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At least 559 records · Page 31
All sourcesNASA NTRSDOE OSTI
NASA NTRS1987

Electronic heterodyne moire deflectometry: A method for transient and three dimensional density fields measurements

Effects of diffraction and nonlinear photographic emulsion characteristics on the performance of deferred electronic heterodyne moire deflectometry are investigated. The deferred deflectometry is used for measurements of nonsteady phase objects where it is difficult to complete the analysis of the field in real time. The sensitivity, accuracy and resolution of the system are calculated and it is shown that they are weakly affected by diffraction and by nonlinear recording. The feactures of the system are significantly improved compared with the conventional deferred intensity moire technique, and are comparable with the online heterodyne moire. The system was evaluated experimentally by deferred measurements of the refractive index gradients of a weak phase object consisting of a large KD*P crystal. This was done by photographing the phase object through a Ronchi grating and analyzing the tranparency with the electronic heterodyne readout system. The results are compared with the measurements performed on the same phase object with online heterodyne moire deflectometry and with heterodyne holographic interferometry methods. Some practical considerations for system improvement are discussed.

Stricker, Josef↗
NASA NTRS1987

The first products made in space - Monodisperse latex particles

Monodisperse latex particles developed by seeded emulsion polymerization on various Space Shuttle flights are analyzed. The flight hardware was composed of a monodisperse latex reactor and a support electronics package, and the particles were examined by optical microscopy and TEM. Data on the particle size distributions, larger and smaller off-size particles, and conversion-time curves for the particles are examined and compared to ground-based results. It is observed that the ground-based polymerizations have more coagulum than the flight polymerizations; the flight latex particles have narrower size distributions than the ground particles; and the number of off-size larger particles in the flight particles is smaller than in the ground data.

Vanderhoff, J. W.↗
NASA NTRS1986

Stopping of relativistic heavy ions in various media

The residual ranges of (900 + or - 3)-MeV/amu gold nuclei accelerated at the Lawrence Berkeley Laboratory Bevalac have been measured in several different media. The energy of the beam of nuclei was measured directly using a new time-of-flight system. The ranges were measured by absorption in linear wedges of polyethylene, carbon, aluminum, copper, tin, and lead and in circular wedges of polystyrene, aluminum, and gold, and by total absorption in nuclear emulsion. The measured ranges were significantly different from those calculated from the best available theoretical estimates of the energy loss of highly charged nuclei. It is concluded that at present energy losses and residual ranges of relativistic heavy ions in an arbitrary medium cannot be predicted with better than an approximately 2 percent accuracy.

Waddington, C. J.↗
NASA NTRS1986

Average transverse momentum and energy density in high-energy nucleus-nucleus collisions

Emulsion chambers were used to measure the transverse momenta of photons or pi(0) mesons produced in high-energy cosmic-ray nucleus-nucleus collisions. A group of events having large average transverse momenta has been found which apparently exceeds the expected limiting values. Analysis of the events at early interaction times, of the order of 1 fm/c, indicates that the observed transverse momentum increases with both rapidity density and energy density.

Burnett, T. H.↗
NASA NTRS1986

Undercooling and crystallization behaviour of antimony droplets

The droplet emulsion technique is presently used to examine the undercooling and crystallization behavior of pure antimony. Control of droplet size and applied cooling rate allowed maximum undercooling to be extended from 0.08 to 0.23 T(m). A droplet coating was produced by means of emulsification which appears to furnish a favorable crystallographic matching for effective nucleation catalysis of a metastable simple cubic structure. Thermal analysis shows the melting temperature of the single cubic phase to be about 625 C.

Graves, J. A.↗
NASA NTRS1986

Hybrid X-ray telescope systems

It has been known for some time that glancing incidence X-ray optics have sharply peaked point response functions. The spatial resolution of Wolter X-ray telescope systems is frequently limited by the performance characteristics of the X-ray detector rather than by the optics, even when high resolution detectors such as photographic emulsions are used. This problem becomes even more severe when it is desirable to take advantage of the high sensitivity and broad wavelength response afforded by modern solid state detectors such as charge coupled devices or multi-anode microchannel arrays. Results of theoretical investigations of methods for increasing the telescope plate scale by the use of glancing incidence hyperboloid/ellipsoid X-ray microscope optics and normal incidence contoured layered synthetic microstructure optics for coupling the Wolter mirrors to the detector are reported. The relative merits of the different hybrid X-ray telescope systems which result will be discussed. Considerations will be made concerning applications of these systems to high resolution imagery and spectroscopy of astronomical X-ray/XUV sources.

Shealy, David L.↗
NASA NTRS1987

Nucleus-nucleus interactions between 20 and 65 GeV per nucleon

A hybrid electronic-counter/emulsion-chamber instrument was exposed to high-energy cosmic rays on a balloon. The data on 105 nucleus-nucleus collisions in the energy range 20-65 GeV/nucleon and for incident nuclear charges Zp in the range of 22 to 28 are presented. Inclusive characteristics of particle production on different targets (plastic, emulsion, and lead) are shown and compared with models based on the superposition of nucleon-nucleus interactions. Features of a subset of the more central collisions with a plastic target and some characteristics of individual events with the highest multiplicity of produced particles are described.

Burnett, T. H.↗
NASA NTRS1984

Preparation of large-particle-size monodisperse latexes in space - Polymerization kinetics and process development

Monodisperse polystyrene latexes are prepared by seeded emulsion polymerization; however, sizes larger than 2 microns are difficult to prepare because of the creaming and settling of the particles and their sensitivity to mechanical shear. Preparation in space would obviate the creaming and settling, and allow agitation just sufficient for good heat transfer and mixing. Three polymerizations yielding 3-5 micron size particles were carried out successfully on the third flight of the 'Columbia' launched Mar. 22, 1982; however, four polymerizations yielding sizes up to 10 microns on the fourth flight launched June 27, 1982 were incomplete owing to apparatus malfunction. The results of these polymerizations and the prospects of developing a preparative space process are reviewed.

Vanderhoff, J. W.↗
NASA NTRS1985

The formation of small scale granularities in latex particles

A series of latices were synthesized using emulsifier-free emulsion copolymerization of styrene and sodium styrene sulfonic acid. The final latex particles display an internal granular structure which can be ascribed to the primary particles present in the early stages of particle growth. In these systems, the primary particles appear to have maintained their integrity during the swelling and growth stage.

Zukoski, C. F.↗
NASA NTRS1986

Kinetics of successive seeding of monodisperse polystyrene latexes. I - Initiation via potassium persulfate. II - Azo initiators with and without inhibitors

The polymerization kinetics of monodisperse polystyrene latexes with diameters of 1 micron are studied. The monodisperse latexes were prepared by the successive seeding method using 1 mM K2S2O8 with an 8 percent emulsifier surface coverage and 0.5 mM K2S2O8 with a 4 percent emulsifier surface coverage, and the kinetics were measured in a piston/cylinder dialometer. The data reveal that the polymerization rate decreases with increasing particle size; and the surface charge decreases with increasing particle size. The effects of initiators (AIBN and AMBN) and inhibitors (NH24SCN, NaNO2, and hydroquinone) on the product monodispersity and polymerization kinetics of latexes with diameters greater than 1 micron are investigated in a second experiment. It is observed that hydroquinone combined with AMBN are most effective in reducing nucleation without causing flocculation. It is noted that the kinetic transition from emulsion to bulk is complete for a particle size exceeding 1 micron in which the polymerization rate is independent of the particle size.

Sudol, E. D.↗
NASA NTRS1986

A dual plate thermoplastic recording device for holographic interferometry

The development of a dual plate holographic interferometer using thermoplastic recording devices is described. The operational characteristics of the thermoplastic devices are investigated and optimized for fringe contrast and signal-to-noise ratio. The dual plate device was demonstrated in a transonic wind tunnel at NASA Ames Research Center. The interferograms derived from the thermoplastic device are compared with those derived from conventional photographic emulsions. The fringe contrast achieved with the optimized thermoplastic device is equivalent to the contrast achieved with conventional techniques.

Umstatter, Holly L.↗
NASA NTRS1988

Demixing of aqueous polymer two-phase systems in low gravity

Experiments on the effect of gravity on phase emulsion demixing were performed in order to study the potential of two-phase partitioning in space. The behavior of phase systems possessing phase density differences and systems with essentially identical phase densities was investigated during one-g and low-g parabolic aircraft maneuvers. It is found that demixing can occur rather rapidly in space, although more slowly than on earth. The Ostwald ripening theory predicts demixing rates many orders of magnitude lower than the observed values.

Bamberger, S.↗
NASA NTRS1989

Photopolymerization Of Levitated Droplets

Experimental containerless process combines two established techniques to make variety of polymeric microspheres. In single step, electrostatically-levitated monomer droplets polymerized by ultraviolet light. Faster than multiple-step emulsion polymerization process used to make microspheres. Droplets suspended in cylindrical quadrupole electrostatic levitator. Alternating electrostatic field produces dynamic potential along axis. Process enables tailoring of microspheres for medical, scientific, and industrial applications.

Rembaum, Alan↗
NASA NTRS1988

In-reach and out-reach programs

Information is given in viewgraph form on in-reach and out-reach programs in in-space technology experiments. Information is given on thermal energy storage materials technology, industry/university in-space technology experiments, heat pipe performance, working fluid behavior, a tank pressure control experiment, spacecraft glow, the Mid-Deck Zero-Gravity Dynamics Experiment, and emulsion chamber technology.

Pyle, Jon S.↗
NASA NTRS1989

Holographic interferometry with an injection seeded Nd:YAG laser and two reference beams

The performance of twin injection seeded Nd:YAG lasers is compared with the performance of an argon-ion laser for recording dual-reference-beam holograms in AGFA 8E56 emulsion. Optical heterodyning is used to measure interference, and the results are expressed in terms of heterodyning signal level and intensity signal-to-noise. The Nd:YAG laser system is to be used for optical inspections of structures for cracks, defects, gas leaks, and structural changes.

Decker, Arthur J.↗
NASA NTRS1989

Expanding the utility of manned observations of earth - 70 mm film tests on the Space Shuttle

The Space Shuttle Orbiter provides opportunities for testing different ways to record terrestrial scenes using film. Such opportunities are limited by launch schedules and orbital parameters, properties of the Orbiter windows, available astronaut time and equipment stowage, and the necessity for safety qualification of equipment. To date, astronauts have accomplished several successful tests using color-infrared film, plane-polarizing filters, and a faster color emulsion, both on single 70-mm cameras and using a dual camera mount.

Amsbury, David L.↗
NASA NTRS1989

Online submicron particle sizing by dynamic light scattering using autodilution

Efficient production of a wide range of commercial products based on submicron colloidal dispersions would benefit from instrumentation for online particle sizing, permitting real time monitoring and control of the particle size distribution. Recent advances in the technology of dynamic light scattering (DLS), especially improvements in algorithms for inversion of the intensity autocorrelation function, have made it ideally suited to the measurement of simple particle size distributions in the difficult submicron region. Crucial to the success of an online DSL based instrument is a simple mechanism for automatically sampling and diluting the starting concentrated sample suspension, yielding a final concentration which is optimal for the light scattering measurement. A proprietary method and apparatus was developed for performing this function, designed to be used with a DLS based particle sizing instrument. A PC/AT computer is used as a smart controller for the valves in the sampler diluter, as well as an input-output communicator, video display and data storage device. Quantitative results are presented for a latex suspension and an oil-in-water emulsion.

Nicoli, David F.↗
NASA NTRS1989

JACEE long duration balloon flights

JACEE balloon-borne emulsion chamber detectors are used to observe the spectra and interactions of cosmic ray protons and nuclei in the energy range 1 to 100A TeV. Experience with long duration mid-latitude balloon flights and characteristics of the detector system that make it ideal for planned Antarctic balloon flights are discussed.

Burnett, T.↗