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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3
All sourcesNASA NTRSDOE OSTI
NASA NTRS1976

Use of fractography and sectioning techniques to study fracture mechanisms

Recent investigations of the effect of microstructure on the fracture mechanisms and fracture toughness of steels, aluminum alloys, and titanium alloys have used standard fractographic techniques and a sectioning technique on specimens plastically deformed to various strains up to fracture. The specimens are prepared metallographically for observation in both optical and electron beam instruments. This permits observations to be made about the fracture mechanism as it occurs in thick sections and helps remove speculation from the interpretation of fractographic features. This technique may be used in conjunction with other standard techniques such as extraction replicas and microprobe analyses. Care must be taken to make sure that the microstructural features which are observed to play a role in the fracture process using the sectioning technique can be identified with fractography.

Van Stone, R. H.↗
NASA NTRS1993

Micro-optics technology and sensor systems applications

The current generation of electro-optical sensors utilizing refractive and reflective optical elements require sophisticated, complex, and expensive designs. Advanced-technology-based electro-optical sensors of minimum size and weight require miniaturization of optical, electrical, and mechanical devices with an increasing trend toward integration of various components. Micro-optics technology has the potential in a number of areas to simplify optical design with improved performance. This includes internally cooled apertures, hybrid optical design, microlenses, dispersive multicolor microlenses, active dither, electronically controlled optical beam steer, and microscopic integration of micro-optics, detectors, and signal processing layers. This paper describes our approach to the development of micro-optics technology with our main emphasis for sensors applications.

Gal, George↗
NASA NTRS2004

Microanalytical Efforts in Support of NASA's Materials Science Programs

Following a brief overview of NASA s Microgravity Materials Science programs, specific examples will be given showing electron beam and optical microscopic applications to two-phase glass structures, dendrite tip radii, solid solution semiconductors, undercooled two-phase stainless steels and meteorites.

Gillies, Donald C.↗
NASA NTRSDate not supplied

Indigenous Organic Matter Associated with Unusual Low Temperature Aqueous Secondary Phases in the Mars Meteorite Nakhla

In freshly fractured chips of the Mars meteorite Nakhla, we found carbonaceous phases intimately associated with secondary aqueous alteration phases, both mineral and amorphous, interpreted to have formed through the low-temperature, mineral-water dissolution of the host Martian basalt.We have characterized the nature of carbonaceous matter and spatially associated secondary phases within Nakhla using a multidisciplinary suite of optical and electron beam instrumentation(Thomas-Keprta et al., 2022). Secondary Phases: The preserved secondary mineral phases are best described as ‘juvenile’ hydrated amorphous silica formed when water interacts with mafic rocks. Although amorphous silica on Earth rarely persists through geologic time due to alteration into other phases, e.g.,microcrystalline opal-CT and eventually quartz, the lack of maturation of primarily amorphous silica with embedded nano phase ferrihydrite in Nakhla infers these phases formed in a limited water environment by low temperature, circumneutral pH fluids stabilized by the presence of coexisting amorphous silica.Additionally, we report the presence of the ferrous hydroxycarbonate mineral chukanovite (Fe2(OH)2CO3)within some of the secondary mineral aggregates studied. Organic Matter:Indigenous Nakhla carbonaceous matter is present both in condensed phases and in a dispersed state spatially associated with secondary alteration phases. In the former, discrete refractory micron to submicron assemblages were identified that appear macromolecular in nature and, in several cases, associated with F and, in one case, significant N. While organically bound Fhas yet to be detected remotely on Mars, the identification of organic N within one of the carbonaceous phases is considered a prerequisite for Martian astrobiological potential. Summary: Neither the intimate association of carbonaceous matter with secondary phases nor the identification of chukanovite have been previously reported in any of the Martian meteorites.A variety of habitability-related metastable solid-phase, oxidation-reduction, and organic-molecular sample attributes in Nakhla formed hundreds of millions of years ago near Mars’ surface; these alteration products persisted on Mars until very recentlyand resemble the amorphous materials observed at Gale crater by Mars Science Laboratory CuriosityRover (Rampe et al., 2020).Similar phases may be expected to occur elsewhere on Mars (e.g., Jezerocrater). References: Rampe E. B. et al.(2020) Mineralogy and geochemistry of sedimentary rocks and eolian sediments in Gale crater, Mars: A review after six Earth years of exploration with Curiosity.Geochemistry80, 125605; Thomas-Keprta K.L. et al. (2022) Indigenous carbon-rich matter associated with unusual aqueous alteration features in Nakhla: Complex formation and preservation history. Geochim. et Cosmochim. Acta320, 41-78 (online).

Mars meteorite↗
DOE OSTI2023

Large active-area superconducting microwire detector array with single-photon sensitivity in the near-infrared

Superconducting nanowire single photon detectors (SNSPDs) are the highest-performing technology for time-resolved single-photon counting from the UV to the near-infrared. The recent discovery of single-photon sensitivity in micrometer-scale superconducting wires is a promising pathway to explore for large active area devices with application to dark matter searches and fundamental physics experiments. We present 8-pixel $1 mm^2$ superconducting microwire single photon detectors (SMSPDs) with $1\,\mathrm{\mu m}$-wide wires fabricated from WSi and MoSi films of various stoichiometries using electron-beam and optical lithography. Devices made from all materials and fabrication techniques show saturated internal detection efficiency at 1064 nm in at least one pixel, and the best performing device made from silicon-rich WSi shows single-photon sensitivity in all 8 pixels and saturated internal detection efficiency in 6/8 pixels. This detector is the largest reported active-area SMSPD or SNSPD with near-IR sensitivity published to date, and the first report of an SMSPD array. By further optimizing the photolithography techniques presented in this work, a viable pathway exists to realize larger devices with $cm^2$-scale active area and beyond.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
NASA NTRS1981

Free electron lasers for transmission of energy in space

A one-dimensional resonant-particle model of a free electron laser (FEL) is used to calculate laser gain and conversion efficiency of electron energy to photon energy. The optical beam profile for a resonant optical cavity is included in the model as an axial variation of laser intensity. The electron beam profile is matched to the optical beam profile and modeled as an axial variation of current density. Effective energy spread due to beam emittance is included. Accelerators appropriate for a space-based FEL oscillator are reviewed. Constraints on the concentric optical resonator and on systems required for space operation are described. An example is given of a space-based FEL that would produce 1.7 MW of average output power at 0.5 micrometer wavelength with over 50% conversion efficiency of electrical energy to laser energy. It would utilize a 10 m-long amplifier centered in a 200 m-long optical cavity. A 3-amp, 65 meV electrostatic accelerator would provide the electron beam and recover the beam after it passes through the amplifier. Three to five shuttle flights would be needed to place the laser in orbit.

Segall, S. B.↗
NASA NTRS1989

Dual cathode system for electron beam instruments

An electron beam source having a single electron optical axis is provided with two coplanar cathodes equally spaced on opposite sides from the electron optical axis. A switch permits selecting either cathode, and a deflection system comprised of electromagnets, each with separate pole pieces equally spaced from the plane of the cathodes and electron optical axis, first deflects the electron beam from a selected cathode toward the electron optical axis, and then in an opposite direction into convergence with the electron optical axis. The result is that the electron beam from one selected cathode undergoes a sigmoid deflection in two opposite directions, like the letter S, with the sigmoid deflection of each being a mirror image of the other.

Bradley, James G.↗
NASA NTRS2002

Diffractive optical elements on non-flat substrates using electron beam lithography

The present disclosure describes a technique for creating diffraction gratings on curved surfaces with electron beam lithography. The curved surface can act as an optical element to produce flat and aberration-free images in imaging spectrometers. In addition, the fabrication technique can modify the power structure of the grating orders so that there is more energy in the first order than for a typical grating. The inventors noticed that by using electron-beam lithography techniques, a variety of convex gratings that are well-suited to the requirements of imaging spectrometers can be manufactured.

Maker, Paul D.↗
DOE OSTI2025

Beam optics ramping in underconstrained lattice design: Application to Electron-Ion Collider hadron storage ring cooling section

This paper presents the lattice design and optics ramping strategy for the cooling section of the hadron storage ring at the electron-ion collider. The main challenge is that available tuning knobs exceed beam-optics constraints. Independently optimized injection and top-energy optics often yield disconnected solutions, making interpolation impossible. To address this, we propose two new methods. The first is an intermediate-penalty scheme that ensures ramping path continuity by penalizing constraint violations at intermediate states. The second is a continuation-based approach that adapts high-energy optics to low energy, guided by an adaptive weighting scheme to balance injection and ramping constraints. The solutions meet all beam dynamics and hardware limits. The two methods offer a general strategy for ramping in systems where the solution space is under-constrained and the starting and target configurations are far apart.

43 PARTICLE ACCELERATORS↗
DOE OSTI2026

Evaluation of the interfacial bonding strength between hafnia and silica layers deposited by electron-beam evaporation

Factors contributing to the mechanical strength of multilayer optical coatings involving alternating layers of electron-beam evaporated hafnia and silica is investigated. It is observed that upon rupture resulting from nanosecond laser damage, fragments consisting of layer pairs are produced. These pairs are formed as a result of a strong asymmetry in adhesion strength between interfaces, leading to preferential delamination at interfaces where silica is deposited on hafnia, and not the reverse, despite the fact that both interface types consist of the same pair of materials. The observed disparity in adhesion strength was further studied using nanomechanical scratch tests, revealing loads at which fracture occurs, and fracture morphology, both of which are highly dependent on deposition order. Based on these measurements, along with the morphological analysis of the nanostructure of the coatings, we conclude that the surface microstructure in each coating layer affects its adhesion strength with the succeeding layer. The findings outlined here are particularly relevant to the production of large aperture, high-performance optics designed for use in next-generation lasers.

adhesion strength↗
NASA NTRS1986

An electromagnetic/electrostatic dual cathode system for electron beam instruments

A method of providing cathode redundancy which consists of two fixed cathodes and uses electromagnetic and/or electrostatic fields to direct the electron beam to the electron optical axis is presented, with application to the cathode system of the Scanning Electron Microscope and Particle Analyzer proposed for NASA's Mariner Mark II Comet Rendezvous/Asteroid Flyby projected for the 1990s. The symmetric double deflection system chosen has the optical property that the image of the effective electron source is formed above the magnet assembly near the apparent position of the effective source, and it makes the transverse positions of the electron sources independent of the electron beam energy. Good performance of the system is found, with the sample imaging resolution being the same as for the single-axis cathode.

Bradley, J. G.↗
DOE OSTI2023

Direct density modulation of photo-assisted field emission from an RF cold cathode

This paper explores direct density modulation of high-current electron beam emission from an RF cold cathode using optical excitation. We theoretically study the photo-assisted field emission of periodically bunched electron beams of various pulse shapes under the combined excitation of an RF field and an optical field, using an exact quantum model. Both continuous-wave (CW) and pulsed optical fields are considered. The emission current pulse amplitude, pulse width, electron number density per pulse, as well as pulse shape and its harmonic contents are investigated in detail. For CW photon sources in the UV to NIR range (i.e., 200–1200 nm), increasing the optical intensity under an RF bias tends to change the current pulse from a Gaussian to sinusoidal-like shape, thus offering strong flexibility to control the frequency components in beam current emission. Pulsed photon sources combined with an RF field can produce sharp, high-current electron bunches with pulse duration comparable with or even less than that of the optical pulse. A contour map of the density modulation depth is constructed for different combinations of RF and laser fields. The results provide insight into unlocking new opportunities to achieve direct density modulation during electron current emission by optical means.

Physics↗
NASA NTRS1993

Optical observations of the beam-plasma discharge phenomenon

Spectroscopic observations of optical emissions from the beam-plasma discharge (BPD) phenomenon were made with NASA's vacuum chamber facility, at the Johnson Space Center, configured to simulate the physical conditions of magnetospheric electron beam injection into the ionospheric/upper-atmospheric environment. Nonlinear N2 and N2(+) optical emission growth rates (with respect to incremental electron beam current values) were observed from the chamber gas during transition to the BPD state. For electron-beam currents (I) near the BPD transition value (I(sub c)), the band emissions from the chamber gas produced by relatively low energy (less than or equal to 50 eV) electrons interacting with N2 were anomalously more intense than those requiring higher energy (greater than 100 eV) electrons to excite them. For I more greater than I(sub c), the optical emissions increased linearly with I (as was the case for I less than I(sub c)) and their ratios decreased significantly from the peak values attained when I approximately equals I(sub c). These observations suggest that during BPD some of the energy of the primary electron beam is efficiently transferred, via wave-particle interactions, to local electrons produced through ionization of the chamber gas; the resulting suprathermal electrons provide an additional source of excitation for the relatively low energy states (A, B and C) of N2. Such nonlinear excitation of upper atmospheric gas may occur in certain auroral events wherein the current due to the precipitating electrons approaches a value close to I(sub c).

Sivjee, G. G.↗
NASA NTRS1983

Vibration-Isolation Bench for Testing in Vacuum

Precise optical systems tested without contamination. Vibration isolator is one of three such units supporting cast-iron table. Table used to test optical systems in vacuum. Isolator made from commercially available components. Scaled-down version finds wider application in electron optics or electron-beam lithography.

Dankowski, J. C.↗
NASA NTRS2001

Performance Evaluation of Titanium Ion Optics for the NASA 30 cm Ion Thruster

The results of performance tests with titanium ion optics were presented and compared to those of molybdenum ion optics. Both titanium and molybdenum ion optics were initially operated until ion optics performance parameters achieved steady state values. Afterwards, performance characterizations were conducted. This permitted proper performance comparisons of titanium and molybdenum ion optics. Ion optics' performance A,as characterized over a broad thruster input power range of 0.5 to 3.0 kW. All performance parameters for titanium ion optics of achieved steady state values after processing 1200 gm of propellant. Molybdenum ion optics exhibited no burn-in. Impingement-limited total voltages for titanium ion optics where up to 55 V greater than those for molybdenum ion optics. Comparisons of electron backstreaming limits as a function of peak beam current density for molybdenum and titanium ion optics demonstrated that titanium ion optics operated with a higher electron backstreaming limit than molybdenum ion optics for a given peak beam current density. Screen grid ion transparencies for titanium ion optics were as much as 3.8 percent lower than those for molybdenum ion optics. Beam divergence half-angles that enclosed 95 percent of the total beam current for titanium ion optics were within 1 to 3 deg. of those for molybdenum ion optics. All beam divergence thrust correction factors for titanium ion optics were within 1 percent of those with molybdenum ion optics.

Soulas, George C.↗