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NASA NTRSDate not supplied

Updated assessment of TROPOMI NO2 and HCHO columns using airborne spectrometers during the MOOSE and TRACER-AQ field campaigns

Airborne spectrometer data offers the opportunity to evaluate satellite product performance without the impact of subpixel heterogeneity between the different satellite and ground-based measurement footprints. Previous measurements during the Long Island Sound Tropospheric Ozone Study were used to evaluate TROPOMI’s v1.3 NO2 product and found very strong relationships (r2=0.96) between the airborne spectrometer and TROPOMI with a systematic low bias mostly attributed to the coarse a priori profile assumption within the standard TROPOMI retrieval. This presentation will update that analysis using the most up-to-date version 2 TROPOMI NO2 product as well as expand analysis to the HCHO product. In summer 2021, NASA GeoCAPE Airborne Simulator (GCAS) collected measurements over southeast Michigan/western Ontario for the Michigan-Ontario Ozone Source Experiment (MOOSE) and Houston, Texas during the TRacking Aerosol Convection ExpeRiment – Air Quality (TRACER-AQ). Flight strategies for both deployments included repeated systematic sampling over common areas of interest coinciding with TROPOMI. During these flights, GCAS NO2 tropospheric columns are available at 250 m x 560 m resolution. Preliminary evaluation of GCAS NO2 retrievals with Pandora spectrometer data in Houston, Texas (3 sites) shows a median percent difference of 1.4% with an interquartile range of -15.5-14.9% (r2=0.72). Column HCHO was also retrieved at a slightly coarser resolution in Houston, Texas (750 m x 1680 m) showing distinct spatial patterns associated with secondary production through the oxidation of VOCs downwind of industrial facilities. Comparison to Pandora HCHO showed a low bias of ~25% (r2=0.29) with further investigation needed to identify the cause for this bias. This presentation will share how the GCAS/Pandora/TROPOMI NO2 and HCHO intercompare and will also extend analysis toward thinking about how these assets will contribute to the validation of future geostationary observations.

Laura Judd↗

NASA NTRSDate not supplied

The Third Flight of the Marshall Grazing Incidence X-Ray Spectrometer (MaGIXS-3)

The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is the first X-ray slitless imaging spectrograph sounding rocket instrument designed to observe spectrally dispersed soft X-ray images of the solar corona over a wide field-of-view. During the first flight of MaGIXS (MaGIXS-1), occurred on 30 July 2021, several emission lines from coronal structures including X-ray bright points were observed. Further, MaGIXS-1 analysis also demonstrated the successful inversion of overlappograms using robust unfolding algorithms. Given the demonstrated success of MaGIXS-1, the second flight of the instrument with a simplified optical design, MaGIXS-2, is scheduled for 2024 to observe high temperature diagnostic emission lines. Results from MaGIXS-1 discovered dominant missing emission lines near 15A, arising from relatively cool plasma that peaks around 2 MK. This wavelength region hosts several closely spaced satellite lines of Fe XVII, Fe XVI and Fe XV ions, which are expected to be enhanced at lower temperatures and are currently unmodeled in the CHIANTI atomic database. This wavelength region offers one of the most unique diagnostics to measure electron temperature, as well as signatures of equilibrium state of the plasma in active regions, which has not been studied so far. The goal of MaGIXS-3 mission is the to determine coronal heating parameters, such as the spatial and temporal properties of coronal heating events, by measuring discriminating observations, such as electron temperature, effective temperature, density, abundance, and departures from thermal equilibrium of the plasma, by observing the Sun in the SXR wavelength range. To meet this goal, the MaGIXS instrument will be upgraded with a new X-ray telescope mirror that will provide higher spatial and spectral resolution and throughput, allowing for spectral lines to be observed at the relevant spatial and temporal scales. In addition, MaGIXS-3 will also carry The Resolving Inversion Context X-ray Spectrometer (TRICXS), a high dispersion Bragg crystal spectrometer to spectrally resolve the lines near 14.9 to 15.9A, critical to unlock the full diagnostic potential of this wavelength range. Here we will present the preliminary concept design of MaGIXS-3 and discuss the potential observations.

X-ray Imaging↗

NASA NTRSDate not supplied

The Next Generation Marshall Grazing Incidence X-Ray Spectrometer (MaGIXS) Sounding Rocket Experiments

The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is a sounding rocket experiment that carries an X-ray slitless imaging spectrograph to observe spectrally dispersed soft X-ray (SXR) images of the solar corona over a wide field-of-view. The first flight of MaGIXS occurred on 30 July 2021, during which several emission lines from coronal structures including X-ray bright points were observed. Analysis of MaGIXS-1 data demonstrated the application of new inversion techniques and opened a new arena of inverting complex spectroheliogram data, which has spatial-spectral information overlapped. The second flight of MaGIXS, with a simplified optical design, is scheduled for 2024. The goal of MaGIXS-2 is to observe high temperature diagnostic emission lines within an active region core. MaGIXS-1 discovered dominant missing emission lines near 15Å wavelength region, which hosts several closely spaced satellite lines of Fe XVII, Fe XVI, and Fe XV ions, arising from relatively cool plasma that peaks near 2MK. These lines are expected to be enhanced at lower temperatures and offers one of the most unique diagnostics to measure electron temperature, as well as signatures of equilibrium state of the plasma in active regions, which has not been studied so far. The science goal of the third sounding rocket flight of MaGIXS is to determine coronal heating parameters, such as the spatial and temporal properties of coronal heating events, by measuring discriminating observations, such as electron temperature, effective temperature, density, abundance, and departures from thermal equilibrium of the plasma, by observing the Sun in the SXR wavelength range. For this, the MaGIXS instrument will be upgraded with a new X-ray telescope mirror that will provide higher spatial and spectral resolution and throughput, allowing for spectral lines to be observed at the relevant spatial and temporal scales. In addition, MaGIXS-3 will also carry The Resolving Inversion Context X-ray Spectrometer (TRICXS), a high dispersion Bragg crystal spectrometer to spectrally resolve the lines near 15Å, critical to unlock the full diagnostic potential of this wavelength range. Here we will present the preliminary concept design of MaGIXS-3 and discuss the potential observations.

X-ray Imaging↗

NASA NTRS2024

The Peregrine Ion Trap Mass Spectrometer (PITMS) Investigation Development and Pre-Flight Planning

The Peregrine Ion Trap Mass Spectrometer (PITMS) is a mass spectrometer instrument that operated during the Astrobotic Peregrine Mission-1 as part of the NASA Commercial Lunar Payload Services (CLPS) initiative. This paper describes the instrument and investigation design, development, and planning conducted by the PITMS team consisting of a successful partnership between NASA Goddard Space Flight Center (GSFC), The Open University (OU), NASA, and ESA. PITMS was designed to measure the abundance and temporal variability of volatile species in the near-surface lunar exosphere from a landed platform on the lunar surface. The PITMS instrument consisted of an ESA-provided Exospheric Mass Spectrometer (EMS; including sensor, electronics, controller, power supply boards) and a GSFC wrapper that provided structural elements, thermal control, and a deployable dust cover. PITMS was designed to operate as a passive sampler, where ambient gases would enter PITMS through an aperture, diffuse around the mass analyzer cavity, become ionized by electron impact and trapped in a radiofrequency field, then sequentially released to a detector to build a mass spectrum. PITMS was capable of measuring species with a massto-charge ratio (m/z) from 10 to 150 Da, with a mass resolution of approximately 0.5 amu. The PITMS science investigation was planned to be operated by GSFC with an international team of scientists. Though the mission did not achieve its lunar landing, information about the PITMS instrument and planning is provided to be able to understand and effectively use data that will be forthcoming from the investigation.

Barbara Cohen↗

DOE OSTI2015

Differentially pumped dual linear quadrupole ion trap mass spectrometer

The present disclosure provides a new tandem mass spectrometer and methods of using the same for analyzing charged particles. The differentially pumped dual linear quadrupole ion trap mass spectrometer of the present disclose includes a combination of two linear quadrupole (LQIT) mass spectrometers with differentially pumped vacuum chambers.

47 OTHER INSTRUMENTATION↗

DOE OSTI2016

Differentially pumped dual linear quadrupole ion trap mass spectrometer

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2012

High collection efficiency X-ray spectrometer system with integrated electron beam stop, electron detector and X-ray detector for use on electron-optical beam lines and microscopes

An X-ray spectrometer systems and methods are provided for implementing signal detection for use on electron-optical beam lines and microscopes. The X-ray Spectrometer System (XSS) includes an X-ray detector (XD) measuring the X-ray signal and positioned proximate to a specimen. An environmental isolation window together with an electron beam stop is disposed between XD and the specimen. The environmental isolation window and the electron beam stop protect XD from electrons directly transmitted through the specimen. An electron detector is located between the electron beam stop and the specimen allowing the measurement of scattered electrons. The XD measures an X-ray signal in the X-ray spectrometer system.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2020

Multi-cone x-ray imaging Bragg crystal spectrometer

Embodiments provide a multi-cone X-ray imaging Bragg crystal spectrometer for spectroscopy of small x-ray sources with a well-defined spectral resolution. The spectrometer includes a glass substrate machined to a multi-cone form; and a thin crystal slab attached to the glass substrate, whereby the multi-cone X-ray imaging Bragg crystal spectrometer provides rotational symmetry of a ray pattern, providing for accurate imaging, for each wavelength in the spectral range of interest. One or more embodiments include a streak camera and/or a gated strip detector.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2021

Methods for aligning a spectrometer

An example method for aligning a spectrometer is described herein. The spectrometer includes a radiation source, a crystal analyzer, and a detector that are all positioned on an instrument plane. The method includes rotating the crystal analyzer about an axis that is within the instrument plane and perpendicular to a rotation plane such that (i) a reciprocal lattice vector of the crystal analyzer is within the instrument plane or (ii) a component of the reciprocal lattice vector within the rotation plane is perpendicular to the instrument plane. An origin of the reciprocal lattice vector is located on the axis. The method further includes tilting the crystal analyzer or translating the detector such that the reciprocal lattice vector bisects a line segment that is bounded by the detector and the radiation source. Example spectrometers related to the example method are also disclosed.

Mortensen, Devon R.↗

DOE OSTI2013

Development of the Low Granularity Pair Spectrometer counters in Hall D at JLab

The pair spectrometer in the photon beam line of Hall D at JLab is designed to monitor the stability of photon flux and the relative tagging efficiency of the photon tagger via a well known electron-positron pair production measurement. The pair spectrometer consists of a thin foil converter, a dipole magnet, and two identical left and right arm detector packages. Each detector package covers the electron or position energy from 3 GeV to 6.25 GeV. It consists of a front detector array for fine position resolution and rear scintillating hodoscopes to provide fast timing to form the pair production trigger. This presentation will focus on the construction and testing of the Low-Granularity Pair Spectrometer counters.

Dzbenski, Nathan↗

DOE OSTI2013

Spectrometer Optics Calibration for Jefferson Lab $ g_2^ p $ Experiment

The proton spin-dependent structure function gp2 in the resonance region has been measured in a recent experiment at Jefferson Lab's Hall A. The goal of this experiment is to determine the gp2 structure function in the Q2 region of 0.02-0.20 GeV2 by using a transversely polarized NH3 target. The Hall A High Resolution Spectrometers (HRS) were used to provide an inclusive measurement of scattered electrons at 5.69 deg. A pair of septum magnets were used to bend the 5.69 deg scatted electrons into the 12.5 deg spectrometers. A full optics calibration of the spectrometer is required to extract the kinematic quantities at the interaction vertex. However, the calibration procedure is challenging due to the complications from the strong transverse target field (2.5 T and 5.0 T) and the varied field configurations of the septum magnets. The details of the optics calibration and the progress will be described in this talk.

Gu, Chao↗

DOE OSTI2024

Compact hyperspectral spectrometers based on semiconductor nanomembranes

Hyperspectral resonant cavity imaging spectrometers and imaging systems incorporating the resonant cavity spectrometers are provided. The spectrometers include an array of photodetectors based on photosensitive semiconductor nanomembranes disposed between two dielectric spacers, each of the dielectric spacers having a thickness gradient along a lateral direction, such that the resonant cavity height differs for different photodetectors in the array.

Ma, Zhenqiang↗

DOE OSTI2019

The SeaQuest spectrometer at Fermilab

The SeaQuest spectrometer at Fermilab was designed to detect oppositely-charged pairs of muons (dimuons) produced by interactions between a 120 GeV proton beam and liquid hydrogen, liquid deuterium and solid nuclear targets. The primary physics program uses the Drell–Yan process to probe antiquark distributions in the target nucleon. The spectrometer consists of a target system, two dipole magnets and four detector stations. The upstream magnet is a closed-aperture solid iron magnet which also serves as the beam dump, while the second magnet is an open aperture magnet. Each of the detector stations consists of scintillator hodoscopes and a high-resolution tracking device. The FPGA-based trigger compares the hodoscope signals to a set of pre-programmed roads to determine if the event contains oppositely-signed, high-mass muon pairs.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Incident beamline design for a modern cold triple axis spectrometer at the High Flux Isotope Reactor

A modern cold triple axis spectrometer is being planned for the High Flux Isotope Reactor (HFIR) at Oak Ridge National Laboratory. Here, we describe the design of an incident beamline that will put a flux of ~ 10 8 $\frac {n}{cm^{2}s}$ on a sample with an area of 2 cm X 2 cm. It takes current physical constraints at HFIR into account and it can accommodate both single and multiplexed analyzer-detector secondary spectrometers and large superconducting magnets. The proposed incident beamline includes a multi-channel guide with horizontal focusing, a neutron velocity selector, components to facilitate an incident beam polarization option, and a double-focusing pyrolytic graphite monochromator. Here, this work describes the process of optimizing the guide system and monochromator and summarizes the expected performance of the incident beamline for non-polarized operation.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2012

Streaked x-ray spectrometer having a discrete selection of Bragg geometries for Omega

The streaked x-ray spectrometer (SXS) is used with streak cameras [D. H. Kalantar, P. M. Bell, R. L. Costa, B. A. Hammel, O. L. Landen, T. J. Orzechowski, J. D. Hares, and A. K. L. Dymoke-Bradshaw, in 22nd International Congress on High-Speed Photography and Photonics, edited by D. L. Paisley and A. M. Frank (SPIE, Bellingham, WA, 1997), Vol. 2869, p. 680] positioned with a ten-inch manipulator on OMEGA [T. R. Boehly et al., Opt. Commun. 133, 495 (1997)] and OMEGA EP [L. J. Waxer et al., Presented at CLEO/QELS 2008, San Jose, CA, 4-9 May 2008 (Paper JThB1)] for time-resolved, x-ray spectroscopy of laser-produced plasmas in the 1.4- to 20-keV photon-energy range. These experiments require measuring a portion of this photon-energy range to monitor a particular emission or absorption feature of interest. The SXS relies on a pinned mechanical reference system to create a discrete set of Bragg reflection geometries for a variety of crystals. A wide selection of spectral windows is achieved accurately and efficiently using this technique. It replaces the previous spectrometer designs that had a continuous Bragg angle adjustment and required a tedious alignment calibration procedure. The number of spectral windows needed for the SXS was determined by studying the spectral ranges selected by OMEGA users over the last decade. These selections are easily configured in the SXS using one of the 25 discrete Bragg reflection geometries and one of the six types of Bragg crystals, including two curved crystals.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2013

A combined electron-ion spectrometer for studying complete kinematics of molecular dissociation upon shell selective ionization

A combined electron-ion spectrometer has been built to study dissociation kinematics of molecular ions upon various electronic decay processes ensuing from ionization of neutral molecules. The apparatus can be used with various ionization agents. Ion time-of-flight (ToF) spectra arising from various electronic decay processes are acquired by triggering the ToF measurement in coincidence with energy analyzed electrons. The design and the performance of the spectrometer in a photoionization experiment is presented in detail. Electron spectra and ion time of flight spectra resulting from valence and 2p{sub 1/2} ionization of Argon and those from valence ionization of CO are presented to demonstrate the capability of the instrument. The fragment ion spectra show remarkable differences (both kinematic and cross sectional) dependent on the energy of the ejected electron, corresponding to various electron loss and decay mechanisms in dissociative photoionization of molecules.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2014

Forward fitting of experimental data from a NE213 neutron detector installed with the magnetic proton recoil upgraded spectrometer at JET

In this paper, we present the results obtained from the data analysis of neutron spectra measured with a NE213 liquid scintillator at JET. We calculated the neutron response matrix of the instrument combining MCNPX simulations, a generic proton light output function measured with another detector and the fit of data from ohmic pulses. For the analysis, we selected a set of pulses with neutral beam injection heating (NBI) only and we applied a forward fitting procedure of modeled spectral components to extract the fraction of thermal neutron emission. The results showed the same trend of the ones obtained with the dedicated spectrometer TOFOR, even though the values from the NE213 analysis were systematically higher. This discrepancy is probably due to the different lines of sight of the two spectrometers (tangential for the NE213, vertical for TOFOR). The uncertainties on the thermal fraction estimates were from 4 to 7 times higher than the ones from the TOFOR analysis.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2016

GOAmazon Thermal Desorption Chemical Ionization Mass Spectrometer

Ion abundance measured by Thermal Desorption Chemical Ionization Mass Spectrometer (using quadrupole mass spectrometer) Data file format: Column 1: date and time (UTC) Column 2: measurement uncertainty (units: integrated ion counts) Column 3: ion intensity (units: integrated ion counts) Column 4: 1 min SO2 mixing ratio in ppb Measurement uncertainty is +/- 0.2 ppb.

54 ENVIRONMENTAL SCIENCES↗