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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 559 records · Page 31
All sourcesNASA NTRSDOE OSTI
DOE OSTI2024

Spatiotemporally Registered In-Situ and Ex-Situ Datasets for Laser-based Blown Powder Directed Energy Deposition

This dataset is comprised of in situ sensing data collected during laser-based, blown powder directed energy deposition (DED) of Inconel 718 representing eight different printing conditions: (1) nominal, (2) +15% scan speed, (3) +12% laser power, (4) +42% powder feed rate, (5) +100% jerk limit, (6) +10% layer height, (7) +20% hatch spacing, (8) +20% carrier gas flow. All eight DED builds constructed an identical test coupon geometry consisting of geometric features representative of industrial print requirements (e.g., bulk deposition, thin walls, overhangs). In situ data consists of xyz-coordinates (100 Hz) and on-axis melt pool camera video (60 Hz), both of which have been temporally synchronized to spatially map the melt pool camera data. In addition, post-build X-ray computed tomography (XCT) data for each of the eight test geometries have been spatially registered to the recorded xyz-coordinates, allowing for comparisons between melt pool camera data and flaws identified in the XCT data.

additive manufacturing↗
DOE OSTI2020

Application and Certification of Comparative Vacuum Monitoring Sensors for Structural Health Monitoring of 737 Wing Box Fittings

Multi-site fatigue damage, hidden cracks in hard-to-reach locations, disbonded joints, erosion, impact, and corrosion are among the major flaws encountered in today's extensive fleet of aging aircraft and space vehicles. The use of in-situ sensors for real-time health monitoring of aircraft structures are a viable option to overcome inspection impediments stemming from accessibility limitations, complex geometries, and the location and depth of hidden damage. Reliable, structural health monitoring systems can automatically process data, assess structural condition, and signal the need for human intervention. Prevention of unexpected flaw growth and structural failure can be improved if on-board health monitoring systems are used to continuously assess structural integrity. Such systems are able to detect incipient damage before catastrophic failures occurs. Condition-based maintenance practices could be substituted for the current time-based maintenance approach. Other advantages of on-board distributed sensor systems are that they can eliminate costly, and potentially damaging, disassembly, improve sensitivity by producing optimum placement of sensors and decrease maintenance costs by eliminating more time- consuming manual inspections. This report presents a Sandia Labs-aviation industry effort to move SHM into routine use for aircraft maintenance. This program addressed formal SHM technology validation and certification issues so that the full spectrum of concerns, including design, deployment, performance and certification were appropriately considered. The Airworthiness Assurance NDI Validation Center (AANC) at Sandia Labs, in conjunction with Boeing, Delta Air Lines, Structural Monitoring Systems Ltd., Anodyne Electronics Manufacturing Corp. and the Federal Aviation Administration (FAA) carried out a certification program to formally introduce Comparative Vacuum Monitoring (CVM) as a structural health monitoring solution to a specific aircraft wing box application. Validation tasks were designed to address the SHM equipment, the health monitoring task, the resolution required, the sensor interrogation procedures, the conditions under which the monitoring will occur, the potential inspector population, adoption of CVM into an airline maintenance program and the document revisions necessary to allow for routine use of CVM as an alternate means of performing periodic structural inspects. To carry out the validation process, knowledge of aircraft maintenance practices was coupled with an unbiased, independent evaluation. Sandia Labs designed, implemented, and analyzed the results from a focused and statistically-relevant experimental effort to quantify the reliability of the CVM system applied to the Boeing 737 Wing Box fitting application. All factors that affect SHM sensitivity were included in this program: flaw size, shape, orientation and location relative to the sensors, as well as operational and environmental variables. Statistical methods were applied to performance data to derive Probability of Detection (POD) values for CVM sensors in a manner that agrees with current nondestructive inspection (NDI) validation requirements and also is acceptable to both the aviation industry and regulatory bodies. This report presents the use of several different statistical methods, some of them adapted from NDI performance assessments and some proposed to address the unique nature of damage detection via SHM systems, and discusses how they can converge to produce a confident quantification of SHM performance An important element in developing SHM validation processes is a clear understanding of the regulatory measures needed to adopt SHM solutions along with the knowledge of the structural and maintenance characteristics that may impact the operational performance of an SHM system. This report describes the major elements of an SHM validation approach and differentiates the SHM elements from those found in NDI validation. The activities conducted in this program demonstrated the feasibility of routine SHM usage in general and CVM in particular for the application selected. They also helped establish an optimum OEM-airline-regulator process and determined how to safely adopt SHM solutions. This formal SHM validation will allow aircraft manufacturers and airlines to confidently make informed decisions about the proper utilization of CVM technology. It will also streamline the regulatory actions and formal certification measures needed to assure the safe application of SHM solutions.

42 ENGINEERING↗
DOE OSTI2021

An Analysis of Shallow Orographic Cumulus Clouds Observed During the CACTI Field Campaign: A SULI Internship Final Report

In 2018, the Atmospheric Radiation Measurement Aerial Facility (AAF) deployed its G-1 research aircraft to the Sierras de Córdoba mountain range in north-central Argentina to support the research of environmental factors on deep convective cycles as part of the Cloud, Aerosol, and Complex Terrain Interactions (CACTI) field campaign. The aircraft was fitted with a suite of instruments to holistically measure in situ the current state of the atmosphere. In this study, we organize the campaign’s 22 flights by environmental conditions. Data from each flight was transected by the aircraft’s position relative to cloud, allowing for in depth analysis of cloud processing on aerosol populations. My project was a case study of selected flights where warm, shallow orographic cumulus clouds were observed.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2023

Quantifying neptunium oxidation states in nitric acid through spectroelectrochemistry and chemometrics

Controlled-potential in situ thin-layer spectropotentiometry was leveraged to generate visible/near-infrared (VIS/NIR) absorption spectral data sets for the development of chemometric models to quantify Np(III/IV/V/VI) oxidation states in HNO 3 . This technology would be valuable in laboratory studies and when monitoring process solutions to guide feed adjustments for radiochemical separations—the performance of which depends on oxidation state. This approach successfully isolated and stabilized Np species in pure (~99%) oxidation states without compromising solution optical properties. Multivariate curve resolution–alternating least squares models were evaluated to resolve spectral and component concentrations from a scan that sequentially produced Np(VI), Np(V), Np(IV), and Np(III) spectra with mixtures of two valences at a time. Although it provided a useful approximation, the method was not able to quantitively resolve each component likely because of rotational ambiguity. Additionally, partial least squares regression models were built from artificial and electrochemically generated VIS/NIR spectral training sets to study the effect of interionic interactions on spectral characteristics. Models built with true Bi-chemical mixtures of coexisting Np oxidation states and spectra generated from additive combinations of pure end points had similar prediction performance. This methodology can be used to directly quantify Np concentration and the ratio of Np oxidation states and other actinides in remote settings such as hot cells.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2021

New Insights Into Lignification via Network and Multi-Omics Analyses of Arogenate Dehydratase Knock-Out Mutants in Arabidopsis thaliana

Multiple Arabidopsis arogenate dehydratase (ADT) knock-out (KO) mutants, with phenotypes having variable lignin levels (up to circa 70% reduction), were studied to investigate how differential reductions in ADTs perturb its overall plant systems biology. Integrated "omics" analyses (metabolome, transcriptome, and proteome) of wild type (WT), single and multiple ADT KO lines were conducted. Transcriptome and proteome data were collapsed into gene ortholog (GO) data, with this allowing for enzymatic reaction and metabolome cross-comparisons to uncover dominant or likely metabolic biosynthesis reactions affected. Network analysis of enzymes-highly correlated to stem lignin levels-deduced the involvement of novel putative lignin related proteins or processes. These included those associated with ribosomes, the spliceosome, mRNA transport, aminoacyl tRNA biosynthesis, and phosphorylation. While prior work helped explain lignin biosynthesis regulation at the transcriptional level, our data here provide support for a new hypothesis that there are additional post-transcriptional and translational level processes that need to be considered. These findings are anticipated to lead to development of more accurate depictions of lignin/phenylpropanoid biosynthesis models in situ, with new protein targets identified for further biochemical analysis and/or plant bioengineering. Additionally, using KEGG defined functional categorization of proteomics and transcriptomics analyses, we detected significant changes to glucosinolate, a-linolenic acid, nitrogen, carotenoid, aromatic amino acid, phenylpropanoid, and photosynthesis-related metabolic pathways in ADT KO mutants. Metabolomics results also revealed that putative carotenoid and galactolipid levels were generally increased in amount, whereas many glucosinolates and phenylpropanoids (including flavonoids and lignans) were decreased in the KO mutants.

Arabidopsis, arogenate dehydratases, lignin, multi↗
NASA NTRS1984

Evaluation of airborne lidar wind measurements

The verification of the Doppler lidar wind measurement is continued. The in situ measurements on a 500 meter tall tower are used to check the lidar determined winds (flight 4), followed by other tests applied to the extensive data sets of flights 19 and 21. After checking for possible software errors in the processing programs, the inconsistency was not solved. The source of the errors appears to be the uncertainty in the calculation of the contribution of the aircraft motion to the lidar measured line of sight speed. Possible techniques for estimating the aircraft motion errors from the aircraft data are investigated.

Carroll, J. J.↗
NASA NTRS2001

Microphysics, Meteorology, Microwave and Modeling of Mediterranean Storms: The M(sup 5) Problem

Comprehensive understanding of the microphysical nature of Mediterranean storms requires a combination of in situ meteorological data analysis and radar-passive microwave data analysis, effectively integrated with numerical modeling studies at various scales, particularly from synoptic scale down to mesoscale. The microphysical properties of and their controls on severe storms are intrinsically related to meteorological processes under which storms have evolved, processes which eventually select and control the dominant microphysical properties themselves. Insofar as hazardous Mediterranean storms, highlighted by the September 25-28/1992 Genova flood event, the October 5-7/1998 Friuli flood event, and the October 13-15/2000 Piemonte flood event (all taking place in northern Italy), developing a comprehensive microphysical interpretation requires an understanding of the multiple phases of storm evolution and the heterogeneous nature of precipitation fields within the storm domains. This involves convective development, stratiform transition and decay, orographic lifting, and sloped frontal lifting proc esses. This also involves vertical motions and thermodynamical instabilities governing physical processes that determine details of the liquid/ice water contents, size distributions, and fall rates of the various modes of hydrometeors found within the storm environments. This paper presents detailed 4-dimensional analyses of the microphysical elements of the three severe Mediterranean storms identified above, investigated with the aid of SSM/I and TRMM satellite measurements (and other remote sensing measurements). The analyses are guided by nonhydrostatic mesoscale model simulations at high resolution of the intense rain producing portions of the storm environments. The results emphasize how meteorological controls taking place at the large scale, coupled with localized terrain controls, ultimately determine the most salient features of the bulk microphysical properties of the storms. These results have bearing on precipitation remote sensing from space, and the role of modeling in designing precipitation retrieval algorithms.

Smith, Eric A.↗
NASA NTRS2016

Evaluating Multispectral Snowpack Reflectivity With Changing Snow Correlation Lengths

This study investigates the sensitivity of multispectral reflectivity to changing snow correlation lengths. Matzler's ice-lamellae radiative transfer model was implemented and tested to evaluate the reflectivity of snow correlation lengths at multiple frequencies from the ultraviolet (UV) to the microwave bands. The model reveals that, in the UV to infrared (IR) frequency range, the reflectivity and correlation length are inversely related, whereas reflectivity increases with snow correlation length in the microwave frequency range. The model further shows that the reflectivity behavior can be mainly attributed to scattering rather than absorption for shallow snowpacks. The largest scattering coefficients and reflectivity occur at very small correlation lengths (approximately 10(exp -5 m) for frequencies higher than the IR band. In the microwave range, the largest scattering coefficients are found at millimeter wavelengths. For validation purposes, the ice-lamella model is coupled with a multilayer snow physics model to characterize the reflectivity response of realistic snow hydrological processes. The evolution of the coupled model simulated reflectivities in both the visible and the microwave bands is consistent with satellite-based reflectivity observations in the same frequencies. The model results are also compared with colocated in situ snow correlation length measurements (Cold Land Processes Field Experiment 2002-2003). The analysis and evaluation of model results indicate that the coupled multifrequency radiative transfer and snow hydrology modeling system can be used as a forward operator in a data-assimilation framework to predict the status of snow physical properties, including snow correlation length.

Kang, Do Hyuk↗
NASA NTRS2018

In Situ Thermal Inspection of Automated Fiber Placement Operations for Tow and Ply Defect Detection

The advent of Automated Fiber Placement (AFP) systems have aided the rapid manufacturing of composite aerospace structures. One of the challenges that AFP systems pose is the uniformity of the deposited prepreg tape layers, which complicates detection of laps, gaps, overlaps and twists. The current detection method used in industry involves halting fabrication and performing a time consuming, visual inspection of each tape layer. Typical AFP systems use a quartz lamp to heat the base layer to make the surface tacky as it deposits another tape layer. The innovation proposed in this paper is to use the preheated base layer as a through-transmission heat source for inspecting the newly added tape layer in situ using a thermographic camera mounted on to the AFP hardware. Such a system would not only increase manufacturing throughput by reducing inspection times, but it would also aid in process development for new structural designs or material systems by providing data on as-built parts. To this end, a small thermal camera was mounted onto an AFP robotic research platform at NASA, and thermal data was collected during typical and experimental layup operations. The data was post processed to reveal defects such as tow overlap/gap, wrinkling, and peel-up. Defects that would have been impossible to detect visually were also discovered in the data, such as poor/loss of adhesion between plies and the effects of vacuum debulking. This paper will cover the results of our experiments, and the plans for future versions of this inspection system.

Juarez, Peter D.↗
NASA NTRS2020

Assessment of NO2 Observations During DISCOVER-AQ and KORUS-AQ Field Campaigns

NASA’s Deriving Information on Surface Conditions from Column and Vertically Resolved Observations Relevant to Air Quality (DISCOVER-AQ, conducted in 2011–2014) campaign in the United States and the joint NASA and National Institute of Environmental Research (NIER) Korea–United States Air Quality Study (KORUS-AQ, conducted in 2016) in South Korea were two field study programs that provided comprehensive, integrated data sets of airborne and surface observations of atmospheric constituents, including nitrogen dioxide (NO2), with the goal of improving the interpretation of spaceborne remote sensing data. Various types of NO2 measurements were made, including in situ concentrations and column amounts of NO2 using ground- and aircraft-based instruments, while NO2 column amounts were being derived from the Ozone Monitoring Instrument (OMI) on the Aura satellite. This study takes advantage of these unique datasets by first evaluating in situ data taken from two different instruments on the same aircraft platform, comparing coincidently sampled profile-integrated columns from aircraft spirals with remotely sensed column observations from ground-based Pandora spectrometers, intercomparing column observations from the ground (Pandora), aircraft (in situ vertical spirals), and space (OMI), and evaluating NO2 simulations from coarse Global Modeling Initiative (GMI) and high-resolution regional models. We then use these data to interpret observed discrepancies due to differences in sampling and deficiencies in the data reduction process. Finally, we assess satellite retrieval sensitivity to observed and modeled a priori NO2 profiles. Contemporaneous measurements from two aircraft instruments that likely sample similar air masses generally agree very well but are also found to differ in integrated columns by up to 31.9 %. These show even larger differences with Pandora, reaching up to 53.9 %, potentially due to a combination of strong gradients in NO2 fields that could be missed by aircraft spirals and errors in the Pandora retrievals. OMI NO2 values are about a actor of 2 lower in these highly polluted environments due in part to inaccurate retrieval assumptions (e.g., a priori pro-files) but mostly to OMI’s large footprint (>312 km2).

Nitrogen dioxide↗
NASA NTRSDate not supplied

Improving “Domain-Relevant Metadata Requirements” for Supporting Open-Source Science Initiative

Implementation of the NASA Open-Source Science Initiative (OSSI) requires sharing of all relevant information to ensure “open reproducible science” [1]. However, there are several challenges in applying the OSSI to airborne field campaigns focused on atmospheric composition, which often involve a wide variety of in-situ measurements for trace gases, aerosol and cloud properties, meteorological parameters, and radiation fields. To ensure open reproducibility from airborne field campaigns, it is essential to obtain detailed measurement descriptions, which include the detection principle, sample procedure and treatment, and data processing and correction method. The challenge is that some information, e.g., sampling procedure and treatment, may be instrument-specific and campaign or platform-dependent. The data processing may also involve empirical corrections which may evolve over time. In addition, these details (especially operation- or campaign-specific ones) are often not given in journal publications. Given these issues, there is a need to leverage and improve the current “domain-relevant metadata requirements” to represent the measurement description in standardized metadata. These requirements can then facilitate systematic collection of measurement specific metadata and serve as a foundation to develop tools for making the information accessible and data more interoperable and usable or reusable. Here we show a review of existing metadata collections, use cases, and needs for new standards.

Sean Leavor↗
NASA NTRS2014

Assessing the Ability of Instantaneous Aircraft and Sonde Measurements to Characterize Climatological Means and Long-Term Trends in Tropospheric Composition

Over four decades of measurements exist that sample the 3-D composition of reactive trace gases in the troposphere from approximately weekly ozone sondes, instrumentation on civil aircraft, and individual comprehensive aircraft field campaigns. An obstacle to using these data to evaluate coupled chemistry-climate models (CCMs)the models used to project future changes in atmospheric composition and climateis that exact space-time matching between model fields and observations cannot be done, as CCMs generate their own meteorology. Evaluation typically involves averaging over large spatiotemporal regions, which may not reflect a true average due to limited or biased sampling. This averaging approach generally loses information regarding specific processes. Here we aim to identify where discrete sampling may be indicative of long-term mean conditions, using the GEOS-Chem global chemical-transport model (CTM) driven by the MERRA reanalysis to reflect historical meteorology from 2003 to 2012 at 2o by 2.5o resolution. The model has been sampled at the time and location of every ozone sonde profile available from the Would Ozone and Ultraviolet Radiation Data Centre (WOUDC), along the flight tracks of the IAGOSMOZAICCARABIC civil aircraft campaigns, as well as those from over 20 individual field campaigns performed by NASA, NOAA, DOE, NSF, NERC (UK), and DLR (Germany) during the simulation period. Focusing on ozone, carbon monoxide and reactive nitrogen species, we assess where aggregates of the in situ data are representative of the decadal mean vertical, spatial and temporal distributions that would be appropriate for evaluating CCMs. Next, we identically sample a series of parallel sensitivity simulations in which individual emission sources (e.g., lightning, biogenic VOCs, wildfires, US anthropogenic) have been removed one by one, to assess where and when the aggregated observations may offer constraints on these processes within CCMs. Lastly, we show results of an additional 31-year simulation from 1980-2010 of GEOS-Chem driven by the MACCity emissions inventory and MERRA reanalysis at 4o by 5o. We sample the model at every WOUDC sonde and flight track from MOZAIC and NASA field campaigns to evaluate which aggregate observations are statistically reflective of long-term trends over the period.

Atmospheric composition↗
NASA NTRS2005

Experimental Investigation of Magnesium Powder Combustion With C02 for Mars Ascent Applications

Combustion of metals with CO2 has been identified as a possible propellant for Mars ascent applications. CO2 could be condensed from the Martian atmosphere, reducing the amount of propellant that must be transported from Earth. An attractive feature of this approach compared to other in situ propellant concepts is that no chemical processing on Mars is required. Magnesium has been identified as the most promising metal for this application because it ignites and burns easily in CO2. Preliminary systems studies indicate a 2 to 1 delivered mass advantage for Mg ascent propulsion using in situ C02, as compared to a conventional storable propellant system. The Propulsion Research Center at MSFC is undertaking an experimental investigation of magnesium powder combustion with CO2 in order to provide fundamental data on the combustion performance of Mg powder + CO2 mixtures needed to assess the feasibility of developing a practical Mg powder + CO2 rocket engine. Initial combustion experiments will be carried out in a small scale atmospheric pressure dump combustor. Effects of varying the Mg particle size, firing rate and O/F ratio on combustion stability and efficiency will be investigated. The combustion process will be characterized by optical flame measurements and extraction of combustion product samples. The experimental facility is currently being prepared and combustion experiments will begin during the first quarter of 2005. The final paper will describe the test facility and initial experimental results.

Foote, John P.↗
DOE OSTI2024

Martensite decomposition during rapid heating of Ti-6Al-4V studied via in situ synchrotron X-ray diffraction

Martensite, α‘, commonly appears in Ti-6Al-4V upon rapid cooling from above the β-transus temperature. It is known that α‘ decomposes into α and β at high temperatures but well below the β-transus temperature. Here, we study the decomposition of martensitic Ti-6Al-4V under rapid laser heating, employing in situ synchrotron X-ray diffraction. A comparison is made with post-annealed Ti-6Al-4V under heating to elucidate changes without martensite decomposition. The fast acquisition of X-ray diffraction data at 250 Hz temporally resolves the decomposition process initiated by annihilating dislocations in α‘. The recovery process is accompanied by structural changes in martensite, followed by the phase transformation to β. Thermal profiles estimated from the lattice parameter data reveal the influence of heating rates and dislocation densities on the decomposition process. Throughout the analysis of the diffraction profiles with respect to estimated temperature, we propose a straightforward method for approximating the initiation temperature of martensite decomposition.

42 ENGINEERING↗
DOE OSTI2022

SkX_NN: Neural Network for skyrmion identification in Lorentz TEM

A neural network for segmenting and processing Lorentz TEM images of skyrmion lattices. This software based on U-Net architecture is capable of identifying skyrmions in out-of-focus Lorentz TEM images based on training data. This isspecifically useful for analyzing large area data from in-situ experiments.

PHATAK, CHARUDATTA↗
NASA NTRS1988

In situ measurements of thermospheric composition, temperature, and winds by mass spectrometry

Mass spectrometry, in which a beam of electrons ionizes a sample of atmospheric gas and then analyses the ions thus produced to determine the concentration of each species in the sample, is presently evaluated as a basis for the study of earth atmosphere and other planetary atmospheres' properties. Recent applications of in situ mass spectrometry have measured thermospheric neutral gas composition, temperatures, and winds, with a spatial resolution sufficiently high to reveal previously unsuspected atmospheric variability. It is expected that analyses of these data will lead to a more detailed understanding of the deposition processes governing the thermosphere's highly variable structure.

Spencer, N. W.↗
NASA NTRS1989

Remote sensing and numerical modeling of suspended sediment in Laguna de Terminos, Campeche, Mexico

It is necessary to understand the complex physical processes at work in coastal lagoons in order to manage them effectively. Improved methods of data collection and analysis must be found to provide synoptic, timely hydrodynamic information because of the sheer size of some lagoons and the difficulty of acquiring in situ data (particularly in the tropics). This paper summarizes research to model salinity and suspended sediment distributions in Laguna de Terminos, Mexico, using (1) a coupled hydrodynamic and dispersion model and (2) analysis of two Landsat Thematic Mapper images collected on November 25, 1984 and April 24, 1987. Atmospherically corrected chromaticity data derived from Thermatic Mapper data were significantly correlated with modeled total suspended sediment concentrations for the two dates. Comparison between numerically modeled and remotely sensed suspended sediment maps at 1.5 x 1.5 km resolution yielded a covariation map useful for identifying areas of discrepancy between the remotely sensed data and model output.

Jensen, John R.↗
NASA NTRS1994

The status of measurement technologies concerning micrometer and submicrometer space articulate matter capture, recovery, velocity and trajectory

The return of a pristine sample from a comet would lead to greater understanding of cometary structures, as well as offering insights into exobiology. The paper presented at the Discovery Program Workshop outlined a set of measurements for what was identified as a SOCCER-like interplanetary mission. Several experiments comprised the total instrumentation. This paper presents a summary of CCSR with an overview of three of the four major instruments. Details of the major dust dynamics experiment including trajectory are given in this paper. The instrument proposed here offers the opportunity for the return of cometary dust particles gathered in situ. The capture process has been employed aboard the space shuttle with successful results in returning samples to Earth for laboratory analysis. In addition, the sensors will measure the charge, mass, velocity, and size of cometary dust grains during the encounter. This data will help our understanding of dusty plasmas.

Alexander, W. M.↗