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DOE OSTI2018

Toward better hydraulic fracturing fluids and their application in energy production: A review of sustainable technologies and reduction of potential environmental impacts

Recent advances in hydraulic fracturing, in conjunction with horizontal drilling, have enabled large-scale extraction of natural gas and oil from shale formations. Despite its advances and enormous economic benefits, opportunities remain to increase hydraulic fracturing efficiency and minimize potential environmental impacts. This review specifically examines three key themes associated with development and utilization of hydraulic fracturing fluids: 1) characteristics and behavior of fracturing fluids, 2) understanding and predicting migration and fate of fracturing fluids, 3) technologies to reduce environmental impact of fracturing fluids. Furthermore, the paper discusses key and new techniques and findings on rheology of hydrogel-based fluids, high fidelity simulation of propagation transport, potential environmental impacts, geosynthetics in mitigating contamination, and greener fracturing fluids. It is indicated that future development relies on advances in understanding of physical processes, modeling capabilities, and monitoring techniques.

02 PETROLEUM↗

DOE OSTI2024

Beyond the Surface: Non-Invasive Low-Field NMR Analysis of Microbially-Induced Calcium Carbonate Precipitation in Shale Fractures

Microbially-induced calcium carbonate precipitation (MICP) is a biological process in which microbially-produced urease enzymes convert urea and calcium into solid calcium carbonate (CaCO 3 ) deposits. MICP has been demonstrated to reduce permeability in shale fractures under elevated pressures, raising the possibility of applying this technology to enhance shale reservoir storage safety. For this and other applications to become a reality, non-invasive tools are needed to determine how effectively MICP seals shale fractures at subsurface temperatures. In this study, two different MICP strategies were tested on 2.54 cm diameter and 5.08 cm long shale cores with a single fracture at 60 °C. Flow-through, pulsed-flow MICP-treatment was repeatedly applied to Marcellus shale fractures with and without sand (“proppant”) until reaching approximately four orders of magnitude reduction in apparent permeability, while a single application of polymer-based “immersion” MICP-treatment was applied to an Eagle Ford shale fracture with proppant. Low-field nuclear magnetic resonance (LF-NMR) and X-Ray computed microtomography (micro-CT) techniques were used to assess the degree of biomineralization. With the flow-through approach, these tools revealed that while CaCO 3 precipitation occurred throughout the fracture, there was preferential precipitation around proppant. Without proppant, the same approach led to premature sealing at the inlet side of the core. In contrast, immersion MICP-treatment sealed off the fracture edges and showed less mineral precipitation overall. This study highlights the use of LF-NMR relaxometry in characterizing fracture sealing and can help guide NMR logging tools in subsurface remediation efforts.

MICP↗

DOE OSTI2019

Effect of natural fractures on determining closure pressure

Abstract In Utah FORGE reservoir, eight pressure transient tests (microhydraulic fracturing and DFIT™) show natural fracture/pressure-dependent leakoff. This behavior may lead to misinterpretation of the closure pressure (proxy for minimum principal stress). The closure pressures obtained from DFIT™ (or microhydraulic fracturing) testing may reflect shear failure along natural fractures or discontinuities rather than tensile failure and lead to inaccurate estimates of the minimum principal stress. In pressure tests conducted at the Utah FORGE site showed that reactivation or opening of natural fractures intersecting the wellbore and were suggested by multiple closure events in DFIT™ tests. In addition, comparisons between the pre- and post-well-tests FMI logs show that there are populations of induced fracture and reactivated natural fractures which are mostly vertical and sub-vertical. In this study, DFIT™ (or microhydraulic fracturing) test analysis and numerical simulations were used to suggest that hydraulic shearing of critically stressed natural fractures can contribute to multiple closure signatures and possibly lead to incorrect determination of the minimum principal stress. As other authors have previously advocated, the DFIT™ test analyses and numerical simulations suggest that better estimations of minimum principal stress may be derived by injecting at relatively high rate and pressure and insuring that tensile breakdown is reached. In addition, extended shut-in period is required to determine accurate reservoir characteristics and fluid flow regime.

Nadimi, S.↗

DOE OSTI2017

Fragility Fractures of the Pelvis: New Approaches to Classification and Management

Purpose of Review: The purpose of the present article is to review the new approaches to classification and management of fragility fractures of pelvis. Recent Findings: Fragility fractures of the pelvis (FFPs) account for approximately 7% of fragility fractures and are increasing in incidence due to the aging population, an increase in life expectancy, and a more active life-style. The FFPs are characterized by isolated bone disruption and are generally more stable than high-energy pelvic ring fractures due to intact ligaments. Due to differences in the degrees of instability, the traditional classification systems (Tile or Young and Burgess) for acute pelvic ring injuries from high-energy trauma may not be applicable to FFPs. Through a classification system based on fracture location and the degree of instability, FFPs can be appropriately managed with either conservative treatment or surgery. Summary: Fragility fractures occur in patients with primary or secondary osteoporosis from low-energy trauma or no known trauma. FFPs are different from high-energy pelvic fractures in the degree of instability and the approach to fracture management. Diagnosis of FFPs requires a high index of suspicion and the early use of CT or MRI to prevent long-term complications.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2018

Hip Fractures: A Practical Approach to Diagnosis and Treatment

Purpose of Review: To summarize relevant anatomy, imaging, and treatment of hip fractures, and to synthesize a treatment-based approach for description and classification of hip fractures. Recent Findings: Hip fractures are predominantly seen in the elderly, where they are increasing in incidence, and can substantially reduce healthy life-years. The osseous and vascular anatomy of the proximal femur can help to understand the clinical implications of various types of hip fracture. Radiographs are the principal imaging modality for assessment of hip fracture, although there is a clear role for CT and MRI for assessment of radiographically occult fractures. There are multiple classifications of hip fractures in the orthopedic literature; however, these are not commonly used in clinical practice due to complexity, poor reported inter-observer agreement, and relatively few methods of surgical fixation. Summary: A simplified anatomic and treatment-based approach to hip fractures can help guide image interpretation and clinical management.

62 RADIOLOGY AND NUCLEAR MEDICINE↗

DOE OSTI2020

Onset dynamics of air-water menisci on rock fracture surfaces

Information on menisci dynamics and equilibrium contact angles, θ e , is needed for modeling multiphase flow of fluids in geologic formations. The wettability of fracture faces is relevant to applications such as waterflooding in enhanced oil recovery and evaluation of caprock integrity for geologic carbon sequestration. We investigated the vertical capillary rise of air-water menisci on exposed fracture faces for a sandstone, a shale, and three granites. The experimental design approximated that employed in the Wilhelmy plate method. Replicate fracture faces were prepared by fracturing cylindrical rock cores using the Brazilian method and splitting the fractured cores apart along their fracture planes. Meniscus onset was imaged from a cross-sectional perspective using dynamic neutron radiography, and quantified with change point analysis. An existing model for meniscus onset fitted the experimental data very well (median R 2 = 0.96). Capillary rise was typified by t 2/3 scaling (where t is time), followed by a constant equilibrium height, z e . The average time taken for the menisci to reach z e was 0.39 s, with no differences between rock types. The menisci achieved a greater vertical extent on the fracture faces of the sedimentary rocks as compared to those of the granites. Apparent θ e values were calculated from the best fit estimates of z e using the Wilhelmy plate equation for a smooth and planar vertical surface. Despite the fractal roughness of some of the fracture faces, there was a significant linear relationship (R 2 = 0.80) between the apparent θ e values and intrinsic θ e values measured on polished surfaces of the same rocks using the sessile drop method. The regression equation indicated the apparent θ e values were consistently greater than the intrinsic values. This overestimation may be due to averaging of pixels at the air-water-solid interface, a required step in the image analysis. Further exploration of the range of applicability and measurement accuracy of this proposed new technique would be valuable.

58 GEOSCIENCES↗

DOE OSTI2018

Joint opening or hydroshearing? Analyzing a fracture zone stimulation at Fenton Hill

Here, we analyze a deep hydraulic stimulation of a fracture zone that was conducted as part of the classical Fenton Hill Hot Dry Rock Program in the 1970s. At the time, it was suggested that a pre-existing fracture or multiple fractures within the fracture zone were jacked open by injection-induced increase in pressure. In this study, we analyze the same stimulation experiment, but investigate the possibility of an alternative mechanism of shear reactivation of pre-existing fractures. We conduct modeling that accounts for both jacking (or elastic-fracture opening) and shear-slip dilation and demonstrate that injection-induced shear reactivation (or hydroshearing) could have occurred simultaneously with seismic events of magnitudes lower than what can be felt by humans. In fact, simulations considering shear reactivation seem to better match observed fluid recovery after multiple injection cycles. Shear reactivation and shear dilation results in locked-open fractures, especially near the injection well that provides permeability of higher flow recovery. We then investigate the sensitivity of the proposed model by varying some of the critical parameters such as maximum aperture, dilation angle, as well as fracture density. Interestingly, none of the simulated cases resulted in a large event that could have been felt by humans, but did result in a cumulative seismic magnitude of less than 1 for each given stimulation step. In conclusion, these results suggest that a permanent irreversible permeability increase of several orders of magnitude can be obtained by hydroshearing in a “seismically” safe manner.

58 GEOSCIENCES↗

DOE OSTI2020

Fracture toughness evaluation for Zr-4 clad tubing structure with pellet inserts

Applying fracture mechanics approach to spent nuclear fuel (SNF) system reliability investigation is warranted due to the inherent flaws and hydride structures existed in a SNF system after nuclear reactor operation. However, none of the existing fracture toughness data deal with fuel cladding specific geometry or spent fuel material conditions, such as cladding structure with the pellet-inserts and the associated pellet clad mechanical interactions induced mixed-mode damage mechanisms. Thus, the development of an intrinsic fracture mechanics approach that is suitable for SNF materials is needed. Due to thin wall and small dimension of clad tubing structure, the spiral notch torsion test (SNTT) method of small specimen approach was used to estimate the clad tubing structure fracture toughness. The estimated fracture toughness for Zr-4 cladding with alumina-pellet inserts are presented in this report. For SNTT samples with a short or medium crack length, between 5.4-mm and 8-mm, the estimate JIQ upon fracture initiation for the baseline Zr-4 cladding is at 50 kJ/m2 with 2-sigma uncertainty of 3.26 kJ/m2, and the associated KIQ is at 67.46 MPa√m. For SNTT samples with a long crack length, around 13-mm, the crack initialization is deviated from that of the Mode-I tensile fracture and appears to be a mixed-mode fracture of Mode I – tensile stress and Mode III – out of plane shear stress; the estimated JMQ is at 18.9 kJ/m2, the associated KMQ is at 41.4 MPa√m.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Thin-Film Fracture Behavior for Diketopyrrolopyrrole Semiconducting Polymeric Films

Fracture energy, which quantifies a material’s resistance to the propagation of a pre-existing crack, is a key parameter for ensuring the mechanical reliability of stretchable organic electronic devices. However, most existing methods, such as a four-point bending fracture energy, utilized for measuring the fracture energy of semiconducting polymeric thin films are complicated by substrate effects, making it challenging to isolate the intrinsic behavior of the film from interfacial influences. In this study, we employed a pseudo free-standing pure shear method to systematically investigate the cohesive fracture energy of poly(diketopyrrolopyrrole-terthiophene) P(DPP-T)-based thin films to examine the effects of nanoconfinement, side chain length, degree of crystallinity, and strain rates. This method effectively eliminates substrate interference, enabling a direct assessment of the cohesive fracture energy of P(DPP-T) thin films. We found that thinner films and those with lower molecular weights exhibited significantly reduced fracture energies due to diminished chain entanglements. Additionally, films with shorter side chains displayed notably higher fracture energies, which were attributed to an increase in the degree of crystallinity. Finally, slower strain rates led to higher fracture energies, consistent with an enhanced stress relaxation. These insights offer practical guidelines for designing mechanically robust semiconducting polymers, contributing to the advancement of reliable, durable, flexible, and wearable electronic devices.

Zhang, Song [Univ. of Southern Mississippi, Hattie↗

DOE OSTI2016

Numerical Simulation of Permeability Change in Wellbore Cement Fractures after Geomechanical Stress and Geochemical Reactions Using X-ray Computed Tomography Imaging

X-ray microtomography (XMT) imaging combined with a three-dimensional (3D) computational fluid dynamics (CFD) modeling technique was used to study the effect of geochemical and geomechanical processes on fracture properties in composite Portland cement–basalt caprock core samples. The effect of fluid properties and flow conditions on fracture permeability was numerically studied by using fluids with varying physical properties and simulating different pressure conditions. CFD revealed that the application of geomechanical stress led to increased fluid flow, which resulted in increased fracture permeability. After CO2-reaction, XMT images displayed preferential precipitation of calcium carbonate within the fractures in the cement matrix and less precipitation in fractures located at the cement–basalt interface. CFD predicted changes in flow characteristics and differences in absolute values of flow properties due to different pressure gradients. CFD was able to highlight the profound effect of fluid properties on flow characteristics and hydraulic properties of fractures. This study demonstrates the applicability of XMT imaging and CFD as powerful tools for characterizing the hydraulic properties of fractures in a number of applications like geologic carbon sequestration and storage, hydraulic fracturing for shale gas production, and enhanced geothermal systems.

CO2 storage↗

DOE OSTI2019

Scalable En Echelon Shear‐Fracture Aperture‐Roughness Mechanism: Theory, Validation, and Implications

Abstract Shear fractures can facilitate fluid conductivity through rock. Aperture and roughness are controlling characteristics for a fracture's fluid conductivity. Inspired by en echelon fractures, we develop a shear “fracturelet” model that predicts anisotropic aperture with respect to the direction of shearing, rougher (nonplanar) rather than smoother (planar) fractures, and the bounds of this roughness for a coalesced fracture. This tendency for rougher fracture creation is validated by in situ X‐ray images and fluid conductivity measurements from triaxial direct shear experiments on anhydrite and shale. These experiments were conducted at confining stresses from 4 to 30 MPa and shear displacement magnitudes from 0 to 2 mm on initially intact rock specimens. Hydraulic, dilatational, and local fracture apertures were measured in the experiments. Apertures exhibited strong anisotropy with more conductive flow paths forming perpendicular to the direction of shearing. Local and dilatational aperture were found to be positively correlated with increasing shear displacement but hydraulic aperture was found to vary significantly, always having values smaller than the other aperture measures at factors ranging from 0.6 to 0.0. An implication of these results is that shear fractures have a mechanism for simultaneously exhibiting very low fluid conductivity and high fluid storage volume.

Frash, Luke P.↗

DOE OSTI2016

Approaching a universal scaling relationship between fracture stiffness and fluid flow

A goal of subsurface geophysical monitoring is the detection and characterization of fracture alterations that affect the hydraulic integrity of a site. Achievement of this goal requires a link between the mechanical and hydraulic properties of a fracture. Here we present a scaling relationship between fluid flow and fracture-specific stiffness that approaches universality. Fracture-specific stiffness is a mechanical property dependent on fracture geometry that can be monitored remotely using seismic techniques. A Monte Carlo numerical approach demonstrates that a scaling relationship exists between flow and stiffness for fractures with strongly correlated aperture distributions, and continues to hold for fractures deformed by applied stress and by chemical erosion as well. This new scaling relationship provides a foundation for simulating changes in fracture behaviour as a function of stress or depth in the Earth and will aid risk assessment of the hydraulic integrity of subsurface sites.

42 ENGINEERING↗

DOE OSTI2022

Fracture toughness of schist, amphibolite, and rhyolite from the Sanford Underground Research Facility (SURF), Lead, South Dakota

The Cracked Chevron Notched Brazilian Disc (CCNBD) method was selected for Mode I fracture toughness tests on Poorman schist, Yates amphibolite, and rhyolite dikes from the EGS Collab site at the SURF in Lead, South Dakota. The effects of lithology, anisotropy, and loading rate were investigated. Fracture toughness was greatest in amphibolite, with schist and rhyolite having similar toughness values ($K$ amphibolite > $K$ rhyolite ≈ $K$ schist ). The effects of anisotropy on fracture toughness were investigated in the foliated schist samples. Schist samples were prepared in three geometries (divider, arrester, and short transverse) which controlled how the fracture would propagate relative to foliations. The divider geometry was strongest and short transverse geometry was the weakest ($K$ divider > $K$ arrester > $K$ shorttransverse ). Fracture toughness was observed to decrease with decreasing loading rate. Optical and SEM microscopy revealed that for the short transverse geometry, fractures tended to propagate along grain boundaries, whereas in arrester and divider geometries fractures tended to propagate through grains. In foliated samples, the tortuosity of the fracture observed in thin section was greater in arrester and divider geometries than in short transverse geometries.

58 GEOSCIENCES↗

DOE OSTI2025

Mechanistic understanding of carbon mineralization in fracture systems using microfluidics

Carbon mineralization in mafic and ultramafic rocks presents an opportunity for permanent carbon storage in the Earth's subsurface. However, due to their lower permeability, pre-existing fracture networks are key for mineralization to occur. Therefore, to fully develop this technology, a mechanistic understanding of the mineralization behavior in fractures with the consideration of hydrodynamic components is required. We use high-pressure microfluidics to investigate key mechanisms influencing dissolution–precipitation in a fracture network. The experiments were conducted in micromodels made of natural rocks with a comb-shaped flow channel to mimic a fracture network. This enabled studying the effect of injection rate on coupled dissolution–precipitation in advection and diffusion-dominated flow paths. We used gypsum carbonation as an analog reaction to allow for realistic experimental time frames due to its rapid reaction kinetics. The experimental work is coupled with high-fidelity numerical simulations to enhance our understanding of the parameters affecting the mineralization reaction. Our results demonstrate the importance of flow rate on the rate and nature of the gypsum carbonation reaction revealing that higher flow rates enable deeper penetration of the mineral precipitation front into the dead-end channels. This is an important finding since for sustained mineralization in a fracture network, precipitation in dead-ends while still allowing for flowing fractures is critical. Detailed characterization of the precipitates showed that lower flow rates led to porous and loose precipitates in the form of aragonite while higher flow rates mimicked supersaturation behavior leading to the formation of calcite. The reactive transport simulations further demonstrated the significance of flow velocity in advection-dominated channels to influence the efficiency of carbon mineralization in diffusion-dominated channels, potentially clogging of dead-end channels. These findings highlight the need for coupling chemical, mechanical, and hydrodynamic processes to evaluate the nature and extent of carbon mineralization in fractured media critical for permanent storage in mafic and ultramafic formations. This research further highlights the need for more investigation in potential subsurface fracture generation techniques to aid carbon mineralization.

25 ENERGY STORAGE↗

DOE OSTI2024

Investigating In-Situ Fracture Behaviors of Polymer Pipeline Materials in Hydrogen and Hydrogen-Methane Blended Gas Environments

To reduce carbon emissions, the US natural gas infrastructure is seen as a primary solution for efficiently transporting hydrogen gas. Blending hydrogen gas with natural gas and transporting it across a national infrastructure could save significant infrastructure costs. To properly operate the infrastructure under the new gas system, it is critical to understand material compatibility with hydrogen under various conditions. The Blended Gas CRADA, a Hyblend project, is established to determine the material compatibility of existing natural gas pipes with hydrogen gas. In this study, we investigate the in-plane fracture behaviors of MDPEMarlex and HDPEGDB exposed to hydrogen and hydrogen-methane blended gas. Single-edge notch bending geometry is used. All tests are executed in-situ with the gas environment. The experimental results show a significant effect of the gas environment on HDPEGDB specimens, reducing 5% (H2) to 42% (Blended gas) of specific fracture energy compared to non-aged specimens. For the MDPEMarlex, the effects of the gas environment have increased the specific fracture energy by 10% (H2) to 15% (Blended gas). Fracture surfaces of the tested samples are observed using an electronic microscope. The in-plane fracture surface of HDPEGDB shows a pronounced dimple fracture pattern after exposure to hydrogen and blended gas. The expanded fracture pattern contributes to lower the specific fracture energy. These observations provide critical information for validating polymer pipeline materials when interact with hydrogen and hydrogen-blend gas.

Ko, Seunghyun↗

DOE OSTI2021

Investigating Fracture Network Deformation Using Noble Gas Release

We investigate deformation mechanics of fracture networks in unsaturated fractured rocks from subsurface conventional detonation using dynamic noble gas measurements and changes in air permeability. We dynamically measured the noble gas isotopic composition and helium exhalation of downhole gas before and after a large subsurface conventional detonation. These noble gas measurements were combined with measurements of the subsurface permeability field from 64 discrete sampling intervals before and after the detonation and subsurface mapping of fractures in borehole walls before well completion. We saw no observable increase in radiogenic noble gas release from either an isotopic composition or a helium exhalation point of view. Large increases in permeability were observed in 13 of 64 discrete sampling intervals. Of the sampling intervals which saw large increases in flow, only two locations did not have preexisting fractures mapped at the site. Given the lack of noble gas release and a clear increase in permeability, we infer that most of the strain accommodation of the fractured media occurred along previously existing fractures, rather than the creation of new fractures, even for a high strain rate event. These results have significant implications for how we conceptualize the deformation of rocks with fracture networks above the percolation threshold, with application to a variety of geologic and geological engineering problems.

Gardner, W. Payton↗

DOE OSTI2021

Characterization of an electrically conductive proppant for fracture diagnostics

Fracture diagnosis with electromagnetic (EM) and electrical tools requires proppants with high electrical conductivity and mechanical strength. Lab measurements of the electrical and hydraulic conductivity of proppants are critical for selecting the best candidates. Such measurements greatly benefit simulations, field tests, and the ultimate application of such proppants in the field. To that end, a new lab protocol is developed for measuring the electrical and hydraulic conductivity of proppants. The lab setup, which mainly includes a resistivity core holder and a Hassler sleeve core holder, allows for simulation of realistic pressure and temperature conditions when making measurements. Petroleum coke (PC) is proposed as a candidate proppant because of its widespread availability and low cost. Lab measurements show that the effective electrical conductivity of pure PC in a model fracture is approximately 5000 S/m, under a closure stress greater than [Formula: see text] (4000 psi). When PC is mixed with sand, the effective electrical conductivity of the mixture decreases with an increasing weight percentage of sand. Although sand degrades the contact between PC particles, the electrical conductivity stays reasonably high (approximately 1700 S/m) when 50% sand is added. Hydraulic conductivity measurements show that when a fracture is propped with pure PC, the measured fracture conductivity is greater than [Formula: see text] ([Formula: see text]) (dimensionless fracture conductivity greater than 100 for a shale with [Formula: see text] or 100 nD permeability) under a confining pressure of [Formula: see text] (6000 psi). This means that a fracture propped with PC is infinitely conductive in a typical shale formation. When sand is added, the fracture’s hydraulic conductivity becomes even higher, which clearly shows PC’s ability of sustaining high stresses. The proposed protocol provides a robust and effective method that can be generalized for lab testing for other candidate proppants. The data presented clearly show that PC has the potential for field-scale applications in EM hydraulic fracture diagnostics.

Geochemistry & Geophysics↗

DOE OSTI2018

Environmental Impact Analysis on the Hydraulic Fracture Test Site (HFTS)

Objective The Hydraulic Fracture Test Site (HFTS) provided a platform to test new extraction and production techniques and technologies to understand fracture geometry and increase the efficiency of shale hydrocarbon production. Eleven test wells were drilled in the Upper and Middle Wolfcamp formations, hydraulically fractured, and produced. Air quality, groundwater quality, and produced water chemistry and microbiology were monitored through the duration of the field experiment and one year into production. Methods BTEX, methane, VOCs, SOx, NOx, and PM 10 were measured 1,000 ft up-wind and 1,000 ft down-wind of the HFTS experiment before operations began, during hydraulic fracturing, flowback, and several months into production to evaluate operational impact on local air quality. The underlying Edward-Trinity Plateau aquifer was monitored using 5 groundwater wells within 2 miles of the HFTS pad; BTEX, methane, petroleum hydrocarbons, and a comprehensive suite of anions and metals were analyzed from samples taken before operations began, during hydraulic fracturing, flowback, and one year after production. Water produced from 3 of the 11 HFTS wells was analyzed for chemical and microbiological properties 1.5 years into production. Observations There was no significant impact to air quality from HFTS operations, although elevated BTEX concentrations were measured 1,000 ft. away from the well-pads during the flowback period. We detected no migration of hydrocarbon or fracture fluid chemical migration into the Edward-Trinity Plateau aquifer. Source waters used for hydraulic fracturing contained naturally occurring high concentrations (~500ppm) of sulfate. Rapid microbially induced corrosion was detected in several wells, leading to biocide dosing. Microbiological populations were significantly altered by biocide treatment, but still continued to increase in population size six months after application. Significance After hydraulic fracturing, detailed chemical and microbiological analysis provides evidence for microbiologicallymediated sub-surface transformations of supplied sulfate and organic carbon into sulfides. This report discusses air quality, water quality, and produced water analytical results for the HFTS experiment and further implications for the unconventional oil and gas industry.

Eisenlord, Sarah↗