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NASA NTRS2016

TES-Based X-Ray Microcalorimeter Performances Under AC Bias and FDM for Athena

Athena is a European X-ray observatory, scheduled for launch in 2028. Athena will employ a high-resolution imaging spectrometer called X-ray integral field unit (X-IFU), consisting of an array of 4000 transition edge sensor (TES) microcalorimeter pixels. For the readout of X-IFU, we are developing frequency domain multiplexing, which is the baseline readout system. In this paper, we report on the performance of a TES X-ray calorimeter array fabricated at Goddard Space Flight Center (GSFC) at MHz frequencies for the baseline of X-IFU detector. During single-pixel AC bias characterization, we measured X-ray energy resolutions (at 6 keV) of about 2.9 eV at both 2.3 and 3.7 MHz. Furthermore, in the multiplexing mode, we measured X-ray energy resolutions of about 2.9 eV at 1.3 and 1.7 MHz.

Transition edge sensors X-ray microcalorimeter Fre↗

NASA NTRS2016

Laboratory Measurements of the K-Shell Transition Energies in L-Shell Ions of Si and S

We have measured the energies of the strongest 1s-2 ℓ (azimuthal quantum number) (ℓ = s, p (s, p are angular momentum states)) transitions in He- through Ne-like silicon and sulfur ions to an accuracy of less than 1 electronvolt using the Lawrence Livermore National Laboratory's electron beam ion traps, EBIT-I and SuperEBIT, and the NASA/GSFC EBIT Calorimeter Spectrometer (ECS). We identify and measure the energies of 18 and 21 X-ray features from silicon and sulfur, respectively. The results are compared to new Flexible Atomic Code calculations and to semi-relativistic Hartree-Fock calculations by Palmeri et al. (2008). These results will be especially useful for wind diagnostics in high-mass X-ray binaries, such as Vela X-1 and Cygnus X-1, where high-resolution spectral measurements using Chandraʼs high-energy transmission grating has made it possible to measure Doppler shifts of 100 kilometers per second. The accuracy of our measurements is consistent with that needed to analyze Chandra observations, exceeding Chandraʼs 100 kilometers per second limit. Hence, the results presented here not only provide benchmarks for theory, but also accurate rest energies that can be used to determine the bulk motion of material in astrophysical sources. We show the usefulness of our results by applying them to redetermine Doppler shifts from Chandra observations of Vela X-1.

atomic data↗

NASA NTRS2017

Test and Analysis of Solid Rocket Motor Nozzle Ablative Materials

Asbestos free solid motor internal insulation samples were tested at the MSFC Hyperthermal Facility. Objectives of the test were to gather data for analog characterization of ablative and in-depth thermal performance of rubber materials subject to high enthalpy/pressure flow conditions. Tests were conducted over a range of convective heat fluxes for both inert and chemically reactive sub-sonic free stream gas flow. Instrumentation included use of total calorimeters, thermocouples, and a surface pyrometer for surface temperature measurement. Post-test sample forensics involved measurement of eroded depth, charred depth, total sample weight loss, and documentation of the general condition of the eroded profile. A complete Charring Material Ablator (CMA) style aero-thermal analysis was conducted for the test matrix and results compared to the measured data. In general, comparisons were possible for a number of the cases and the results show a limited predictive ability to model accurately both the ablative response and the in-depth temperature profiles. Lessons learned and modeling recommendations are made regarding future testing and modeling improvements that will increase understanding of the basic chemistry/physics associated with the complicated material ablation process of rubber materials.

Clayton, J. Louie↗

NASA NTRS2017

Arc Jet Test and Analysis of Asbestos Free Solid Rocket Motor Nozzle Dome Ablative Materials

Asbestos free solid motor internal insulation samples were recently tested at the MSFC Hyperthermal Arc Jet Facility. Objectives of the test were to gather data for solid rocket motor analog characterization of ablative and in-depth thermal performance of rubber materials subject to high enthalpy/pressure flow conditions. Tests were conducted over a range of convective heat fluxes for both inert and chemically reactive sub-sonic free stream gas flow. Active instrumentation included use of total calorimeters, in-depth thermocouples, and a surface pyrometer for in-situ surface temperature measurement. Post-test sample forensics involved determination of eroded depth, charred depth, total sample weight loss, and documentation of the general condition of the eroded profile. A complete Charring Material Ablator (CMA) style aero thermal analysis was conducted for the test matrix and results compared to the measured data. In general, comparisons were possible for a number of the cases and the results show a limited predictive ability to model accurately both the ablative response and the in-depth temperature profiles. Lessons learned and modeling recommendations are made regarding future testing and modeling improvements that will increase understanding of the basic chemistry/physics associated with the complicated material ablation process of rubber materials.

Clayton, J. Louie↗

NASA NTRS2016

Development of X-Ray Microcalorimeter Imaging Spectrometers for the X-Ray Surveyor Mission Concept

Four astrophysics missions are currently being studied by NASA as candidate large missions to be chosen inthe 2020 astrophysics decadal survey.1 One of these missions is the X-Ray Surveyor (XRS), and possibleconfigurations of this mission are currently under study by a science and technology definition team (STDT). Oneof the key instruments under study is an X-ray microcalorimeter, and the requirements for such an instrument arecurrently under discussion. In this paper we review some different detector options that exist for this instrument,and discuss what array formats might be possible. We have developed one design option that utilizes eithertransition-edge sensor (TES) or magnetically coupled calorimeters (MCC) in pixel array-sizes approaching 100kilo-pixels. To reduce the number of sensors read out to a plausible scale, we have assumed detector geometriesin which a thermal sensor such a TES or MCC can read out a sub-array of 20-25 individual 1 pixels. In thispaper we describe the development status of these detectors, and also discuss the different options that exist forreading out the very large number of pixels.

multiplexing↗

NASA NTRS2016

Dios: The Dark Baryon Exploring Mission

DIOS (Diffuse Intergalactic Oxygen Surveyor) is a small satellite aiming for a launch around 2022 with JAXA's Epsilon rocket. Its main aim is a search for warm-hot intergalactic medium with high-resolution X-ray spectroscopy of redshifted emission lines from OVII and OVIII ions. The superior energy resolution of TES microcalorimeters combined with a wide field of view (30 diameter) will enable us to look into gas dynamics of cosmic plasmas in a wide range of spatial scales from Earths magnetosphere to unvirialized regions of clusters of galaxies. Mechanical and thermal design of the spacecraft and development of the TES calorimeter system are described. Employing an enlarged X-ray telescope with a focal length of 1.2 m and fast repointing capability, DIOS can observe absorption features from X-ray afterglows of distant gamma-ray bursts.

X-ray telescope↗

NASA NTRS2016

Characterization of an Atomic Hydrogen Source for Charge Exchange Experiments

We characterized the dissociation fraction of a thermal dissociation atomic hydrogen source byinjecting the mixed atomic and molecular output of the source into an electron beam ion trapcontaining highly charged ions and recording the x-ray spectrum generated by charge exchangeusing a high-resolution x-ray calorimeter spectrometer. We exploit the fact that the charge exchangestate-selective capture cross sections are very different for atomic and molecular hydrogen incidenton the same ions, enabling a clear spectroscopic diagnostic of the neutral species.

issociationX-ray spectrometersX-ray spectraMolecul↗

NASA NTRS2016

First Peek of ASTRO-H Soft X-Ray Telescope (SXT) In-Orbit Performance

ASTRO-H (Hitomi) is a Japanese X-ray astrophysics satellite just launched in February, 2016, from Tanegashima, Japan by a JAXA's H-IIA launch vehicle. It has two Soft X-ray Telescopes (SXTs), among other instruments, that were developed by the NASA Goddard Space Flight Center in collaboration with ISAS/JAXA and Nagoya University. One is for an X-ray micro-calorimeter instrument (Soft X-ray Spectrometer, SXS) and the other for an X-ray CCD camera (Soft X-ray Imager, SXI), both covering the X-ray energy band up to 15 keV. The two SXTs were fully characterized at the 30-m X-ray beam line at ISAS/JAXA. The combined SXT+SXS system effective area is about 250 and 300 cm(exp 2) at 1 and 6 keV, respectively, although observations were performed with the gate valve at the dewar entrance closed, which blocks most of low energy X-rays and some of high energy ones. The angular resolution for SXS is 1.2 arcmin (Half Power Diameter, HPD). The combined SXT+SXI system effective area is about 370 and 350 cm (exp 2) at 1 and 6 keV, respectively. The angular resolution for SXI is 1.3 arcmin (HPD). The both SXTs have a field of view of about 16 arcmin (FWHM of their vignetting functions).The SXT+SXS field of view is limited to 3 x 3 arcmin by the SXS array size. In-flight data available to the SXT team was limited at the time of this conference and a point-like source data is not available for the SXT+SXS. Although due to lack of attitude information we were unable to reconstruct a point spread function of SXT+SXI, according to RXJ1856.5-3754 data, the SXT seems to be working as expected in terms of imaging capability. As for the overall effective area response for both SXT+SXS and SXT+SXI, consistent spectral model fitting parameters with the previous measurements were obtained for Crab and G21.5-0.9 data. On the other hand, their 2-10 keV fluxes differ by about 20% at this point. Calibration work is still under progress. The SXT is the latest version of the aluminum foil X-ray mirror, which is extremely light-weight and very low cost, yet produces large effective area over a wide energy-band. Its area-mass ratio is the largest, 16 cm(exp 2)/kg, among ASTRO-H, Chandra, and XMM-Newton mirrors. The aluminum foil mirror is a still compelling technology depending on the mission science goal.

X-rays↗

NASA NTRS2016

The ASTRO-H SXT Performance to the Large Off-Set Angles

The X-ray astronomy satellite ASTRO-H, which is the 6th Japanese X-ray astronomy satellite and is renamed Hitomi after launch, is designed to observe celestial X-ray objects in a wide energy band from a few hundred eV to 600 keV. The Soft X-ray Telescopes (SXTs) onboard ASTRO-H play a role of collecting and imaging X-rays up to approximately 12 keV. Although the field of view of the SXT is approximately 15' (FWHM), due to the thin-foil-nested Wolter-I type optics adopted in the SXTs, X-rays out of the field of view can reach the focal plane without experiencing a normal double reflection. This component is referred to as 'stray light'. Owing to investigation of the stray light so far, 'secondary reflection' is now identified as the main component of the stray light, which is composed of X-rays reflected only by secondary reflectors. In order to cut the secondary reflections, a 'pre-collimator' is equipped on top of the SXTs. However, we cannot cut all the stray lights with the pre-collimator in some off-axis angle domain. In this study, we measure the brightness of the stray light of the SXTs at some representative off-axis angles by using the ISAS X-ray beam line. ASTRO-H is equipped with two modules of the SXT; one is for the Soft X-ray Spectrometer (SXS), an X-ray calorimeter, and the other is for the Soft X-ray Imager (SXI), an X-ray CCD camera. These SXT modules are called SXT-S and SXT-I, respectively. Of the two detector systems, the SXI has a large field of view, a square with 38' on a side. To cope with this, we have made a mosaic mapping of the stray light at a representative off-axis angle of 30' in the X-ray beam line at the Institute of Space and Astronautical Science. The effective area of the brightest secondary reflection is found of order approximately 0.1% of the on-axis effective area at the energy of 1.49 keV. The other components are not so bright (less than 5 x 10(exp -4) times smaller than the on-axis effective area). On the other hand, we have found that the effective area of the stray light in the SXS field of view (approximately 3' x 3') at large off-axis angles (greater than 15') are approximately 1(exp -4) times smaller than the on-axis effective area (approximately 590 sq cm at 1.49 keV).

X-rays↗

NASA NTRS2016

In-Flight Performance of the Soft X-Ray Spectrometer Detector System on ASTRO-H

The SXS instrument was launched aboard the Astro-H observatory on February 17, 2016. The SXS spectrometer is based on a high sensitivity x-ray calorimeter detector system that has been successfully deployed in many ground and sub-orbital spectrometers. The instrument was to provide essential diagnostics for nearly every class of x-ray emitting objects from the atmosphere of Jupiter to the outskirts of galaxy clusters, without degradation for spatially extended objects. The SXS detector system consisted of a 36-pixel cryogenic microcalorimeter array operated at a heat sink temperature of 50 mK. In pre-flight testing, the detector system demonstrated a resolving power of better than 1300 at 6 keV with a simultaneous band-pass from below 0.3 keV to above 12 keV with a timing precision better than 100 microsecond. In addition, a solid-state anti-coincidence detector was placed directly behind the detector array for background suppression. The detector error budget included the measured interference from the SXS cooling system and the spacecraft. Additional margin for on-orbit gain-stability, and on-orbit spacecraft interference were also included predicting an on-orbit performance that meets or exceeds the 7 eV FWHM at 6 keV requirement. The actual on-orbit spectral resolution was better than 5 eV FWHM at 6 keV, easily satisfying the instrument requirement. Here we discuss the actual on-orbit performance of the SXS detector system and compare this to performance in pre-flight testing and the on-orbit predictions. We will also discuss the on-orbit gain stability, additional on-orbit interference, and measurements of the on-orbit background.

X-ray astrophysics↗

NASA NTRS2016

Vibration Isolation System for Cryocoolers of Soft X-Ray Spectrometer (SXS) Onboard ASTRO-H (Hitomi)

Soft X-ray Spectrometer (SXS) onboard ASTRO-H (named Hitomi after launch) is a micro-calorimeter-type spectrometer, installed in a dewar to be cooled at 50 mK. The energy resolution of the SXS engineering model suffered from micro-vibration from cryocoolers mounted on the dewar. This is mitigated for the flight model by introducing vibration isolation systems between the cryocoolers and the dewar. The detector performance of the flight model was verified before launch of the spacecraft in both ambient condition and thermal-vac condition, showing no detectable degradation in energy resolution. The in-orbit performance was also consistent with that on ground, indicating that the cryocoolers were not damaged by launch environment. The design and performance of the vibration isolation system along with the mechanism of how the micro-vibration could degrade the cryogenic detector is shown.

Microcalorimeter↗

NASA NTRS2017

Design and Optimization of Multi-Pixel Transition-Edge Sensors for X-Ray Astronomy Applications

Multi-pixel transition-edge sensors (TESs), commonly referred to as 'hydras', are a type of position sensitive micro-calorimeter that enables very large format arrays to be designed without commensurate increase in the number of readout channels and associated wiring. In the hydra design, a single TES is coupled to discrete absorbers via varied thermal links. The links act as low pass thermal filters that are tuned to give a different characteristic pulse shape for x-ray photons absorbed in each of the hydra sub pixels. In this contribution we report on the experimental results from hydras consisting of up to 20 pixels per TES. We discuss the design trade-offs between energy resolution, position discrimination and number of pixels and investigate future design optimizations specifically targeted at meeting the readout technology considered for Lynx.

Smith, Stephen J.↗

NASA NTRS2017

Heat Loads Due to Small Penetrations in Multilayer Insulation Blankets

The main penetrations (supports and piping) through multilayer insulation systems for cryogenic tanks have been previously addressed by heat flow measurements. Smaller penetrations due to fasteners and attachments are now experimentally investigated. The use of small pins or plastic garment tag fasteners to each the handling and construction of multilayer insulation (MLI) blankets goes back many years. While it has long been understood that penetrations and other discontinuities degrade the performance of the MLI blanket, quantification of this degradation has generally been lumped into gross performance multipliers (often called degradation factors or scale factors). Small penetrations contribute both solid conduction and radiation heat transfer paths through the blanket. The conduction is down the stem of the structural element itself while the radiation is through the hole formed during installation of the pin or fastener. Analytical models were developed in conjunction with MLI perforation theory and Fouriers Law. Results of the analytical models are compared to experimental testing performed on a 10 layer MLI blanket with approximately 50 small plastic pins penetrating the test specimen. The pins were installed at 76-mm spacing inches in both directions to minimize the compounding of thermal effects due to localized compression or lateral heat transfer. The testing was performed using a liquid nitrogen boil-off calorimeter (Cryostat-100) with the standard boundary temperatures of 293 K and 78 K. Results show that the added radiation through the holes is much more significant than the conduction down the fastener. The results are shown to be in agreement with radiation theory for perforated films.

Structural attachments↗

NASA NTRS2016

Examining the Angular Resolution of the Astro-H's Soft X-Ray Telescopes

The international x-ray observatory ASTRO-H was renamed Hitomi after launch. It covers a wide energy range from a few hundred eV to 600 keV. It is equipped with two soft x-ray telescopes (SXTs: SXT-I and SXT-S) for imaging the soft x-ray sky up to 12 keV, which focus an image onto the respective focal-plane detectors: CCD camera (SXI) and a calorimeter (SXS). The SXTs are fabricated in a quadrant unit. The angular resolution in half-power diameter (HPD) of each quadrant of the SXTs ranges between 1.1 and 1.4 arc min at 4.51 keV. It was also found that one quadrant has an energy dependence on the HPD. We examine the angular resolution with spot scan measurements. In order to understand the cause of imaging capability deterioration and to reflect it to the future telescope development, we carried out spot scan measurements, in which we illuminate all over the aperture of each quadrant with a square beam 8 mm on a side. Based on the scan results, we made maps of image blurring and a focus position. The former and the latter reflect figure error and positioning error, respectively, of the foils that are within the incident 8 mm x 8 mm beam. As a result, we estimated those errors in a quadrant to be approx. 0.9 to 1.0 and approx. 0.6 to 0.9 arc min, respectively. We found that the larger the positioning error in a quadrant is, the larger its HPD is. The HPD map, which manifests the local image blurring, is very similar from quadrant to quadrant, but the map of the focus position is different from location to location in each telescope. It is also found that the difference in local performance causes energy dependence of the HPD.

Astro-H/Hitomi; soft x-ray telescope; SXT; Wolter ↗

NASA NTRS2016

Flow Characterization Studies of the 10-MW TP3 Arc-Jet Facility: Probe Sweeps

This paper reports computational simulations and analysis in support of calibration and flow characterization tests in a high enthalpy arc-jet facility at NASA Ames Research Center. These tests were conducted in the NASA Ames 10-MW TP3 facility using flat-faced stagnation calorimeters at six conditions corresponding to the steps of a simulated flight heating profile. Data were obtained using a conical nozzle test configuration in which the models were placed in a free jet downstream of the nozzle. Experimental surveys of arc-jet test flow with pitot pressure and heat flux probes were also performed at these arc-heater conditions, providing assessment of the flow uniformity and valuable data for the flow characterization. Two different sets of pitot pressure and heat probes were used: 9.1-mm sphere-cone probes (nose radius of 4.57 mm or 0.18 in) with null-point heat flux gages, and 15.9-mm (0.625 in) diameter hemisphere probes with Gardon gages. The probe survey data clearly show that the test flow in the TP3 facility is not uniform at most conditions (not even axisymmetric at some conditions), and the extent of non-uniformity is highly dependent on various arc-jet parameters such as arc current, mass flow rate, and the amount of cold-gas injection at the arc-heater plenum. The present analysis comprises computational fluid dynamics simulations of the nonequilibrium flowfield in the facility nozzle and test box, including the models tested. Comparisons of computations with the experimental measurements show reasonably good agreement except at the extreme low pressure conditions of the facility envelope.

Goekcen, Tahir↗

NASA NTRS2018

Combining Fractional Calorimetry with Statistical Methods to Characterize Thermal Runaway

Thermal management systems designed to handle the impacts of thermal runaway (TR) are key to safe operation of lithium-ion (Li-ion) batteries. Critical factors for optimizing these systems include the total energy released and the fraction of the total energy that is released through the cell casing versus through the ejecta material. A unique calorimeter, designed to characterize said factors, was utilized to examine the TR behavior of a variety of 18650-format Li-ion cells. Statistical methods were implemented to interpret the data.

Walker, William↗

NASA NTRS2016

Flow Characterization Studies of the 10-MW TP3 Arc-Jet Facility: Probe Sweeps

CFD↗

NASA NTRS2018

Coupling Fractional Thermal Runaway Calorimetry (FTRC) Results with Statistical Analysis Methods

Important factors to consider when optimizing Lithium-ion (Li-ion) battery thermal management systems, from a battery safety perspective, include the total energy released during a single cell thermal runaway (TR) event and the fraction of the total energy that is released through the cell casing versus through the ejecta material. A fractional thermal runaway calorimeter (FTRC) was used to examine the TR behavior of the following 18650-format Li-ion cells: (1) Molicel 18650-J, (2) LG 18650-HG2, (3) Samsung 18650-30Q, (4) 3.35 Ah LG 18650 test cell, (5) Sony 18650-VC7, and (6) LG 18650-MJ1. These cells were intentionally selected to represent a variety of manufacturers, chemistries, capacities, and safety features. Because of the large number of random and non-random variables associated with the FTRC results, a linear regression model, developed using engineering statistical methods, was utilized to provide final interpretation of the TR behavior for each cell type and design variable combination.

Walker, William↗