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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 541 records · Page 30
All sourcesNASA NTRSDOE OSTI
DOE OSTI2010

Responsivity of Diamond X-ray Photodiodes Calibrated at NSLS

Single crystal, high purity synthetic diamond is used as photoabsorption and carrier transport medium in x-ray photodiodes. While the thermal / mechanical robustness and high x-ray transmission of diamond make such devices attractive for synchrotron instrumentation, state-of-the-art quality material and electrical interfaces further make such detectors feasible. The present work develops methodology for attaining calculable responsivity (photocurrent yield) over a wide range of photon energies (0.2 to 28 keV) to within 5% accuracy. These methods achieve linear response for up to 0.2 W absorbed x-ray power and response time as low as 1 ns. Details of contact formation / robustness and bias configuration are explored.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2011

Long-Working-Distance Kirkpatrick-Baez Mirrors for Hard X-ray Beamlines at SPring-8

We designed and installed two types of long-working-distance Kirkpatrick-Baez (KB) mirrors and mirror manipulators, which were customized into each experiment for hard x-ray undulator beamlines at SPring-8. For the BL32XU RIKEN Targeted Proteins beamline, 400-mm-long KB focusing mirrors for a beam size of 1 {mu}m with a 730-mm-long working distance were designed for carrying out the structural analysis of protein microcrystals. We realized a focusing beam size of 0.9x0.9 {mu}m{sup 2}(FWHM) and a focusing intensity of 6x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV. For the BL19LXU RIKEN SR Physics beamline, we developed KB mirrors for 100-nm focusing with a 100-mm-working distance for the purpose of nano-focus x-ray diffraction. A focusing beam size of 100x100 nm{sup 2}(FWHM) and a high focusing intensity of 3.7x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV were realized.

43 PARTICLE ACCELERATORS↗
DOE OSTI2011

Present Status of the Nanotomography System at BL47XU at SPring-8 and Its Efficiency Improvement Using Double-Condenser Optics

Although imaging x-ray nanotomography developed at beamline BL47XU of SPring-8 has reached a spatial resolution less than 200 nm, poor intensity and low signal-to-noise ratio are more serious problems in the system using zone plate optics. Improvement of the diffraction efficiency of Koehler illumination optics is attempted by doubling two condenser zone plates, which have a constant grating pitch of 200 nm. Although a long longitudinal distance between two condensers is possible ({approx}100 mm), efficiency varies periodically as the distance is changed due to the Talbot effect. A maximum efficiency close to 0.3 is obtained with a periodic distance of approximately 500 {mu}m.

43 PARTICLE ACCELERATORS↗
DOE OSTI2012

U.S. Department of Energy Office of Legacy Management Calibration Facilities - 12103

This paper describes radiometric calibration facilities located in Grand Junction, Colorado, and at three secondary calibration sites. These facilities are available to the public for the calibration of radiometric field instrumentation for in-situ measurements of radium (uranium), thorium, and potassium. Both borehole and hand-held instruments may be calibrated at the facilities. Aircraft or vehicle mounted systems for large area surveys may be calibrated at the Grand Junction Regional Airport facility. These calibration models are recognized internationally as stable, well-characterized radiation sources for calibration. Calibration models built in other countries are referenced to the DOE models, which are also widely used as a standard for calibration within the U.S. Calibration models are used to calibrate radiation detectors used in uranium exploration, remediation, and homeland security. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2012

On the possibility of designing a high-resolution heterodyne spectrometer for near-IR range on the basis of a tunable diode laser

The results of heterodyning of broadband radiation in the near-IR range are presented. A stabilised DFB laser was used as a local oscillator, while the role of a broadband radiation source was played by another DFB laser, excited by the pump current below its threshold value. A fibre-optical Y-coupler based on the single-mode silica fibre served as a diplexer. The radiation mixed in the singlemode fibre was incident on the photodetector, the role of which was played by a p - i - n photodiode. The signal from the photodiode was amplified by the preamplifier with the feedback resistance 240 k{Omega} and the bandwidth {approx}1 MHz and then digitised using a 16-digit ADC. The frequency scanning was implemented via the variation of the local oscillator frequency. The developed registration system provides the sensitivity {approx}1.4 % of the shot noise value at the acquisition time {approx}40 min.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2011

Plasma wave undulator for laser-accelerated electrons

Laser-plasma accelerators have become compact sources of ultrashort electron bunches at energies up to the gigaelectronvolt range thanks to the remarkable progress made over the past decade. A direct application of these electron bunches is the production of short pulse x-ray radiation sources. In this letter, we study a fully optically driven x-ray source based on the combination of a laser-plasma accelerator and a plasma wave undulator. The longitudinal electric field of a laser-generated plasma wave is used to wiggle electrons transversally. The period of this plasma undulator being equal to the plasma wavelength, tunable photon energies in the 10 keV range can be achieved with electron energies in the 100-200 MeV range. Considering a 10s TW class femtosecond laser system, undulators with a strength parameter K{approx}0.5 and with about ten periods can be combined with a laser-plasma accelerator, resulting in several 10{sup -2} emitted x-ray photons per electron.

43 PARTICLE ACCELERATORS↗
DOE OSTI2012

Single-shot X-ray phase-contrast imaging using two-dimensional gratings

We developed a two-dimensional gratings-based X-ray interferometer that requires only a single exposure for clinical radiography. The interferometer consisted of a checkerboard phase grating for {pi} phase modulation and a latticed amplitude grating. Using a synchrotron radiation source, the phase grating modulates the X-rays and generates a self-image, transformed to a moire fringe by the amplitude grating. To allow use of a conventional X-ray tube, the latticed source grating was installed downstream from the X-ray tube. Differential phase-contrast and scattering images in two orthogonal directions were obtained by Fourier analysis of the single moire fringe image and an absorption image. Results show that characteristic features of soft tissue in two orthogonal directions were clearly shown in the differential phase-contrast images.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2015

Room-temperature calorimeter for x-ray free-electron lasers

We have developed a room-temperature calorimeter for absolute radiant power measurements of x-ray free-electron lasers. This room-temperature calorimeter is an electrical substitution device based on the equivalence of electrical and radiant heating. Consequently, the measured radiant powers are traceable to electrical standards, i.e., the International System Units (SI). We demonstrated the performance of the room-temperature calorimeter by electrical power measurements (offline tests). In the offline tests, the room-temperature calorimeter was proven to be able to measure external powers up to at least 6.9 mW, which exceeds the upper limit (∼4 mW) of a cryogenic radiometer (the primary standard detector in Japan). In addition, measurement uncertainties of the room-temperature calorimeter were evaluated to be less than 1.0%, which is adequate for the radiant power measurements of x-ray free-electron lasers. An indirect comparison with the cryogenic radiometer was performed using a synchrotron radiation source to confirm the validity of the absolute radiant powers measured with the room-temperature calorimeter. The absolute radiant powers measured by the calorimeter agreed with those measured by the cryogenic radiometer within 0.6%, which is less than the relative standard uncertainty of the comparison (1.0%)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2013

Basis set expansion for inverse problems in plasma diagnostic analysis

A basis set expansion method [V. Dribinski, A. Ossadtchi, V. A. Mandelshtam, and H. Reisler, Rev. Sci. Instrum. 73, 2634 (2002)] is applied to recover physical information about plasma radiation sources from instrument data, which has been forward transformed due to the nature of the measurement technique. This method provides a general approach for inverse problems, and we discuss two specific examples relevant to diagnosing fast z pinches on the 20–25 MA Z machine [M. E. Savage, L. F. Bennett, D. E. Bliss, W. T. Clark, R. S. Coats, J. M. Elizondo, K. R. LeChien, H. C. Harjes, J. M. Lehr, J. E. Maenchen, D. H. McDaniel, M. F. Pasik, T. D. Pointon, A. C. Owen, D. B. Seidel, D. L. Smith, B. S. Stoltzfus, K. W. Struve, W. A. Stygar, L. K. Warne, J. R. Woodworth, C. W. Mendel, K. R. Prestwich, R. W. Shoup, D. L. Johnson, J. P. Corley, K. C. Hodge, T. C. Wagoner, and P. E. Wakeland, in Proceedings of the Pulsed Power Plasma Sciences Conference (IEEE, 2007), p. 979]. First, Abel inversion of time-gated, self-emission x-ray images from a wire array implosion is studied. Second, we present an approach for unfolding neutron time-of-flight measurements from a deuterium gas puff z pinch to recover information about emission time history and energy distribution. Through these examples, we discuss how noise in the measured data limits the practical resolution of the inversion, and how the method handles discontinuities in the source function and artifacts in the projected image. We add to the method a propagation of errors calculation for estimating uncertainties in the inverted solution.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2010

Status and evolution of the ESRF beamline ID19

The ESRF synchrotron beamline ID19, dedicated to full-field parallel-beam imaging techniques such as phase-contrast and absorption microtomography and X-ray topography, is one of the most versatile instruments of its kind. This paper presents key characteristics of ID19 in its present form, names examples for research and development performed on the beamline, and outlines the plans for an upgrade on the beamline in coming years, to adapt to the growing needs of the user community. The technical goals envisioned include an increase in available beam size and maximum photon energy, and a substantial increase in flux density for applications using beams of small and intermediate size.

43 PARTICLE ACCELERATORS↗
DOE OSTI2010

Present status of SPring-8 macromolecular crystallography beamlines

Seven beamlines are operated for macromolecular crystallography (MX) at SPring-8. The three undulator beamlines are developed for cutting edge target and four bending-magnet beamlines are developed for high throughput MX. The undulator beamline, BL41XU that provides the most brilliant beam, is dedicated to obtain high quality data even from small-size and weakly-diffracting crystals. The minimum beam size at sample position is achieved to 10 {mu}m diameter using a pin-hole collimator. Its photon flux at wavelength {lambda} = 1.0 A is 2.8x10{sup 11} photons/sec. This small beam coupled with irradiation point scanning method is quite useful to take diffraction dataset from small crystals by suppressing the radiation damage. These advanced technologies made a number of difficult protein structure analysis possible, (i.e. Sodium-potassium ATPase). The bending-magnet beamlines BL26B1/B2 and BL38B1 provide automatic data collection exploiting the high mobility of the beam. The beamline operation software 'BSS', sample auto-changer 'SPACE' and web-based data management software 'D-Cha' have made the automatic data collection possible. The 'Mail-in data collection system' that accepts distant users samples via courier service have made users possible to collect diffraction data without visiting SPring-8. The structural genomics research is promoted by these beamlines.

43 PARTICLE ACCELERATORS↗
DOE OSTI2010

Design and Technical Aspects of a New in Vacuum Transfocator at ESRF Beamline ID11

A tunable X-Ray focusing apparatus based on compound refractive lenses (CRL), referred to as a transfocator, has been installed for monochromatic beam (IAT in air transfocator) two years ago in the second optics hutch at ID11 at the ESRF. By varying the number of lenses in the beam, the energy focused and the focal length can be varied continuously throughout a large range of energies and distances.Based the success of the IAT, an in-vacuum transfocator (IVT) has now been built and installed at ID11.The aim of this poster is to describe and show the mechanical and technical solutions used to design and manufacture this new IVT.The IVT was installed last January in the first optics hutch at ID11. The IVT consists of nine water cooled cartridges containing 1, 2, 4, 8, 16, 32 Be lenses, and 32 and 64 Al lenses, and a protective aperture of Oe 900 {mu}m. The mechanical design is based on a system of pneumatically actuated cartridges with an auto positioning on two stainless steel rods. The vacuum vessel has translations and rotations perpendicular to the beam direction in order to align the axis of the cartridges with the x-ray beam.

43 PARTICLE ACCELERATORS↗
DOE OSTI2010

Thermal gradient crystals as tuneable monochromator for high energy X-rays

At the high energy synchrotron radiation beamline BW5 at DORIS III at DESY a new monochromator providing broad energy bandwidth and high reflectivity is in use. On a small 10x10x5 mm{sup 3} silicon crystal scattering at the (311) reflection a thermal gradient is applied, which tunes the scattered energy bandwidth. The (311) reflection strongly suppresses the higher harmonics allowing the use of an image plate detector for crystallography. The monochromator can be used at photon energies above 60 keV.

43 PARTICLE ACCELERATORS↗
DOE OSTI2010

Benefits of Synchrotron Microangiography for Dynamic Studies of Smooth Muscle and Endothelial Roles in the Pathophysiology of Vascular Disease

Changes in endothelial and smooth muscle function compromise organ perfusion in the chronic disease states of diabetes, atherosclerosis and hypertension. Moreover, vascular dysfunction increases the likelihood of lethal acute events such as myocardial infarction and stroke, which are now leading causes of adult mortality. Many circulating and local tissue factors in these disease states contribute to impaired vasomotor regulation of the arterial vessels, leading to spasm, chronic constriction and eventually vessel remodelling. X-ray contrast absorption imaging allows assessment of vessel lumen diameter and the factors contributing to steady-state vessel calibre, however, conventional clinical devices (>200 {mu}m resolution) are not adequate to detect microvessels or accurately assess function in real time. Using synchrotron imaging we are now able to detect small vessel calibres ({approx}30 {mu}m) and quantify regional differences in calibre even under conditions of high heart rate (>500 bpm). Herein we describe recent experiments that were conducted at the Japanese Synchrotron, SPring-8 using anaesthetised Sprague-Dawley rats and C57Bl/6 mice and a synchrotron radiation contrast angiography (single narrow energy bandwidth) approach based on selective arterial injection of iodine contrast agents. Application of this approach to imaging of the heart and other vasculatures are described. Our studies show that within-animal comparisons of 3-4 branching orders of arterial vessels are possible using small bolus contrast injections and appropriate contrast washout times (15-30 min) in many organ systems. Determination of relative calibre changes before and after any treatment allows us to evaluate the contributions of different endogenous factors and ligand-receptor pathways in the maintenance of vasomotor tone. Finally, we will present our findings relating to novel therapies to prevent endothelial dysfunction in heart failure.

62 RADIOLOGY AND NUCLEAR MEDICINE↗
DOE OSTI2011

Atomic and electronic structure of Pd{sub 40}Ni{sub 40}P{sub 20} bulk metallic glass from ab initio simulations

The atomic structure of Pd{sub 40}Ni{sub 40}P{sub 20} bulk metallic glass has been simulated using an ab initio molecular dynamics method with projector-augmented wave pseudopotentials for electron-ion interaction and generalized gradient approximation for exchange-correlation energy. The calculated extended x-ray absorption fine structure (EXAFS) spectra of Pd-K and Ni-K edges, the mass density, and the electronic structure agree remarkably well with the available experimental data and the EXAFS spectra measured at the SPring-8 synchrotron radiation facility. Our results show that the atomic structure can be described in terms of P-centered polyhedra. There are no two P atoms that are nearest neighbors at this composition, and this could be a reason for the observed optimal P concentration of about 20 at.%. The neighboring polyhedra share metal (M) atoms and form a polar covalently bonded random network of P-M-P favoring certain angles. The remaining M atoms act as metallic glue with a tendency of nanoscale clustering of Pd-Pd and Ni-Ni atoms.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Versatile and compact wide-range VUV spectrometer for quantitative measurements

Main parameters of a new scheme of a compact VUV grazing incidence spectrometer based on a plane amplitude diffraction grating are considered. The spectrometer will allow simultaneous detection of spectra at the +1st order diffraction edge with a sufficiently high ( λ/δ λ ∼ 150) spectral resolution and in the –1st order with a moderate resolution ( λ/δ λ ∼ 15 – 30), but in a very wide (5 – 200 nm) spectral range. The use of such a spectrometer is promising for measuring the absolute radiation yield in these spectral regions, which is necessary for the diagnostics and control of plasma radiation sources, including those intended for projection EUV nanolithography. (vuv spectroscopy)

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2011

Measurement of the surface profile of a curved optical surface with rotation phase-shifting lateral shear cyclic path optical configuration

We present a new (to our knowledge) technique for introducing phase shifts between the laterally sheared emergent beam components of a cyclic path optical configuration (CPOC). The phase shifts are introduced by applying a small change in the angle of incidence of the incident beam due to the small angular rotation of the CPOC setup. Phase-shifting interferometry has been applied along with this phase-shifting technique for a CPOC with lateral shear to find the surface slope/profile of curved optical surfaces. Results for a spherical optical surface have been discussed. An optical setup for measurement of the surface profile of toroidal beam line mirrors of synchrotron radiation sources is proposed.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2013

Double negative-metamaterial based Terahertz radiation excited by a sheet beam bunch

We describe a new method to generate enhanced terahertz (THz) surface wave (SW) via its coupling with reversed Cherenkov radiation (RCR), excited by a sheet beam bunch which travels in a vacuum above an isotropic double negative metamaterial (DNM). The physical mechanism for the enhancement is that the DNM can support a RCR which can resonantly interact with a sheet electron beam bunch, resulting in an enhanced SW due to its coupling with the enhanced RCR. Numerical results show strong enhancement effect for the SW and RCR in the THz band. This enhanced THz radiation has potential applications to high-power THz radiation sources and Cherenkov detectors which require large signals.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗