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At least 559 records · Page 31

A technique for making clean holes in metallic piping and components

Testing was conducted to develop a technique of providing clean holes in process piping or in a metal surface accessible from one side only without disassembling the system. The method was performed on sample pieces of piping and worked successfully with no contaminants being found on the inside of the pipe. The materials tested were Inconel 600, 304 stainless steel, Hastelloy X, and ASTM-A53 black steel. The technique was developed such that it could be done in the field with hand-held power tools and a portable tungsten inert gas welding machine.

Hecker, T. P.↗

Hot press and roll welding of titanium-6-percent-aluminum-4-percent-vanadium bar and sheet with auto-vacuum cleaning

Hot press butt welds were made in 0.5 in. diameter bar, and roll lap welds were made in 0.060 in. thick sheet of Ti-6A1-4V. For hot press welds made after auto-vacuum cleaning at 1800 F for 2 hours, weld strength and ductility equaled the parent metal properties. Only 5 minutes of pressing time were needed at 1800 F and 200 psi to make the hot press welds. Roll welds were made in sheet at 1750 F with only 10 percent deformation. The welds in the bar and sheet were metallurgically indistinguishable from the parent material.

Holko, K. H.↗

Electric contact phenomena in ultra clean and specifically contaminated systems.

Contact resistance has been used to characterize the processes of physical contact in metallic systems with ultra clean surfaces. The contact resistance versus load curves of iron and two cobalt alloys were used to demonstrate the existence of surface work hardening and interfacial creep during contact as well as the fracture characteristics of an interfacial junction as the load is removed. The presence of an adsorbed film of hydrogen or hydrogen ions on iron completely changes the contact process. A comparison of the contact resistance versus load data for ultra pure iron, an iron-cobalt alloy and a cobalt molybdenum-chromium was used to illustrate the effect of substrate mechanical properties on static adhesion and the ability to convert these data for the estimation of the dynamic coefficient of friction under the particular experimental conditions.

Keller, D. V., Jr.↗

Hydrogen halide cleaning of powder metallurgy nickel-20 chromium-3 thoria.

The Cr2O3 content of powder metallurgy nickel-20 chromium-3 thoria was reduced with atmospheres consisting of hydrogen plus hydrogen chloride (HCl) or hydrogen bromide (HBr). The nonthoria oxygen content or 'oxygen excess' was reduced from an initial amount of greater than 50,000 ppm to less than 100 ppm. Low temperatures were effective, but lowest oxygen levels were achieved with the highest cleaning temperature of 1200 C.

Herbell, T. P.↗

Interaction of sulfur dioxide and carbon dioxide with clean silver in ultrahigh vacuum.

It is shown that when a clean polycrystalline silver surface is subjected to sulfur dioxide at a pressure of 1 nanotorr, sulfur is chemisorbed to the silver. Heating the contaminated silver leads to an estimation of the minimum heat of desorption of 59 kcal/mol. Sulfur Auger peak height and relative function measurements of the surface during exposure show that adsorption occurs during 6 microtorr/sec exposure at 1 nanotorr.

Lassiter, W. S.↗

Code-regenerative clean-up loop for a ranging transponder

Digital processing system phase locks on received ranging signal and creates clean replica of received ranging code. System is broadly applicable to variety of terrestrial ranging problems, including oceanic navigation.

Hurd, W. J.↗

Friction-induced surface activity of some hydrocarbons with clean and oxide-covered iron

Sliding friction studies were conducted on a clean and oxide-covered iron surface with exposure of that surface to various hydrocarbons. The hydrocarbons included ethane, ethylene ethyl chloride, methyl chloride, and vinyl chloride. Auger cylindrical mirror analysis was used to follow interactions of the hydrocarbon with the iron surface. Results with vinyl chloride indicate friction induced surface reactivity, adsorption to surface oxides, friction sensitivity to concentration and polymerization. Variation in the loads employed influence adsorption and accordingly friction. In contrast with ethyl and vinyl chloride, friction induced surface reactivity was not observed with ethane and ethylene.

Buckley, D. H.↗

Oxygen and sulfur interactions with a clean iron surface and the effect of rubbing contact on these interactions

The interaction of sulfur and oxygen with an iron surface was studied with Auger spectroscopy analysis both statically and during sliding-friction experiments in a vacuum environment. Oxygen, hydrogen sulfide, methyl mercaptan, and sulfur dioxide were adsorbed to an iron surface. Results indicate that sulfide films formed on clean iron surfaces are completely displaced by oxygen. Hydrocarbons containing sulfur, such as methyl mercaptan, adsorb dissociatively. Less sulfur is adsorbed during sliding with hydrogen sulfide and methyl mercaptan than in the absence of sliding. With both oxygen and sulfur dioxide, sliding did not affect the amount of material adsorbed to iron.

Buckley, D. H.↗

Cleaning and activation of beryllium-copper electron multiplier dynodes.

Description of a cleaning and activation procedure followed in preparing beryllium-copper dynodes for electron multipliers used in sounding-rocket experiments to detect auroral electrons. The initial degreasing step involved a 5-min bath in trichloroethylene in an ultrasonic cleaner. This was followed by an ultrasonic rinse in methanol and by a two-step acid pickling treatment to remove the oxides. Additional rinsing in water and methanol was followed by activation in a stainless-steel RF induction oven.

Pongratz, M. B.↗

In situ sputter cleaning of thin film metal substrates for UHV-TEM corrosion studies.

A prerequisite for conducting valid corrosion experiments by in situ electron microscopy techniques is not only the achievement of UHV background pressure conditions at the site of the specimen but also the ability to clean the surface of the thin metal substrate specimen before initiation of the corrosive interaction. A miniaturized simple ion gun has been constructed for this purpose. The gun is small enough to be incorporated into an UHV electron microscope specimen chamber with hot stage in such a way as to permit bombardment of the substrate specimen while observing it by transmission electron microscopy TEM. It is shown that the ion beam generated is confined well enough to cause a sputtering removal of substrate material at a rate of approximately 5-10 A/min and to prevent the sputter deposition of contaminating material from the specimen holder.

Heinemann, K.↗

The experimental clean combustor program - Description and status

The experimental clean combustor program is a contract effort with primary objectives including the generation and demonstration of technology for development of advanced commercial CTOL aircraft engines with lower exhaust emissions than current aircraft, and the demonstration of this technology in full scale engines in 1976. The program is being conducted in three phases. These consist of screening of low pollutant combustors, refinement of the best combustors, and engine demonstration of the best combustors. Pollution goals are emission index values of 20 and 4 for carbon monoxide and unburned hydrocarbons respectively at engine idle conditions, and an oxides of nitrogen emission index level of 10 at engine takeoff conditions. Pollution reduction approaches which are being investigated include multiple burning zone combustors, investigations of improved fuel distribution, and preparation and the staging of combustor airflow.

Niedzwiecki, R. W.↗

Sticking probabilities for the adsorption of hydrogen on clean Ni/111/, Ni/100/, Ni sheet and evaporated Ni films

Determination of the sticking probability for hydrogen adsorption on clean Ni(111), Ni(100), polycrystalline nickel sheet, and polycrystalline evaporated nickel films, using a modification of the reflection detector technique of Horgan and King (1970) for metal films. The initial sticking probability for hydrogen adsorption on a nickel film at 300 K by the proposed method is found to be 0.25 in comparison to 0.35 for hydrogen adsorption on a nickel film using the reflection detector technique. Also, the sticking probabilities on smooth single-crystal (111) and (100) planes and polycrystalline sheets are found to be lower than those on the rougher polycrystalline nickel films.

Horgan, A. M.↗

Aerodynamic analysis of several high throat Mach number inlets for the quiet clean short-haul experimental engine

The results of an analytical study to investigate internal and external surface Mach numbers on several inlet geometries for possible application to the nacelle of the Quiet Clean Short-Haul Experimental Engine (QCSEE) are presented. The effects of external forebody geometry and internal lip geometry were illustrated at both low-speed and cruise conditions. Boundary-layer analyses were performed on several geometries to determine if lip flow separation might exist. The results indicated that inner-surface Mach number level and gradient could be reduced with inlets at a 50 deg incidence angle by blunting the external forebody geometry. The external Mach numbers at cruise conditions indicated that a compromise in the external forebody bluntness might be required to satisfy both low-speed and cruise conditions. For a fixed value of bluntness parameter, no lip flow separation was indicated for the 1.46- and 1.57-area-contraction-ratio inlets at low-speed conditions. However, a lip separation condition was obtained with the 1.37-contraction-ratio inlet. The QCSEE nacelle design takeoff operating condition (incidence angle of 50 deg and free-stream Mach number of 0.12) resulted in higher peak surface Mach numbers than the design crosswind (incidence angle of 90 deg and free-stream Mach number of 0.05) or static condition.

Albers, J. A.↗