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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Microstructure and magnetic properties of (001) textured L1(0) FePt films on amorphous glass substrate

L1(0) FePt thin films with an island-like morphology and magnetic perpendicular anisotropy were grown at low temperature (300 < T-dep< 375 degrees C) by magnetron sputtering on Hoya glass substrates using a 30-nm thick Cr (2 0 0) underlayer. An MgO buffer layer with a thickness of 2 nm was used to inhibit the diffusion from the Cr underlayer and promote the growth of (0 0 1) oriented L1(0) FePt films by inducing an in-plane lattice distortion. By varying the substrate temperature and the Ar sputter pressure (3.5 < P-Ar< 15 mTorr) during the deposition, the degree of chemical order, the microstructure and the magnetic properties were tuned and the best properties in term of squareness ratio (M-r/M-s similar to 0.95) and coercive field (H-c similar to 14 kOe) were observed for films deposited at T-dep = 350 degrees C and P-Ar= 5 mTorr, due to the appearance of a tensile strain, which favors the perpendicular anisotropy. The analysis of the angular dependence of remanent magnetization curves on the optimized sample suggests that the magnetization reversal is highly incoherent due to the inter-island interactions. Our results provide useful information on the low temperature growth of FePt films with perpendicular anisotropy onto glass substrates, which are relevant for a variety of technological applications, such as magnetic recording and spintronic devices. (C) 2015 Elsevier B.V. All rights reserved.

Speliotis, T↗
DOE OSTI2018

Textural properties determined CO 2 capture of tetraethylenepentamine loaded SiO 2 nanowires from α-sepiolite

To understand the effect of porous parameters and chemical components on CO 2 capturing performance of solid state amine absorbents and their kinetic parameters, a clay mineral-based CO 2 absorbent was prepared by impregnating five different liquid amines onto SiO 2 nanowire clusters from fibrous sepiolite (Sep). Characterization was conducted by XRD, SEM, FTIR, and N 2 adsorption–desorption isotherm, CO 2 adsorption performances were measured by TGA. After acid treatment, the raw Sep mineral changed into amorphous silica nanowires, and the largest S BET of the obtained SiO 2 nanowires reached 320 m 2 /g, which was 8 times larger than the pristine mineral. Amongst the adapted amines, tetraethylenepentamine (TEPA) showed superiority in the CO 2 adsorption capacity. The optimized adsorption capacity reached 3.7 mmol/g at 75 °C from a CO 2 + N 2 mixture on a ~50 wt% TEPA loaded SiO 2 sample, and the capacity remained 3.6 mmol/g after ten circles of adsorption/desorption tests. The pore size and pore structure of the matrix, rather than the surface area, will obviously affect the adsorption ability of the product. Kinetic parameters for the CO 2 adsorption process fitted well with a fractional-order model, confirming that the CO 2 adsorption process by the solid absorbent should be a combination of both physical and chemical reactions. Results in this article provide detailed parameters for preparing and understanding these clay mineral based solid state CO 2 absorbents.

36 MATERIALS SCIENCE↗
DOE OSTI2021

Mesoporous Textured Fe-N-C Electrocatalysts as Highly Efficient Cathodes for Proton Exchange Membrane Fuel Cells

A new platinum group metal (PGM)-free proton exchange membrane fuel cell (PEMFC) cathode catalyst materials, synthesized using the VariPore™ method by Pajarito Powder, LLC, are characterized for their structure and activity. The physico-chemical analysis of the iron-nitrogen-carbon (Fe-N-C) electrocatalysts show mesoporous carbon material effectively doped with iron and nitrogen. The materials have an average pore size of 7-8 nm and high specific surface area. The Fe-N-C catalysts exhibit good oxygen reduction reaction (ORR) activity in 0.5 M H2SO4 electrolyte with high half-wave potential and sustainable electrochemical stability over 10,000 repeated potential cycles with insignificant losses in their activities. As cathode catalysts in a PEMFC, the Fe-N-C materials deliver remarkably good fuel cell performance at low overpotential approaching that of the commercial Pt catalyst. The high ORR electrocatalytic activity of these Fe-N-C catalysts is credited to the synergy between nitrogen-moieties, specifically pyrrolic-N, pyridinic-N, and graphitic-N, and iron in addition to the high mesoporosity that facilitate an effective reaction path in boosting the electrocatalytic activity and stability.

DIRECT ENERGY CONVERSION↗
DOE OSTI2018

Texturizing Wind Turbine Towers to Reduce Bat Mortality

There is still a great need for the development of mitigation strategies that are economically viable and can be used alone or in combination with other options (e.g., operational minimization, acoustic deterrents) to ensure that bat fatalities are effectively reduced at wind facilities across the U.S. Our goal was to develop a wind turbine tower coating that 1) bats show little or no interest in approaching, 2) can be applied to currently deployed wind turbine towers and to towers as they are constructed, 3) is economically feasible to produce and apply, and 4) ultimately contributes to a reduction in bat mortality at utility-scale wind facilities. Wind turbine tower monopoles are large, smooth surfaces and numerous studies have reported bats making close investigative approaches at turbine tower surfaces that are suggestive of drinking and foraging behavior. We therefore hypothesized that such activity could be contributing to bat-wind turbine fatalities by increasing the amount of time that bats spend in or around the rotor-swept zone. We further hypothesized that a texturizing the tower might minimized bat activity at the towers and therefore reduce fatality risk. To explore this, we designed a series of experiments to characterize how bats interact with smooth and texture-treated surfaces in a controlled environment. We conducted 64 behavioral trials in a flight facility from 10 June to 25 September 2015 and an additional 76 behavioral trials from 9 June to 30 August 2016. The first set of trials showed that while bats did make contact with smooth surfaces, they did not make contact with textured surfaces. We ascertained that bat activity occurred at 0 to 1 m distances from surfaces, suggesting that the bats (used in this study) may need to be this close to a surface to accurately discern its texture. From the results were developed a texture coating. For the second set of trials, we tested the texture coating. Bats showed a >40% reduction in activity within 1 m of the textured surfaces in comparison to the smooth surfaces. Following these controlled experiments, we conducted field tests at Wolf Ridge Wind, LLC. We applied the texture coating to the midsection of turbine monopoles. The texture coating was manually applied to 2 turbine towers, although we noted during the application there was variation in texture coating between turbines. We considered that this variation could potentially impact bat behavior. We then conducted bat activity surveys at both texture-treated towers and 2 nearby control towers, over 55 nights from 24 June to 22 September, 2017. All species of bats known to be present at the site were detected in the acoustic recordings at these turbine towers. We found no significant differences in overall numbers of bats observed and levels of acoustic activity at the smooth and texture-treated towers. When we analyzed the experimental pairs separately, however, we found that a greater proportion of the close range bat activity within Pair 1 occurred at the texture-treated tower and that much of this activity could be attributed to foraging behavior. In contrast at turbine Pair 2, we observed no difference in the proportion of close range bat activity between the smooth and texture-treated tower, with no clear differences in behavior at the two tower types. When we examined acoustic bat activity at the tower pairs separately, we found species-specific differences in activity that differed between the smooth and texture-treated towers within the pairs. For example, hoary bat acoustic activity was significantly higher at the texture-treated tower in Pair 1, but significantly lower at the texture-treated tower in Pair 2. Given the observational nature of the field test, our limited sample size (2 turbine pairs), variation in the texture-coating between the 2 turbine pairs, and different patterns of bat activity observed at the 2 turbine pairs, inferences from this one field test are limited at best. In conclusion, the results from the flight facility experiments were promising (i.e., we observed a significant decrease in bat activity at smooth compared to texture-treated surfaces); however, due to coating installation and application challenges prior to our field test, we were unable to collect sufficient information to understand how these coatings affect bat activity at operational wind turbine towers. Although the results from the field test are inconclusive, the lessons learned will be informative for future research into turbine surface materials that can modify the surface of the turbine tower and therefore alter how bats perceive wind towers. Thus, the outcomes of this research project may have a significant impact on wind energy operators, wind developers, and OEMs by contributing to future impact mitigation strategies. In future research we will test new ideas to improve the development, application, and evaluation of this mitigation technique.

17 WIND ENERGY↗