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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 541 records · Page 30

Scientific Value of Including an Atmospheric Sample as Part of Mars Sample Return (MSR)

The Perseverance rover is meant to collect samples of the martian surface for eventual return to Earth. The headspace gas present over the solid samples within the sample tubes will be of significant scientific interest for what it reveals about the interactions of the solid samples with the trapped atmosphere and for what it will reveal about the martian atmosphere itself. However, establishing the composition of the martian atmosphere will require other dedicated samples. The headspace gas as the sole atmospheric sample is problematic for many reasons. The quantity of gas present within the sample tube volume is insufficient for many investigations, and there will be exchange between solid samples, headspace gas, and tube walls. Importantly, the sample tube materials and preparation were not designed for optimal Mars atmospheric gas collection and storage as they were not sent to Mars in a degassed evacuated state and have been exposed to both Earth's and Mars' atmospheres. Additionally, there is a risk of unconstrained seal leakage in transit back to Earth, which would allow fractionation of the sample (leak-out) and contamination (leak-in). The science return can be improved significantly (and, in some cases, dramatically) by adding one or more of several strategies listed here in increasing order of effectiveness and difficulty of implementation: (1) Having Perseverance collect a gas sample in an empty sample tube, (2) Collecting gas in a newly-designed, valved, sample-tube-sized vessel that is flown on either the Sample Fetch Rover (SFR) or the Sample Retrieval Lander (SRL), (3) Adding a larger (50-100 cc) dedicated gas sampling volume to the Orbiting Sample container (OS), (4) Adding a larger (50-100 cc) dedicated gas sampling volume to the OS that can be filled with compressed martian atmosphere.

Timothy D. Swindle↗

PFAS Treatment Pilot Study using Granular Activated Carbon at Kennedy Space Center, Florida

Per- and polyfluoroalkyl substances (PFAS) have been found in investigative derived waste (IDW) generated from groundwater sampling and remediation activities conducted at Kennedy Space Center (KSC), Florida. PFAS are exceptionally strong compounds because of carbon-fluorine bonds resulting in resistance to degradation, low chemical reactivity, compound stability, and persistence in the environment. The regulatory status of PFAS is very dynamic. PFAS is not considered a hazardous waste and has no federal or state (Florida) cleanup requirements at this time. Due to the current and unknown future of the regulatory and treatment landscape, non-hazardous IDW, based upon site volatile organic compounds (VOCs) regulated under Title 40 of Federal Regulations part 261, containing PFAS is not being processed for off-site waste disposal under KSC’s Resource Conservation and Recovery Act permit as a proactive precaution. Long-term storage of aqueous IDW in the meantime was determined to be inadequate due to the potential for spills and/or leaks. A very limited number treatment methods are available at this time. To date, granular activated carbon (GAC) and ion exchange technologies have been found to be some of the most consistent treatment options for removing PFAS from aqueous media. Therefore, a pilot study using GAC was developed at KSC to determine the feasibility of treating non-hazardous IDW containing PFAS to reduce the total volume of PFAS waste and minimize the risk of leaks or spills while storing the waste until complete PFAS-destructive treatment options are more readily available. NASA wanted the pilot test to be able to demonstrate the ability to completely remove 18 PFAS compounds and the site VOCs to below the state of Florida groundwater cleanup target levels (GCTLs).

Michael J Deliz↗

Use of Diffusion Bonded Cu Strap and Integrated MLI for Thermal Control of 100 K IR Detector on L’Ralph Instrument

Passive cooling of cryogenic instruments is one of the most challenging aspects of spaceflight thermal control systems. They are highly sensitive to parasitic heat leaks from their warmer environment, especially the spacecraft components. The L’Ralph instrument on the Lucy mission is an example of such a system, with its LEISA detector requiring passive cooling to temperatures below 112 K. MLI performance can be measured in terms of estar, and analysts apply bias between a high and low estar value. This approach works well for conventional MLI at room temperature, however, it can be dangerous when a mission goes through a wide range of temperatures during its lifetime, with estar values increasing exponentially as temperatures get colder. Various estar correlations are presented as well as how L’Ralph is approaching the MLI problem with the use of IMLI. IMLI uses discrete spacers to isolate each layer, and doesn’t require intermediate layers such as dacron netting. This results in estar performance that can be more precisely estimated, and yields valuesaround 0.004 at the 112K operating temperature. L’Ralph is using IMLI on the backside of the radiator, which permits a more effective use of increased radiator area, by minimizing the area dependent heat leak impact from the instrument backloading. The detector is thermally coupled to the radiator via a diffusion bonded Cu strap. The diffusion bonding process chemically bonds the Cu foil ends in order to maximize heat transfer effectiveness across the multiple foils used. Employing a pressure compensation design via the use of Ti blocks and a clamp at the strap ends ensures that as temperatures go colder, pre-load is maintained in order to minimize resistance at the strap ends. The use of both of these technologies, and how they work together are crucial to the success of the L’Ralph thermal control system.

Thermal↗

Obtaining cryogenic molecular transport data for analysis

The James Webb Space Telescope (JWST) has a primary mirror, made of 18 segments, and a secondary mirror (SM) that are used to direct the light of desired targets. While on orbit, the secondary mirror assembly (SMA) was stowed for approximately 10 days and was subject to molecular contamination outgassing from the cavity of the secondary mirror support structure (SMSS) in-board hinge (IBH) which contains cables, motors, resolvers, and coatings. The main concern during this period before SMA deployment is the accumulation of ice due to the lack of a heater on the SMA. The temperature differentials between the IBH surfaces and SMA could cause redistribution of contaminants. To address this concern, single layer insulation (SLI) was used to create adequate venting and path redirection of outgassing from the IBH. Two separate thermal vacuum tests were performed to quantify this contamination: one Z307 ASTM E 1559 materials test of the radiator paint used on the motor of the IBH and a separate test on a primary mirror backplane assembly (PMBA) qualification engineering test unit (ETU) of the IBH. These tests approximately followed the predicted SMA pre-deployment thermal environment. To quantify source rates in case of a leak, the motor and resolver sides were separated and quartz crystal microbalances (QCM) were used to measure the deposition of water. The SLI redesign and implementation and outgassing measurements to understand leak effects from the IBH were essential to mitigate the deposition of contamination on the SMA.

James Webb Space Telescope, contamination, cleanro↗

Obtaining Cryogenic Molecular Transport Data for Analysis

The James Webb Space Telescope (JWST) has a primary mirror, made of 18 segments, and a secondary mirror (SM) that are used to direct the light of desired targets. While on orbit, the secondary mirror assembly (SMA) was stowed for approximately 10 days and was subject to molecular contamination outgassing from the cavity of the secondary mirror support structure (SMSS) in-board hinge (IBH) which contains cables, motors, resolvers, and coatings. The main concern during this period before SMA deployment is the accumulation of ice due to the lack of a heater on the SMA. The temperature differentials between the IBH surfaces and SMA could cause redistribution of contaminants. To address this concern, single layer insulation (SLI) was used to create adequate venting and path redirection of outgassing from the IBH. Two separate thermal vacuum tests were performed to quantify this contamination: one Z307 ASTM E 1559 materials test of the radiator paint used on the motor of the IBH and a separate test on a primary mirror backplane assembly (PMBA) qualification engineering test unit (ETU) of the IBH. These tests approximately followed the predicted SMA pre-deployment thermal environment. To quantify source rates in case of a leak, the motor and resolver sides were separated and quartz crystal microbalances (QCM) were used to measure the deposition of water. The SLI redesign and implementation and outgassing measurements to understand leak effects from the IBH were essential to mitigate the deposition of contamination on the SMA. "

James Webb Space Telescope↗

Electron Beam Welding of Additively Manufactured Niobium Alloy Heat Pipes

Additively manufactured refractory alloy-liquid metal heat pipes are being developed and tested for thermal management systems within nuclear propulsion and power applications. This study investigated electron beam (EB) welded joints on a laser powder bed fusion printed niobium alloy (C-103) and the impact of multiple joined heat pipe sections on working fluid flow and container leak-tightness. Results showed that EB welded joints connecting multiple heat pipe sections do not impact working fluid wicking behavior and the printed C-103 material and the EB welds joining the tubular sections created a leak-tight container. Interestingly, CT data showed an order of magnitude greater number and volume of porosity indications in the ground mating surface weld compared to the as-printed mating surface weld. The work concluded that AM is a viable manufacturing process for niobium alloy heat pipes and provided valuable insights for future AM heat pipe research and development.

Electron beam welding↗

Waste Container Filtration To Minimize Microbial Escape During Long-Term Storage On Mars

In the search for life on Mars, keeping its surface pristine and free of microbes due to human presence is of utmost importance. Astronauts will use emptied logistics containers during their Martian stay to store waste. These containers will be left on the planet’s surface and are a potential source of microbial contamination. It is desired for these containers to be free from leaks for a minimum of 50 years. If leaks do occur a likely location will be at the port. At this location the mating surfaces will be sealed using a flexible gasket material like a thin metal or a polymer. Eventually these seals will fail. To mitigate these effects, a particulate filter can be employed to equilibrate the pressure between the Martin environment and inside the container. To meet planetary protection requirements, the filter can only allow particulates smaller than 0.2 um diameter to pass. This paper discusses why a particulate filter may be needed and how such a filter would be tested to survive and operate in the harsh Martian environment.

Planetary Protection Waste Containment↗

Designing the Imaging and Breadboard System for FBCE-TL Project

This presentation outlines the support work done on designing the imaging and breadboard system of the Transfer Line (TL) project, which is the third module for the Flow Boiling and Condensation Experiment (FBCE) operating in the Fluids Integrated Rack on-board the International Space Station (ISS). The goal of the FBCE is to serve as a facility for flow boiling and condensation investigating two-phase flow and heat transfer data in microgravity. The TL module aims use existing FBCE hardware to study cryogenic chilldown, a large component of cryogenic propellant tank transfer research. The TL test module will perform chilldown studies with normal-perfluorohexane (nPFH), a cryogenic simulant, flowing through a super-heated line, which is heated through the process of Joule-heating. SolidWorks and Creo were used to create electrically conductive pipe junctions that connect and seal several Indium Tin Oxide (ITO) coated sapphire tube sections together to allow for low leak probability fluid flow and circumferentially uniform electrical current density. It is necessary to understand and calculate the thermal expansion of the tubing sections such that the junctions would not leak at anticipated operating temperatures and pressures, would maintain electrical contact, and not crack the crystalline tubes. Optical imaging techniques were used to build an experimentally validated image remapping process for flight-like setups of cylindrical tubes. Then MATLAB was used to create an algorithm that distorts an image based on the refraction of light passing through the mediums we were imaging through to accurately visualize the cryogenic chilldown that is of scientific interest. This research will assist NASA to move forward with long-duration spaceflight missions where knowledge of efficient heat transfer processes becomes more critical.

imaging system↗

Waste Container Filtration to Minimize Microbial Escape During Long-Term Storage on Mars

In the search for life on Mars, keeping its surface pristine and free of microbes due to human presence is of utmost importance. Astronauts will use emptied logistics containers during their Mars stay to store waste. These containers will be left on the planet’s surface and are a potential source of microorganism contamination. It is desired for these containers to be free from leaks for a minimum of 50 years. If leaks do occur, a likely location will be at any ports. At these locations the mating surfaces will be sealed using a flexible gasket material like a thin metal or a polymer. Eventually these seals will fail. To mitigate these effects, a particulate filter can be employed to equilibrate the pressure between the Martin environment and inside the container. To meet planetary protection requirements, the filter can only allow particulates smaller than 0.2 m diameter to pass. This paper discusses why a particulate filter may be needed and how such a filter could be tested to survive and operate in the harsh Martian environment.

planetary protection↗

Waste Container Filtration to Minimize Microbial Escape During Long-Term Storage on Mars

In the search for life on Mars, keeping its surface pristine and free of microbes due to human presence is of utmost importance. Astronauts will use emptied logistics containers during their Mars stay to store waste. These containers will be left on the planet’s surface and are a potential source of microorganism contamination. It is desired for these containers to be free from leaks for a minimum of 50 years. If leaks do occur, a likely location will be at any ports. At these locations the mating surfaces will be sealed using a flexible gasket material like a thin metal or a polymer. Eventually these seals will fail. To mitigate these effects, a particulate filter can be employed to equilibrate the pressure between the Martin environment and inside the container. To meet planetary protection requirements, the filter can only allow particulates smaller than 0.2 μm diameter to pass. This paper discusses why a particulate filter may be needed and how such a filter could be tested to survive and operate in the harsh Martian environment.

planetary protection↗

Space Suit Material Compatibility with Space Vehicle Coolant PMS-1.5R

During a survey of 82P on February 11, 2023, a shiny substance was detected on the Progress vehicle. The suspected material was PMS-1.5R, a low volatility silicone oil coolant used in the vehicle. Crew exposure to the coolant was a concern as the low volatility would increase residence time, the time a material will stay on a surface after exposure to vacuum. A review of space suit materials revealed several materials with compatibility concerns that could impact Extravehicular Activity (EVA) operations and safety. To understand the risk, space suit materials were exposed to a simulant and tested. This testing provided the basis for rationale generated to continue with EVA operations for US EVA 86 on April 2, 2023. This testing also served as the basis to assess impacts to ISS EMU hardware due to potential contamination brought inside ISS on Russian space suits during RS EVA 61 on October 25, 2023, following an ISS Russian Multipurpose Lab Module (MLM) radiator leak of the same fluid on October 9, 2023. This paper will discuss the testing performed and analyze test results impacts to EVA operations. Additional work was conducted to determine coolant evaporation rates in space vacuum and demonstrate that no significant unreacted coolant from the MLM leak would remain on ISS surfaces long enough to contaminate the EMU or affect the ISS ECLSS water separator.

Space Suit Materials↗

Recent developments at the Goddard Engineering Test Bed

Work on the Flight Telerobotic Service (FTS) since that reported in Leake (1991) is examined, and initial work on a Hubble servicing mission is outlined. A state-of-the-art force reflecting teleoperation system that uses torque control at the joints of the slave manipulator has been implemented. The master rate/slave damper mode proposed by Langley has proved to be a very efficient operational mode, allowing force reflection ratios up to one to one. A software architecture for real-time Ada robotics systems has been proposed, and implementation has been launched. This architecture builds on the lessons learned from NASA Standard Reference Model Architecture and the prototype FTS effort. The Capaciflector sensor has been integrated into the system, and it has been used to perform a basic berthing task autonomously.

Leake, Stephen↗

Chemical Microsensor Development for Aerospace Applications

Numerous aerospace applications, including low-false-alarm fire detection, environmental monitoring, fuel leak detection, and engine emission monitoring, would benefit greatly from robust and low weight, cost, and power consumption chemical microsensors. NASA Glenn Research Center has been working to develop a variety of chemical microsensors with these attributes to address the aforementioned applications. Chemical microsensors using different material platforms and sensing mechanisms have been produced. Approaches using electrochemical cells, resistors, and Schottky diode platforms, combined with nano-based materials, high temperature solid electrolytes, and room temperature polymer electrolytes have been realized to enable different types of microsensors. By understanding the application needs and chemical gas species to be detected, sensing materials and unique microfabrication processes were selected and applied. The chemical microsensors were designed utilizing simple structures and the least number of microfabrication processes possible, while maintaining high yield and low cost. In this presentation, an overview of carbon dioxide (CO2), oxygen (O2), and hydrogen/hydrocarbons (H2/CxHy) microsensors and their fabrication, testing results, and applications will be described. Particular challenges associated with improving the H2/CxHy microsensor contact wire-bonding pad will be discussed. These microsensors represent our research approach and serve as major tools as we expand our sensor development toolbox. Our ultimate goal is to develop robust chemical microsensor systems for aerospace and commercial applications.

hydrogen sensors↗

ES61 – Mechanical Components Test Facility Capabilities

The Mechanical Components Test Facility (MCTF), also known as "Leak Lab" at MSFC is a multi-capability lab that facilitates payload evolution from proof-of-concept to on-orbit operations. We also have the capability to bring our equipment to various location for off-site testing.

Jamboree↗

ANALYSIS OF CRYOGENIC PROPELLANT FEED SYSTEMS FOR ELECTROTHERMAL ENGINES.

An analytical investigation was made of the problems associated with the long-term storage and control of flow of cryogenic propellants for electrothermal engines. Storage of 35 to 174 pounds of propellant for three years is made difficult by the high ratio of surface area to storage tank volume, and the resulting high rate of heat leak. Vented and non-vented storage, storage as high pressure gas, and the use of refrigeration were considered. Recommended storage methods are: for ethane and ammonia vented storage - by venting propellant stored in excess of mission requirements; for hydrogen and helium - by non-vented storage of cold supercritical vapor; and for methane by storage as a non-vented two-phase mixture. The optimum propellant density in the storage tank and optimum insulation thickness were also determined. Design charts were developed for hydrogen and helium, for estimating the maximum pressure expected in non-vented storage tanks, as function of mission requirements. Separation of the constituent phases of liquid-vapor mixtures is achieved by throttling the two-phase mixture to a lower pressure (and temperature) and vaporizing the liquid in the mixture by heat exchange with the contents of the storage tank. The time limitations for continuous use of this method are discussed. Linde super insulations SI-44 or SI -91 are recommended for insulation. Precooling the insulation to temperatures below the steady state level with cold helium vapor before or during fueling of the storage tank eliminates the flow of heat to the tank contents during countdown and take-off. The masses, sizes, and power requirements of the recommended systems are low. The controls are simple and reliable. From the equations and charts in this report the components of the system for a particular mission can be sized. Recommendations are given for experimental work required for the development and testing of such components.

ELECTROTHERMAL ENGINE↗

Proposal for Determining the Mass of Liquid Propellant Within a Space Vehicle Propellant Tank Subjected to a Zero Gravity Environment

A liquid propellant mass measurement system is proposed for the zero gravity environment. The known thermodynamic relationships for the liquid propellant and helium gas concomitant with state of the art instrumentation are used to provide a system comparable with present day terrestrial mass measuring systems. In particular, the operation of the system is outlined for the propellant transfer method and for the determination of leaks and leakage rates. A second concept which is a simplified version of the proposed mass measurement system is introduced and discussed.

PROPELLANT TANK↗

Feasibility of liquid-metal vacuum seals

A basic component of any ultrahigh-vacuum system is a seal capable of isolating a test chamber from its higher pressure surroundings. Two of the most common vacuum seals now in use are the elastomer O-ring seal and the metallic shear seal. The former has the problem of outgassing and gas permeation; the latter requires a large force per unit seal-length to maintain the sealing action. The search for a seal which would provide minimal virtual and real leak rates in a chamber, without requiring a large force to consummate the seal, led to investigation of a liquid-metal seal.

SEALANT↗