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At least 559 records · Page 31

Preliminary results on the development of vacuum brazed joints for cryogenic wind tunnel aerofoil models

The results of initial experiments show that high-strength void-free bonds can be formed by vacuum brazing of stainless steels using copper and nickel-based filler metals. In Nitronic 40, brazed joints have been formed with strengths in excess of the yield strength of the parent metal, and even at liquid nitrogen temperatures the excellent mechanical properties of the parent metal are only slightly degraded. The poor toughness of 15-5 P.H. stainless steel at cryogenic temperatures is lowered even further by the presence of the brazed bonds investigated. It is highly unlikely that the technique would be used for any critical areas of aerofoil models intended for low-temperature service. Nevertheless, the potential advantages of this simplified method of construction still have attractions for use at ambient temperatures.

Wigley, D. A.↗

Spine Immobilizer for Accident Victims

Proposed conformal bladder filled with tiny spheres called "microballoons," enables spine of accident victim to be rapidly immobilized and restrained and permit victim to be safely removed from accident scene in extremely short time after help arrives. Microballoons expand to form rigid mass when pressure within bladder is less than ambient. Bladder strapped to victim is also strapped to rescue chair. Void between bladder and chair is filled with cloth wedges.

Vykukal, H. C.↗

Laminating Polyimide Films

Thermoplastic polyimide adhesive is used to bond polyimide sheets into flexible laminates. Films are first primed with polyimide adhesive, then bonded together under heat and pressure. Adhesive is cast on separate surface, then sandwiched between polyimide and/or metal films for final assembly. Objectives of process are to improve bonding of high-temperature polyimide film, prepare flexible, large-area, void-free laminates from polyimide film, and laminate polyimide film not only to itself but to metal surfaces.

St. Clair, A. K.↗

Solventless Fabrication of Reinforced Composites

Heat and pressure melt thermoplastic fibers, causing them to flow into voids around graphite reinforcement. On cooling, fiber bundle has been transformed into structural composite. Required temperature and pressure depend on properties of particular thermoplastic used.

Baucom, R. M.↗

Glass shell manufacturing in space

Highly-uniform, hollow glass spheres (shells), which are used for inertial confinement fusion targets, were formed from metal-organic gel powder feedstock in a vertical furnace. As a result of the rapid pyrolysis caused by the furnace, the gel is transformed to a shell in five distinct stages: (a) surface closure of the porous gel; (b) generation of a closed-cell foam structure in the gel; (c) spheridization of the gel and further expansion of the foam; (d) coalescence of the closed-cell foam to a single-void shell; and (e) fining of the glass shell. The heat transfer from the furnace to the falling gel particle was modeled to determine the effective heating rate of the gel. The model predicts the temperature history for a particle as a function of mass, dimensions, specific heat, and absorptance as well as furnace temperature profile and thermal conductivity of the furnace gas. A model was developed that predicts the gravity-induced degradation of shell concentricity in falling molten shells as a function of shell characteristics and time.

Downs, R. L.↗

Design, analysis, and test verification of advanced encapsulation systems

Thermal, optical, structural, and electrical isolation analyses are decribed. Major factors in the design of terrestrial photovoltaic modules are discussed. Mechanical defects in the different layers of an encapsulation system, it was found, would strongly influence the minimum pottant thickness required for electrical isolation. Structural, optical, and electrical properties, a literature survey indicated, are hevily influenced by the presence of moisture. These items, identified as technology voids, are discussed. Analyses were based upon a 1.2 meter square module using 10.2 cm (4-inch) square cells placed 1.3 mm apart as shown in Figure 2-2. Sizing of the structural support member of a module was determined for a uniform, normal pressure load of 50 psf, corresponding to the pressure difference generated between the front and back surface of a module by a 100 mph wind. Thermal and optical calculations were performed for a wind velocity of 1 meter/sec parallel to the ground and for module tilt (relative to the local horizontal) of 37 deg. Placement of a module in a typical array field is illustrated.

Garcia, A.↗

Thermal degradation of the tensile properties of undirectionally reinforced FP-AI203/EZ 33 magnesium composites

The effects of isothermal and cyclic exposure on the room temperature axial and transverse tensile strength and dynamic flexural modulus of 35 volume percent and 55 volume percent FP-Al2O3/EZ 33 magnesium composites were studied. The composite specimens were continuously heated in a sand bath maintained at 350 C for up to 150 hours or thermally cycled between 50 and 250 C or 50 and 350 C for up to 3000 cycles. Each thermal cycle lasted for a total of six minutes with a hold time of two minutes at the maximum temperature. Results indicate to significant loss in the room temperature axial tensile strength and dynamic flexural modulus of composites thermally cycled between 50 and 250 C or of composites isothermally heated at 350 C for up to 150 hours from the strength and modulus data for the untreated, as fabricated composites. In contrast, thermal cycling between 50 and 350 C caused considerable loss in both room temperature strength and modulus. Fractographic analysis and measurement of composite transverse strength and matrix hardness of thermally cycled and isothermally heated composites indicated matrix softening and fiber/matrix debonding due to void growth at the interface and matrix cracking as the likely causes of the strength and modulus loss behavior.

Bhatt, R. T.↗

Effect of aluminum phosphate additions on composition of three-component plasma-sprayed solid lubricant

Image analysis (IA) and electron microprobe X-ray analysis (EMXA) were used to characterize a plasma-sprayed, self-lubricating coating, NASA LUBE PS106, specified by weight percent as 35NiCr-35Ag-30CaF2. To minimize segregation of the powder mixture during the plasma-spraying procedure, monoaluminum phosphate was added to form agglomerate particles. Three concentrations of AlPO4 were added to the mixtures: 1.25, 2.5, and 6.25 percent by weight. Analysis showed that 1.25 wt% AlPO4 yielded a CaF2 deficiency, 2.5 wt% kept the coating closest to specification, and 6.25 wt% yielded excess CaF2 as well as more impurities and voids and a deficiency in silver. Photomicrographs and X-ray maps are presented. The methods of IA and EMXA complement each other, and the reasonable agreement in the results increases the confidence in determining the coating composition.

Jacobson, T. P.↗

An Assessment of Alternate Thermal Protection Systems for the Space Shuttle Orbiter: Executive Summary - Volume 1

Alternate thermal protection system (TPS) concepts to the Space Shuttle Orbiter were assessed. Metallic, ablator, and carbon-carbon concepts which are the result of some previous design, manufacturing and testing effort were considered. Emphasis was placed on improved TPS durability, which could potentially reduce life cycle costs and improve Orbiter operational characteristics. Integrated concept/orbiter point designs were generated and analyzed on the basis of Shuttle design environments and criteria. A merit function evaluation methodology based on mission impact, life cycle costs, and risk was developed to compare the candidate concepts and to identify the best alternate. Voids and deficiencies in the technology were identified, along with recommended activities to overcome them. Finally, programmatic plans, including ROM costs and schedules, were developed for all activities required to bring the selected alternate system up to operational readiness.

Hays, D.↗

Drops and Bubble in Materials Science

The formation of extended p-n junctions in semiconductors by drop migration, mechanisms and morphologies of migrating drops and bubbles in solids and nucleation and corrections to the Volmer-Weber equations are discussed. Bubble shrinkage in the processing of glass, the formation of glass microshells as laser-fusion targets, and radiation-induced voids in nuclear reactors were examined.

Doremus, R. H.↗

Behavior of liquid hydrogen inside an ICF target

The configuration of liquid hydrogen inside spherical glass shell ICF target was studied both theoretically and experimentally. Because of the zero contact angle between the .D2 liquid and glass substrate and the limited wetting surface that is continuous, the liquid hydrogen completely covers the interior of the glass shell, resulting in the formation of a void at the center. For this reason, the present problem distinguishes itself from that for a sessile drop sitting on a flat surface. A theory was formulated to calculate the liquid hydrogen configuration by including the London-dispersion force between the liquid and the substrate molecules. The net result is an augmented Bashforth-Adams equation appropriate to a spherical substrate, which is considered to be the major contribution of the present work. Preliminary calculations indicate that this equation accurately models the liquid hydrogen behavior inside a spherical microshell.

Kim, K.↗

Transient thermal analysis of a titanium multiwall thermal protection system

The application of the SPAR thermal analyzer to the thermal analysis of a thermal protection system concept is discussed. The titanium multiwall thermal protection system concept consists of alternate flat and dimpled sheets which are joined together at the crests of the dimples and formed into 30 cm by 30 cm (12 in. by 12 in.) tiles. The tiles are mechanically attached to the structure. The complex tile geometry complicates thermal analysis. Three modes of heat transfer were considered: conduction through the gas inside the tile, conduction through the metal, and radiation between the various layers. The voids between the dimpled and flat sheets were designed to be small enough so that natural convection is insignificant (e.g., Grashof number 1000). A two step approach was used in the thermal analysis of the multiwall thermal protection system. First, an effective normal (through-the-thickness) thermal conductivity was obtained from a steady state analysis using a detailed SPAR finite element model of a small symmetric section of the multiwall tile. This effective conductivity was then used in simple one dimensional finite element models for preliminary analysis of several transient heat transfer problems.

Blosser, M. L.↗

Develop, demonstrate, and verify large area composite structural bonding with polyimide adhesives

The technology required to produce graphite-polyimide structural components with operational capability at 598 K (600 F) is considered. A series of polyimide adhesives was screened for mechanical and physical properties and processibility in fabricating large midplane bonded panels and honeycomb sandwich panels in an effort to fabricate a structural test component of the space shuttle aft body flap. From 41 formulations, LaRC-13, FM34B-18, and a modified LaRC-13 adhesive were selected for further evaluation. The LaRC-13 adhesive was rated as the best of the three adhesives in terms of availability, cost, processibility, properties, and ability to produce void fee large area (12" x 12") midplane bonds. Surface treatments and primers for the adhesives were evaluated and processes were developed for the fabrication of honeycomb sandwich panels of very good quality which was evidenced by rupture in the honeycomb core rather than in the facesheet bands on flatwise tensile strength testing. The fabrication of the adhesively bonded honeycomb sandwich cover panels, ribs, and leading edge covers of Celion graphite/LARC-160 polyimide laminates is described.

Bhombal, B. D.↗

Irradiation effects in rapidly and conventionally solidified alloys. Phase stability in rapidly solidified N i-Nb under Ni ion irradiation

Two alloy compositions in the Ni-Nb system (Ni60Nb40 and Ni85Nb15) were produced by rapidly quenching from the melt with the piston anvil technique. The Ni60Nb40 was transformed to a metastable, partially crystalline state by heat treatment in a differential scanning calorimeter. The Ni85Nb15 was fully crystalline, with the majority of the grains composed of collections of primary dendrite arms. Both compositions were irradiated with 4 MeV Ni++ ions. The irradiation induced microstructures were examined by transmission electron microscopy and compared with thermally aged samples. The thermal evolution was arrested by ion irradiation in the temperature range studied, by inhibiting the nucleation of the NiNb phase. No irradiation induced voids were observed. It is found that the ion irradiation drives the microstructure along a different path than thermal evolution.

Source record↗

Attachment system for silica tiles

An improved method for markedly increasing the bond strength between a rigid, porous refractory material and non-rigid substrate by densifying the face of the rigid material opposing the substrate is discussed. Densification is accomplished by wetting the refractory material and then impregnating it with a composite slurry having a particle size to fill voids of the porous material.

Dotts, R. L.↗

LARC-TPI: A multi-purpose thermoplastic polyimide

A linear thermoplastic polyimide, LARC-TPI, was characterized and developed for a variety of high temperature applications. In its fully imidized form, this material can be used as an adhesive for bonding metals such as titanium, aluminum, copper, brass, and stainless steel. LARC-TPI was evaluated as a thermoplastic for bonding large pieces of polyimide film to produce flexible, 100 void-free laminates for flexible circuit applications. The development of LARC-TPI as a potential molding powder, composite matrix resin, high temperature film and fiber is also discussed.

St.clair, A. K.↗

Metal/silicon interface formation - The Ni/Si and Pd/Si systems

The valence level spectra of the Ni/Si and Pd/Si systems have been investigated using high resolution X-ray photoelectron spectroscopy. Temperature dependence studies for Ni deposited on thin thermal SiO2 demonstrate the importance of metal aggregation effects in the interpretation of binding energies as chemical shifts. Temperature studies for the Ni/Si system indicate that substantial chemical interaction occurs at the interface at temperatures as low as 100 K. These studies also show the presence of Ni in interstitial voids in the Si near the interface. A comparative study of the core and valence band features for the Ni and Pd silicides provides many valuable insights and a self-consistent picture of the attendent valence charge redistribution and its influence on the observed chemical shifts.

Grunthaner, P. J.↗

Applications of the TIROS-N sounding and cloud motion wind enhancement for the FGGE 'special effort'

In January of 1978, a panel of experts recommended that a 'special effort' be made to enhance and edit satellite soundings and cloud tracked winds in data sparse regions. It was felt that these activities would be necessary to obtain maximum benefits from an evaluation of satellite data during the Global Weather Experiment (FGGE). The 'special effort' is being conducted for the two special observing periods of FGGE. More than sixty cases have been selected for enhancement on the basis of meteorological interest. These cases include situations of blocking, cutoff low development, cyclogenesis, and tropical circulations. The sounding data enhancement process consists of supplementing the operational satellite sounding data set with higher resolution soundings in meteorologically active regions, and with new soundings where data voids or soundings of questionable quality exist.

Atlas, R.↗