Near Tank Treatment System is ideally suited for handling Hanford tanks with large amounts of boehmite, a difficult aluminum phase to dissolve. A pilot-scale Near Tank Treatment System was constructed and tested with a boehmite and iron oxyhydroxide waste simulant to evaluate the robustness and effectiveness of the system. The data from the pilot-scale tests were also used to assess scale-up from previously performed bench-scale tests. It should be noted that any work involving the use of simulated HLW has inherent limitations. For this work, every attempt was made to ensure that the simulant mimicked the actual waste performance as closely as possible. However, there are always limitations in the ability to The NTTS Demonstration Test established that all the subsystems could be operated concurrently to process the waste simulant. The NTTS had a stable performance during the Demonstration Test that required very little external manipulation once a steady state was achieved. The CSL demonstrated effectively 90% dissolution of the hard to leach boehmite phase. The cross flow filtration system was able to deliver decontaminated salt solution to the NTCR system. The NTCR system exceeded the design basis by providing effluent below the detection limit beyond the design basis required time. The NTTS system was successfully demonstrated and has shown that leaching and decontamination of the subsequent permeate can be readily achieved using relatively small footprint equipment in an at tank application. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

DOE OSTI2012

Sorption Behavior of Eu(III) into CSH Gel in Imitated Saline Groundwater - 12145

The sorption behavior of Eu(III) (europium (III)) into CSH (Calcium Silicate Hydrate) gel without dried processes was examined in imitated saline groundwater by using the spectro-fluorometer, Raman spectrophotometer and ICP-AES (Inductively Coupled Plasma- Atomic Emission Spectrometry). Ca/Si ratio was set to 0.4, 0.8, 1.2 and 1.6, and NaCl concentration was also set to 0.6, 0.06 and 0.006. The synthesis of each sample was conducted in a glove box saturated with nitrogen gas. The sealed sample tubes were gently shaken with 120 strokes/min. The time-period to contact Eu(III) with the CSH gel was set to 60 days. The fluorescence emission spectra suggested the incorporation of Eu{sup 3+} into CSH gel in the high Ca/Si ratio samples. On the other hand, from the decay behavior of fluorescence emission spectra, even in the low Ca/Si ratio samples, sorption behavior of Eu{sup 3+} into CSH gel was confirmed. Besides, the Raman spectra showed that the degree of polymerization of Si-O in CSH gel was raised with increasing Na ions concentration. These results suggest that the CSH gel, formed as secondary mineral, would retard the migration of radionuclides even in saline groundwater. Considering the inflow of saline groundwater into repository, this study examined the interaction between CSH gel (without dry processes) and Eu{sup 3+} by using the fluorescence emission spectra, the decay behavior of fluorescence and the Raman spectra. As a result, the fluorescence emission spectra of the sample of more than 0.8 Ca/Si ratio confirmed the intensity split into two peaks around 618 nm (5D0→7F2 transition). Furthermore, even in relatively low Ca/Si ratio samples, the fluorescence lifetimes both of the surface sorption sample and the co-precipitated samples exceeded that of the filtrate sample. These suggested that Eu{sup 3+} is not only hydrolyzed to form Eu(OH){sub 3} colloid, but is also stably incorporated into CSH gel (in Ca/Si ratio>1.2) or is forming complex on the surface of solid phase (in Ca/Si<0.8) in the co-presence of Na ions. On the other hand, the concentrations of Na, Ca and Si after 60 days in the solution filtrated through 0.2 μm membrane filter showed the ion exchange of Ca and Eu apparently in the samples of low Ca/Si ratio. Besides, in the samples with high Ca/Si ratio, Ca and Si concentrations in the solution were raised with increment of initial Na concentration. While Na ions may slightly increase the solubility of CSH gel, the CSH samples were stable, mostly maintaining the initial Ca/Si ratio synthesized. Moreover, the Raman spectra showed that the degree of polymerization of silicate chain in CSH samples increased with increasing Na concentration. Such an immobilized Na into the structure of CSH gel did not obstruct the incorporation of Eu{sup 3+} into CSH gel. The results mentioned above suggested that CSH gel (formed as a secondary mineral around the repository) also can retard the migration of radionuclides even if the repository and its surrounding are saturated by saline groundwater. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗