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NASA NTRS2023

The Effects of Impactor Shape on the Compression After Impact Strength of Carbon/Epoxy Face Sheet Foam Core Sandwich Structure

This study presents experimental results of compression after impact (CAI) strength testing of foam core sandwich structure with carbon/epoxy face sheets impacted at three different energies with either a blunt or sharp tip impactor. The impact energies used were chosen to span the barely visible impact damage (BVID) thresholds for the sharp (4.1 J) and blunt (12.9 J) impactors with an impact energy approximately halfway between these (8.1 J) also used. While most impact testing on composites utilize a hemispherical (blunt) impactor, actual damage to a part may be due to an object impacting the part that is not blunt, but sharp and the impact response and resulting CAI strength values may be different for a given impact energy level. In this study, with regards to the impact response, the sandwich specimens showed larger transverse displacements (by about a factor of two) during the impact event when impacted by a sharp impactor versus a blunt impactor. The maximum load of impact was larger for the blunt impactor by about a factor of three. The barely visible impact damage (BVID) threshold energy was lower by about a factor of three for the sharp impactor. The absorbed energy of impact was higher for the sharp impactor. The CAI strength results showed that the sharp impactor gave lower average CAI strength values at the lowest impact energy level used, slightly lower average CAI strength values for the medium impact energy used and about the same average CAI strength values for the highest impact energy used.

sandwich structure↗

NASA NTRS2020

Additive Manufactured Ultra-Fine Lattice Structures for Propulsion Catalysts

Traditional mono-propulsion catalysts consist of coated ceramic or graphite foams that possess anisotropic mechanical and fluid properties limiting design, cost, availability, and operational use. Ultra-fine lattice structures are repeating unit cells with ligament thickness as small as 100 μm produced via Additive manufacture (AM). These lattice structures have the potential to replace coated foams used in a mono-propellant system catalysts. AM ultrafine lattice structures are designed to mimic the operational intent of coated foams but with improved design flexibility, compressive strength, and flow behavior printed from into a single part directly from the preferred platinum metal alloy. The investigation objective was to conduct feasibility studies of AM ultra-fine lattice structures capable of replacing coated foams with superior functionality. NASA MSFC identified desired lattice characteristics and created designs while EOS developed optimized laser powder bed fusion AM parameters to manufacture Ti6Al4V and tungsten specimens. Optimized designs, computational tools, AM parameters, and post-process methods were developed. Specimens underwent x-ray microfocus CT, metallographic inspection, compression testing, and flow testing. Results demonstrate that AM ultra-fine lattices improved geometric and performance repeatability with the potential for significantly increased availability while decreasing cost and lead time.

Omar R Mireles↗

NASA NTRSDate not supplied

Additive Manufacture of Ultra-Fine Lattice Structures of Green Propulsion Catalysts

Omar Mireles↗

NASA NTRS1992

Mechanisms of compressive failure in woven composites and stitched laminates

Stitched laminates and angle interlock woven composites have been studied in uniaxial, in-plane, monotonic compression. Failure mechanisms have been found to depend strongly on both the reinforcement architecture and the degree of constraint imposed by the loading grips. Stitched laminates show higher compressive strength, but are brittle, possessing no load bearing capacity beyond the strain for peak load. Post-mortem inspection shows a localized shear band of buckled and broken fibers, which is evidently the product of an unstably propagating kink band. Similar shear bands are found in the woven composites if the constraint of lateral displacements is weak; but, under strong constraint, damage is not localized but distributed throughout the gauge section. While the woven composites tested are weaker than the stitched laminates, they continue to bear significant loads to compressive strains of approx. 15 percent, even when most damage is confined to a shear band.

Cox, B. N.↗

NASA NTRSDate not supplied

Additive Manufactured Ultra-Fine Lattice Structures for Propulsion Catalysts

Traditional mono-propulsion catalysts consist of coated ceramic or graphite foams that possess anisotropic mechanical and fluid properties limiting design, cost, availability, and operational use. Ultra-fine lattice structures are repeating unit cells with ligament thickness as small as 100 μm produced via Additive manufacture (AM). These lattice structures have the potential to replace coated foams used in a mono-propellant system catalysts. AM ultra-fine lattice structures are designed to mimic the operational intent of coated foams but with improved design flexibility, compressive strength, and flow behavior printed from into a single part directly from the preferred platinum metal alloy. The investigation objective was to conduct feasibility studies of AM ultra-fine lattice structures capable of replacing coated foams with superior functionality. NASA MSFC identified desired lattice characteristics and created designs while EOS developed optimized laser powder bed fusion AM parameters to manufacture Ti6Al4V and tungsten specimens. Optimized designs, computational tools, AM parameters, and post-process methods were developed. Specimens underwent x-ray micro-focus CT, metallographic inspection, compression testing, and flow testing. Results demonstrate that AM ultra-fine lattices improved geometric and performance repeatability with the potential for significantly increased availability while decreasing cost and lead time.

Omar R Mireles↗

DOE OSTI2020

Progressive collapse analysis of stiffened panel structure with consideration of actual welding distortion and residual stresses

To date, inclusion of welding distortion and residual stresses in determining the strength of marine structures is based on empirical formulations due to welding complexity. In this study, a more feasible numerical model was developed from the perspective of inherent strain theory. The accuracy of this simplified numerical model was confirmed by transient thermo-elastic–plastic finite element analysis using a novel dynamic mesh refining and iterative substructure method which is 50 times faster than conventional finite element method. Welding distortion by the two numerical approaches was validated with experimental measurement. The collapse analyses indicated that the inherent strain model predicted a compressive strength and load-displacement curve with high accuracy, as validated by the transient thermo-mechanical model. The global stiffness and the ultimate strength of the welded structure would be overestimated by about 22% if no welding effects were considered. The proposed computation procedure for determining the ultimate strength of welded structures is accurate, simple, and practical and enables improvement of ultimate strength through optimization of welding joint design to reduce the welding residual stress and distortion.

Huang, Hui↗

DOE OSTI2022

Novel processing route for design and manufacturing of metal toughened nanoceramics: Al–Al 2 O 3 nanocermets

Monolithic alumina is a highly brittle ceramic with a very low fracture toughness, making it an unreliable material for mechanical and structural applications. Ceramic-metal composites (cermets) are the subject of intensive interest to obtain materials which can address the intrinsic brittleness of ceramics without compromising their high strength and light weight. In the present investigation, aluminium-alumina (Al–Al 2 O 3 ) nanocermets were developed. The nanocermets possessed the toughness of Al phase and the strength of reinforced nano Al 2 O 3 particles. Here, the nanocermets green bodies were prepared such that upon sintering each adjacent Al 2 O 3 grain was conformally coated with a continuous Al film. Mechanical milling via a combination of cryo-milling and ball-milling was used to prepare Al–Al 2 O 3 nano-powder mixture. Spark plasma sintering was used to consolidate the green nanocermets. Results show that specimens prepared from 35 h milled powders exhibited superior mechanical properties as compared to other nanocermets, with an improvement in microhardness, elastic modulus, compressive strength, and flexural strength by 88%, 78%, 69% and 40% with respect to sintered pure Al. The indentation toughness of 35 h milled nanocermet showed an increment of 12.5% with respect to sintered pure Al 2 O 3 . Characterization techniques such as XRD, SEM, HR-TEM, X-ray tomography were employed to investigate the phase evolution and structural morphology, while FEM simulations were performed for understanding the crack propagation mechanisms in nanocermets.

36 MATERIALS SCIENCE↗

DOE OSTI2014

Injection repair of carbon fiber/bismaleimide composite panels with bisphenol E cyanate ester resin

Resin injection of bisphenol E cyanate ester, a low viscosity resin that cures into a high temperature thermoset polymer, is investigated as a reliable repair method to restore strength and stiffness in delaminated carbon fiber/bismaleimide composites used in aircraft panels. The influence of temperature on the viscosity of the uncured resin was measured to optimize the injection conditions for high resin infiltration into the delaminations. The repair efficiency of the resin was evaluated by varying the panel thickness and the method by which the delamination damage was created in the composite specimens. Ultrasonic scanning (C-scan), flash thermography images, and cross-section analysis of repaired panels revealed excellent resin infiltration into the damaged region. Evaluation of mechanical repair efficiency using both bending stiffness and in-plain compressive strength of the composite panels as the repair metrics showed values exceeding 100%.

36 MATERIALS SCIENCE↗

NASA NTRS1983

Passive Orbital Disconnect Strut (PODS 3), structural and thermal test program

A test program is undertaken to verify that the lifetime of a shuttle launchable dewar can be increased by using passive orbital disconnect struts (PODS). A detailed design is performed on the cold end (PODS-III) portion of the strut. Structural analysis of the thin-wall fiberglass tube allows selection of the optimum winding angle and tube dimensions. Structural tests on the thin-wall fiberglass tube measure both the tension and compression modulus at ambient and LN2 temperatures, the radial deflection versus side load, and the ultimate compression strength of the tube at LN2 temperature. The thermal expansion of the fiberglass tube plus Invar is also measured down to 78 K. The axial gap at the wedge portion of the stem is set based on these data. The PODS-III test article parts are fabricated and assembled using a detailed assembly procedure. The thermal conductants in the orbital configuration was measured for body temperatures between 5 and 40 K. This temperature range covers the predicted ground hold and orbit temperatures for vapor-cooled supports. The test results are then compared with heat leak values predicted before the test began. Side load, axial compression load, and tension load tests conclude the test program.

Parmley, R. T.↗

DOE OSTI2023

Direct Ink-Write Printing of Ceramic Clay with an Embedded Wireless Temperature and Relative Humidity Sensor

This research presents a simple method to additively manufacture Cone 5 porcelain clay ceramics by using the direct ink-write (DIW) printing technique. DIW has allowed the application of extruding highly viscous ceramic materials with relatively high-quality and good mechanical properties, which additionally allows a freedom of design and the capability of manufacturing complex geometrical shapes. Clay particles were mixed with deionized (DI) water at different ratios, where the most suitable composition for 3D printing was observed at a 1:5 w/c ratio (16.2 wt.%. of DI water). Differential geometrical designs were printed to demonstrate the printing capabilities of the paste. In addition, a clay structure was fabricated with an embedded wireless temperature and relative humidity (RH) sensor during the 3D printing process. The embedded sensor read up to 65% RH and temperatures of up to 85 °F from a maximum distance of 141.7 m. The structural integrity of the selected 3D printed geometries was confirmed through the compressive strength of fired and non-fired clay samples, with strengths of 70 MPa and 90 MPa, respectively. This research demonstrates the feasibility of using the DIW printing of porcelain clay with embedded sensors, with fully functional temperature- and humidity-sensing capabilities.

42 ENGINEERING↗

DOE OSTI2022

Low Cost, High Volume, Carbon Fiber Precursor for Plasma Oxidation

Light weighting with carbon fiber is critical to improving the energy efficiency of wind turbines, airplanes, and automobiles, but the high cost of carbon fiber continues to limit market growth and applications. Half of this cost is in the raw materials. For the carbon fiber market to reach the next level of adoption, the cost of both the raw materials and conversion must be reduced. This project considered the combination of low-cost, textile-grade precursors combined with the increased efficiency of plasma oxidation to greatly reduce the cost of carbon fiber. The primary objective of this project was to make industrial-grade carbon fiber (550 ksi tensile strength, 35 Msi tensile modulus) from textile-grade PAN precursors, something that cannot be achieved with conventional oxidation and to date has not been achieved with any technology. To accomplish this, the project team iteratively optimized the process conditions in the plasma oxidation and carbonization stages to maximize the tensile properties of the resultant carbon fibers. This involved implementing experimental designs for both stages, whereby process conditions (e.g. temperature) were varied and correlated to fiber properties. Samples of oxidized PAN fibers (OPFs) were prepared using a small pilot-scale plasma oxidation oven at 4XTechnologies (4XT). The thermal, chemical, and physical properties of OPF samples were analyzed by the University of Tennessee (UTK) and Oak Ridge National Laboratory (ORNL). The OPF samples were then converted to carbon fiber by subsequent low- and high-temperature carbonization using a lab-scale furnace at ORNL. The resultant carbon fibers were tested for tensile strength also at ORNL, and the results were fed back into the experimental design. Of the hundreds of carbon fiber samples produced over the course of the project, the best sample had an average break strength of 479 ksi and modulus of 33 Msi. While the best tensile properties achieved fell short of the final project targets of 550 ksi for break strength and 35 Msi for modulus, the team demonstrated the potential to produce industrial-grade carbon fiber using textile-grade precursors. The best performing fiber samples had tensile properties that are 87% of the goal for tensile strength and 94% of the goal for tensile modulus. With additional optimization work, it is likely that the targets could be achieved, since only a fraction of the process parameter space was explored during this project. 4XT and its affiliate (4M) have already secured funding through private equity, and there is a CRADA (Cooperative Research and Development Agreement) project currently underway with the Carbon Fiber Technology Center (CFTF) at ORNL to continue this research. Additionally, while not an original goal of the project, the carbon fibers for most samples had diameters >8.5μm. This is considerably larger than commercially available carbon fiber products, which can impart unique properties to the composites (e.g. increased compressive strength) and decrease manufacturing costs even further. Moreover, these fibers were oxidized with plasma oxidation using residence times ranging <60mins, which would be considered fast for normal diameter fibers, but it is as much as 5x faster when factoring in the diameter of the fibers.

36 MATERIALS SCIENCE↗

DOE OSTI2022

Printable Fiber Reinforced Cement Composites – Feasibility Study

Additive manufacturing is enabling the manufacturability of structures with previously unattainable complexity or functionality, and there is growing interest in additive manufacturing of “printed” concrete structures. The focus of this Phase 1 Technical Collaboration (TC) project was to evaluate feasibility of printing hybrid cement composite structures reinforced with textile carbon fibers (tCF). This project leverages other (non-IACMI) projects on cement formulation and printing process development, as well as on the production process for tCF. This project’s primary focus was to explore cement composite mix design with textile carbon fibers to be manufactured by MonteFibre (TC partner) and evaluate suitable fiber-matrix interface or sizing for cement composites working with Michelman (TC Partner). This project supports IACMI’s goal of reducing the cost and embodied energy of carbon fiber composites. Cost is one of the fundamental challenges to carbon fiber reinforced cement composites. Cement is an extremely inexpensive material (approximately $\$$0.05/lb). Adding 1 wt% of conventional carbon fiber to cement quadruples its cost. Therefore, the need to use low-cost carbon fiber and ensure that the additional cost of the carbon fiber has a greater cost benefit to the final product. This was the first preliminary evaluation to integrate tCF reinforcement in cement composites, and such potential tCF utilization should significantly reduce materials cost. Cement composite production is energy and emissions intensive, thus by strengthening it less material will be required. Hence, the embodied energy and production time of the resulting structures will be reduced. Additionally, integrating these new materials into additive processes can enable selective use of the material in high load or stress areas. It is noteworthy that past work in this field of fiber reinforced cement composites did not consider the optimization of fiber-matrix interface using suitable sizing. Carbon fiber reinforcement offers potential added benefits of thermal conductivity (which affects cure rate) and flow behavior that could provide opportunities for site specific utilization of carbon fiber on hybrid cement structures (e.g. use the fiber reinforcement on outer surfaces to enhance strength and modulus and then infiltrating the internal structures with conventional concrete). MonteFibre was the industry lead and planned on supplying the tCF for this project. However, during the short Phase-1 duration of this project, MonteFibre was unable to produce tCF for this project due to manufacturing plant being off-line throughout the course of the project. The project team decided to pursue an alternate option which involved demonstrating printable concrete with steel fibers by the ORNL lead, Dr. Brian Post. The University of Tennessee collaboration team focused on evaluating the suitable chemical sizing for carbon fibers working with Michelman and also developed methods for material characterization of cement-based composites to evaluate the material response for compression, shear, flexure, and tension. The two milestones for University of Tennessee, Knoxville were realized related to identification of one sizing suitable for carbon fiber reinforced cement composite and developing data associated with mechanical behavior of unreinforced (neat) and carbon fiber reinforced cement composites. ORNL could not complete the task of carbon fiber reinforced printed cement composites due to the reasons mentioned earlier, but was able to replace tCF with steel fibers to demonstrate the feasibility of printing with fiber reinforced cement composites. The Project team reviewed possible sizing chemistry available in collaboration with Michelman for use on carbon fiber reinforcement in cement composites and concrete applications. Our initial goal was to identify a sizing most promising for formulation with textile carbon fibers (tCF) to deliver excellent mechanical properties in composite material state. Since tCF was not available for this project as originally envisioned, the team continued this task to identify a suitable sizing for carbon fiber applications by applying such sizing to lower cost carbon fibers currently available commercially from Zoltek called Panex fibers. At a future time this can be optimized for textile carbon fibers from Montefibre. The bulk of previous work on carbon fiber reinforced cement has neglected the importance of fiber-matrix adhesion on mechanical properties of the cement composite and identifying this missing link was an important accomplishment for future research. Tensile behavior of fiber reinforced concrete is important to evaluate in order to realize the dream of concrete products that do not need reinforcing steel. Important sample preparation and testing procedures were addressed in this study and it was concluded that substantial improvements in tensile behavior, without compromising compressive strength, and improved ductility can result from the use of carbon fiber reinforcement.

36 MATERIALS SCIENCE↗

NASA NTRSDate not supplied

Impact Experiments into Granular Targets Containing Solitary Blocks of Varying Strength and Size

Crater scaling relationships provide a means to correlate dimensions of laboratory-scale impact experiments to naturally formed craters at planetary scales. For relatively larger impact events, where gravity is the dominant arresting force against crater growth, these scaling relations are comparatively simple. For smaller craters, however, the target properties have increasing influence over the cratering process. Further complexities are easily envisaged when considering realistic surfaces that contain small-scale heterogeneities in cohesive strength, density, porosity, friction, as these properties will each have unequal effects on the resultant crater morphometry. Even when produced under controlled laboratory conditions, understanding (and controlling) the entire relevant parameter space is daunting, and deconvolution of the relevant contributors can be complicated even in the best-case scenario. To this end, we have begun an extensive series of impact experiments that will provide a nascent framework that will aid in the interpretation of craters observed on complex natural surfaces throughout the solar system. To start with the simplest configuration, experiments were performed with cylindrical PVC buckets that were filled with quartz sand and contained a single cubic block of synthetic sandstone. The blocks varied in size (14-33 mm) and unconfined compressive strength (0.5-7.4 MPa) and were placed in/on the sand along the trajectory of the incoming impactor and buried to different depths. All experiments were conducted using the vertical gun located in the Experimental Impact Lab at NASA Johnson Space Center with alumina projectiles that were accelerated to ~1.53 km s^-1 under a vacuum of 1 torr. After the impact, target containers were removed from the chamber are morphometric data were extracted by using a Peel 2 3D-scanner in combination with the open-source software, CloudCompare. Initial results show that block strength is a secondary effect on crater diameter and depth, but when at least one edge of the block is exposed and the surface (partial burial) the strength will dictate the number of surviving block fragments around the crater, as well as how much disrupted block material is retained within the crater walls.

Christopher J. Cline II↗

DOE OSTI2023

A high-strength precipitation hardened cobalt-free high-entropy alloy

Recent studies on precipitation-hardened high-entropy alloys (HEAs) demonstrate their high strength and thermal stability, making them promising materials for high-temperature structural applications such as nuclear reactors. However, many existing HEAs contain cobalt (Co), which is unsuitable for nuclear applications because of the long-term activation issue of Co. Co is also expensive and considered a critical material for other applications. Therefore, it is desired to exclude Co from the composition. A Co-free (Fe 0.3 Ni 0.3 Mn 0.3 Cr 0.1 ) 88 Ti 4 Al 8 HEA was developed and studied in this work. In contrast to previous Co-free HEAs, this alloy is close to equiatomic in its composition and promises a more pronounced high-entropy effect. Scanning electron microscopy, transmission electron microscopy, atom probe tomography, and synchrotron-based, high-energy X-ray diffraction were used to characterize this alloy and revealed a complex four-phase structure, with an FCC matrix, γ’ precipitates, and a network of B2 and χ phase particles. This structure granted 2151 MPa compressive strength and good thermal stability, but with limited ductility and slow precipitation kinetics. A strengthening analysis of the alloy shows that the B2 and χ provided the most significant strengthening contribution, adding 312 MPa and 788 MPa respectively. Furthermore the strengthening effect from the nanoscale γ' is also considerable, adding 608 MPa in total. This study lays the foundation for the continued development of high-strength Co-free HEAs with improved and satisfactory ductility.

36 MATERIALS SCIENCE↗

NASA NTRS1993

Atmospheric breakup of a small comet in the Earth's atmosphere

The aerodynamic stresses can lead to the deformation and even to destruction of the meteoroids during their flight through the atmosphere. The pressure at the blunt nose of the cosmic body moving at very high speed through the dense layers of the atmosphere may be much larger than the tensile or the compressive strength of the body. So the usage of the hydrodynamics theory is validated. The estimates show that the transverse velocity of the substance of the body U is of the order of (rho(sub a)/rho(sub o))(sup 1/2)V where V is the velocity of the body and rho(sub o) is its density, rho(sub a) is the density of the atmosphere. The separation of the fragments is larger than the diameter of the body D if D is less than D(sub c) = 2H(square root of rho(sub a)/rho(sub o)), where H is the characteristic scale of the atmosphere. For an icy body one obtains U = 1/30(V) and critical diameter D(sub C) = 500 m. The process of the disintegration of the body is still not fully understood and so one can use the numerical simulation to investigate it. Such simulations where conducted for the Venusian atmosphere and the gaseous equation of state of the body was used. For the Earth atmosphere for the velocity V = 50 km/s the pressure at the blunt nose of the body is 25 kbar, and is of the order of bulk modulus of compressibility of the water or ice. The realistic EOS of water in tabular form was used. It was assumed that the initial shape of the body was spherical and the initial diameter D(sub o) of the body is 200 m and so it is smaller than the critical diameter D(sub C). The initial kinetic energy of the icy body is equivalent to the energy of the explosion 1200 Mt of TNT. The results of the simulation of the deformation of the body during its vertical flight through the atmosphere and during its impact into the ocean are presented.

Teterev, A. V.↗

NASA NTRSDate not supplied

Using Controlled Impact Experiments to Understand the Effects of Cohesive Blocks on the Cratering Process

When considering large-scale impact events that occur in the gravity-regime, smallscale target heterogeneities (on order of the projectile diameter) are anticipated to have a minimal effect on the cratering process and are therefore not considered in scaling relations [1-3]. Such heterogeneities and other details of the target's strength and structure, however, become increasingly influential as the magnitude of the impact decreases [4]. At the scale of craters forming mostly in regolith on the Moon (< a few meters), for example, target properties such as cohesive strength, density, porosity, and friction have more leverage than gravity to influence the resultant crater dimensions [5]. Further complications beyond just target properties can manifest in many forms, such as subsurface layers [6]; the presence of random, competent blocks [7]; buried lenses of impact melt; and/or pockets of regolith compacted or indurated to varying degrees by previous impacts. Summing the total effect of target properties and any additional heterogeneities for integration into scaling relations is not straightforward, as each individual parameter will have unequal, and so far, unquantified, effects on the final crater. Even when craters are produced under a best-case scenario of controlled laboratory conditions, understanding the entire relevant parameter space can be a formidable task, and deconvolution of all the contributing factors can be a complex undertaking. To begin the process of quantifying such effects, we are conducting an extensive series of impact experiments to build a framework for the interpretation of craters observed on the characteristically complex surfaces throughout the solar system. Here we present the first, and simplest, configuration to be examined in this multi-year experimental campaign: one in which solitary, cohesive blocks are placed in the path of the projectile’s trajectory at different burial depths in granular, sand targets. Among the variables to be investigated in this configuration are the influence of block size, compressive strength, and burial depth.

impact crater↗

NASA NTRS2024

The Effects of Peel Ply on the Damage Tolerance Characteristics of the Space Launch System (SLS) Payload Adapter Fitting (PAF)

A payload adaptor fitting (PAF) has been manufactured at NASA’s Marshall Space Flight Center (MSFC) in support of the Space Launch System (SLS) program. This structure is essentially a large cone made up of eight curved “lobes” that are joined together to form the cone. The lobes were manufactured via automated fiber placement (AFP). The PAF will carry predominantly compressive loads thus compression strength will be the focus of this study. The lobes are sandwich structure made with aluminum honeycomb core and carbon/epoxy face sheets. The lobes will be inserted into metallic rings at the top and bottom of the cone to form the full cone. Both front and back exterior surfaces of each lobe have a plain weave fabric placed at ±45⁰ to the vertical direction to help prevent fiber “breakout” during drilling. The face sheet of each lobe is thickest at the top and plies are dropped as the cone reaches the main acreage in the bottom section of the cone. The entire structure used resin impregnated peel ply that, once removed, supplies a good bonding surface for secondary bonding steps. The peel ply can be removed either directly after cure, or just before any bonding operation. Since foreign object impact can occur to the structure at any time during its life, damage tolerance of the PAF structure both with and without peel ply needed to be addressed because a previous study, albeit with limited data, showed some significant differences in damage tolerance whether the peel ply was present or not [1]. A literature search showed no results for comparing impact damage on composite laminates with and without peel ply. Load versus deflection of impact curves, visual damage, dent depth, damage as ascertained by thermography and cross-sectional microscopy were evaluated as part of the damage resistance of the structure. Compression After Impact (CAI) was performed to assess damage tolerance. The impact tests were conducted on representative specimens both with and without the peel ply present.

Sandwich Structure↗

DOE OSTI2021

Geodyn Material Library: Pseudocap models for dry porous tocks

This report describes the second edition of the Pseudocap Strength models for porous rocks implemented in GEODYN material library. The first model was developed in 2007 and calibrated for concrete. Then, the model parameters were calibrated based on triaxial tests reported for limestones and sandstones of various porosities. In these models some key parameters were chosen as functions of the reference porosity,Φ. Since then multiple modifications were implemented in the model, therefore, it has been recalibrated for some common porous materials such as limestones, sandstones, alluvium, tuffs and granite. Two types of models are described in this repot. The first type (called Pseudocap Model or PM) is for rocks from a specific location. Parameters were calibrated for several specific geologic materials. The second type (called Generic Pseudocap Model or GPM) is useful for the sites where only basic information (rock type, porosity) is available. Generic models include built-in correlations between porosities and other mechanical properties observed for certain rock types. The models of both types were validated by comparing not only to quasi-static triaxial tests for these materials but also to shock Hugoniot data and spherical explosion data for some materials. All models were derived in the frame of isotropic plasticity. They are designed to be used in explicit finite element/difference codes. Tangent stiffness tensor is not provided but can be calculated numerically for the model to be used in implicit finite element codes. For an isotropic material the stress can be decomposed into volumetric and deviatoric parts. The volumetric part is modeled using an Equation of state (EOS) which calculates the pressure and the bulk sound speed as functions of the internal specific energy and density. Here a simple, Mie-Gruneisen EOS is presented, but tabulated EOS (LEOS) provided by the library can be used as well. The stress is limited by the yield surface which depends on three invariants of the stress tensor and specific internal energy. In addition, to capture the strain-rate dependence a simple multiplier is used for the yield surface which depends on the equivalent plastic strain rate. The failure surface (the ultimate yield, Y f , defined later) is chosen in the Hoek-Brown form, commonly used in rock mechanics. It includes measurable parameters such as Unconfined Compressive Strength (UCS) as well as scale parameters characterizing the quality of the rock such as GSI (Geologic Strength Index). Thus, even though the model is calibrated for small samples it offers a way to extrapolate the strength to the field scale using geological characterization of the rock mass. The model captures effects of brittle-ductile transition in rocks by introducing a cap multiplier to the yield function. The rate of dilatancy (bulking) is proportional to the slope of the yield surface affected by the cap. Therefore, it takes place only at low confinements when the pressure is less than the brittle-ductile transition pressure, P BD . On the contrary, the porous compaction takes place at pressures higher than P BD . The cap moves as the porosity is compacted or new porosity is generated due to dilatancy. The porous compaction is modeled using an evolution equation which includes deviatoric stress so that the onset of compaction corresponds to the cap surface. The model captures effects of shear-enhanced compaction which is an important for porous rocks. Section 2 describes the modeling framework and Section 3 presents the model calibration procedure. Section 4 compares experimental data for various rocks versus model predictions. The model parameters used for this comparison are given in Appendix. The files with material constants are available with the latest GEODYN material library distribution.

58 GEOSCIENCES↗