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Development of techniques to simplify the process of investigation and estimate of natural resources in remote and relatively unexplored areas, Venezuela

The author has identified the following significant results. Based upon the results obtained by both interpretations, radar and satellite, highly fractured zones were outlined and checked against geologic rock samples. Most of the rock samples were collected along the Ventuari River that crosses most of the project area from NE to SE. The structural orientation and fracture patterns were taken into consideration during the planning of flight lines, also the magnetic declination of the area. Most of the flight lines were oriented N 30 deg W across known structural trends; the altitude above ground was 450 feet, and the distance between lines was 3000 feet. The ERTS image permits the obtention of a panoramic vision of the area, and facilitates the exact delineation of major drainages. Topographic changes are easily observed. Rocky outcrops are easily distinguishable on band 5 and 7. Shrub vegetation zones are distinguishable on both bands, without possible separation of forest types, this is possible only when the physiographic conditions of small textural differences are taken into account.

Romero, A. C.↗

Robotic sampling system for an unmanned Mars mission

A major robotics opportunity for NASA will be the Mars Rover/Sample Return Mission which could be launched as early as the 1990s. The exploratory portion of this mission will include two autonomous subsystems: the rover vehicle and a sample handling system. The sample handling system is the key to the process of collecting Martian soils. This system could include a core drill, a general-purpose manipulator, tools, containers, a return canister, certification hardware and a labeling system. Integrated into a functional package, the sample handling system is analogous to a complex robotic workcell. Discussed here are the different components of the system, their interfaces, forseeable problem areas and many options based on the scientific goals of the mission. The various interfaces in the sample handling process (component to component and handling system to rover) will be a major engineering effort. Two critical evaluation criteria that will be imposed on the system are flexibility and reliability. It needs to be flexible enough to adapt to different scenarios and environments and acquire the most desirable specimens for return to Earth. Scientists may decide to change the distribution and ratio of core samples to rock samples in the canister. The long distance and duration of this planetary mission places a reliability burden on the hardware. The communication time delay between Earth and Mars minimizes operator interaction (teleoperation, supervisory modes) with the sample handler. An intelligent system will be required to plan the actions, make sample choices, interpret sensor inputs, and query unknown surroundings. A combination of autonomous functions and supervised movements will be integrated into the sample handling system.

Chun, Wendell↗

Apollo Lunar Sample Photographs: Digitizing the Moon Rock Collection

The Acquisition and Curation Office at JSC has undertaken a 4-year data restoration project effort for the lunar science community funded by the LASER program (Lunar Advanced Science and Exploration Research) to digitize photographs of the Apollo lunar rock samples and create high resolution digital images. These sample photographs are not easily accessible outside of JSC, and currently exist only on degradable film in the Curation Data Storage Facility

Lofgren, Gary E.↗

Carbon, hydrogen and nitrogen in carbonaceous chondrites Abundances and isotopic compositions in bulk samples

Whole-rock samples of 25 carbonaceous chondrites were analyzed for contents of C, H and N and delta C-13, delta D and delta N-15. Inhomogeneous distribution of these isotopes within individual meteorites is pronounced in several cases. Few systematic intermeteorite trends were observed; N data are suggestive of isotopic inhomogeneity in the early solar system. Several chondrites revealed unusual compositions which would repay further, more detailed study. The data are also useful for classification of carbonaceous chondrites; N abundance and isotopic compositions can differentiate existing taxonomic groups with close to 100 percent reliability; Al Rais and Renazzo clearly constitute a discrete 'grouplet', and there are hints that both CI and CM groups may each be divisible into two subgroups.

Kerridge, J. F.↗

Isotopic evidence for a terminal lunar cataclysm

Most highland total rock samples define a single U-Pb isochron which corresponds to a metamorphism age of about 3.9 aeons. This age is also obtained for internal U-Pb isochrons for some of these samples. The data on 18 rock samples range from concordant samples with U-238/Pb-206 ratio of about 1.2 to discordant ones with U-238/Pb-206 ratio of about 0.02. This feature, coupled with a correlated pattern of U-238/Pb-204 ratios, indicates that Pb was extensively mobilized at about 3.9 aeons. The observed Pb-U fractionation is essentially due to Pb volatilization during the metamorphic events. Volatile Pb transport is not accompanied by similar effects in Rb and must therefore be attributed to a specific process. Rb-Sr internal isochrons for the same rocks determine distinct metamorphic events in the interval 3.85 to 4.00 aeons. It is concluded that highland samples from widely separated areas bear the imprint of an event or series of events in a narrow time interval which can be identified with a cataclysmic impacting rate of the moon at about 3.9 aeons, although diffrentiation by internal magma generation cannot be excluded.

Tera, F.↗

The surface chemical composition of lunar samples and its significance for optical properties

The surface Fe, Ti, Ca, and Si concentrations in a variety of soil and rock samples from all the Apollo sites are determined using an Auger spectrometer plus a single-pass cylindrical-mirror analyzer with a standard 15-stage BeCu electron multiplier. It is found that there are no great differences between the surface and bulk concentrations of any of the four elements in the rock samples, but the surface Fe and Ti concentrations in soil samples are higher than the bulk concentrations. Results are also reported for solar-wind simulation experiments in which a pulverized rock sample was bombarded with 2-keV alpha-particles corresponding to about a 30,000-yr dose of the solar-wind proton component. These results indicate that the chemical change induced on the surface of a rock powder by positive-ion bombardment is similar to the change from bulk to surface chemical composition in lunar soil samples. A clear correlation is observed between the surface Fe concentration and albedo of the soil samples.

Gold, T.↗

Microwave dielectric spectrum of rocks

A combination of several measurement techniques was used to investigate the dielectric properties of 80 rock samples in the microwave region. The real part of the dielectric constant, epsilon', was measured in 0.1 GHz steps from 0.5 to 18 GHz, and the imaginary part, epsilon'', was measured at five frequencies extending between 1.6 and 16 GHz. In addition to the dielectric measurements, the bulk density was measured for all the samples and the bulk chemical composition was determined for 56 of the samples. The study shows that epsilon' is frequency-dependent over the 0.5 to 18 GHz range for all rock samples, and that the bulk density rho accounts for about 50 percent of the observed variance of epsilon'. For individual rock types (by genesis), about 90 percent of the observed variance may be explained by the combination of density and the fractional contents of SiO2, Fe2O3, MgO, and TiO2. For the loss factor epsilon'', it was not possible to establish statistically significant relationships between it and the measured properties of the rock samples (density and chemical composition).

Ulaby, F. T.↗

Cautionary Notes on Cosmogenic W-182 and Other Nuclei in Lunar Samples

Leya et al. (2000) showed that neutron capture on Ta-181 results in a production rate of Ta-182 (decays with a half-life of 114 days to W-182) sufficiently high to cause significant shifts in W-182 abundances considering the neutron fluences due to the cosmic ray cascade that were known to occur near the lunar surface. Leya et al. concluded that this cosmogenic production of W-182 may explain the large positive epsilon(sub W-182) values that Lee et al. (1997) had reported in some lunar samples rather than being produced from decay of now extinct Hf-182 (bar tau = 13 x 10(exp 6) yr). If the large range in epsilon(sub W-182) of lunar samples (0 to +11 in whole rock samples) was due to decay of now extinct Hf-182, it would require a very early time of formation and differentiation of the lunar crust-mantle system (with high Hf/W ratios) during the earliest stages of Earth s accretion. This result was both surprising and difficult to understand. The ability to explain these results by a more plausible mechanism is therefore very attractive. In a recent report Lee et al. (2002) showed that there were excesses of W-182 and that epsilon(sub W-182) was correlated with the Ta/W ratios in the mineral phases of individual lunar rock samples. This is in accord with W-182 variations in lunar samples being produced by cosmic-ray induced neutron capture on Ta-182.

Yin, Qingzhu↗

The Surface Chemical Composition of Lunar Samples and Its Significance for Optical Properties

The surface iron, titanium, calcium, and silicon concentration in numerous lunar soil and rock samples was determined by Auger electron spectroscopy. All soil samples show a large increase in the iron to oxygen ratio compared with samples of pulverized rock or with results of the bulk chemical analysis. A solar wind simulation experiment using 2 keV energy alpha -particles showed that an ion dose corresponding to approximately 30,000 years of solar wind increased the iron concentration on the surface of the pulverized Apollo 14 rock sample 14310 to the concentration measured in the Apollo 14 soil sample 14163, and the albedo of the pulverized rock decreased from 0.36 to 0.07. The low albedo of the lunar soil is related to the iron + titanium concentration on its surface. A solar wind sputter reduction mechanism is discussed as a possible cause for both the surface chemical and optical properties of the soil.

Gold, T.↗

The ages of lunar material from Fra Mauro, Hadley Rille, and Spur Crater.

Ar-40/Ar-39 dating techniques were applied to estimate the age of twelve crystalline and fragmented Fra Mauro rock samples and six Hadley Rille and Spur Crater rock samples provided by the Apollo 14 and 15 missions. Genesis histories of some associated lunar surface features are traced back on the basis of obtained rock age values.

Husain, L.↗

Atmospheric rare gases in lunar rock 60015

Aliquots of lunar rock 60015 were subjected to various types of exposure and handling designed to produce terrestrial contamination, in order to test the possibility of a terrestrial origin for the terrestrial-like trapped Xe reported for lunar rock samples. Crushing the rock produced up to order-of-magnitude increases in the abundances of Ar, Kr, and Xe relative to the millimeter-sized chips of 60015 previously analyzed. Contrary to expectations for atmospheric contamination, high temperatures (above 1000 C) were necessary to remove about 75% of the trapped Kr and Xe, and the rare-gas elemental abundance ratios differed from those in terrestrial samples believed to have occluded atmospheric gases. It is concluded, on the basis of similar temperature-release profiles and elemental-fractionation patterns, that the trapped Xe observed in all these 60015 analyses is atmospheric contamination. Such a conclusion cannot unequivocally be drawn for other lunar rocks containing terrestrial-like Xe, but the present results demonstrate that arguments based on high extraction temperatures and elemental abundance ratios cannot be useful to rule out rare-gas atmospheric contamination in such samples.

Niemeyer, S.↗

The search for the cause of the low albedo of the moon

Experimentation concerning lunar weathering and its effect on the albedo of the surface cover consisted of: (1) determination of the surface chemical composition of lunar soil and ground-up rock samples by Auger electron spectroscopy, (2) measurement of the optical albedo of these samples, and (3) proton or alpha-particle irradiation of terrestrial rock chips and rock powders and of ground-up lunar rock samples in order to determine the optical and surface chemical effect of simulated solar wind.

Gold, T.↗

Rheology of Diabase: Implications for Tectonics on Venus and Mars

Two important goals of our experimental investigation of the rheological behavior of diabase rocks were: (1) to determine flow laws describing their creep behavior over wide ranges of temperature, stress and strain rate and (2) to develop an understanding of the physical mechanisms by which these rocks flow under laboratory conditions. With this basis, a primary objective then was to construct constitutive equations that can be used to extrapolate from laboratory to planetary conditions. We specifically studied the rheological properties of both natural rock samples and synthetic aggregates. The former provided constraints for geologic systems, while the latter defined the relative contributions of the constituent mineral phases and avoided the influence of glass/melt found in natural samples. In addition, partially molten samples of crustal rock composition were deformed in shear to large strains (greater than 200%) important in crustal environments. The results of this research yielded essential rheological properties essential for models of crustal deformation on terrestrial planets, specifically Venus and Mars, as well as on the geodynamical evolution of these planets. Over the past three years, we also completed our investigation of the creep behavior of water ice with applications to the glaciers, ice sheets and icy satellites. Constitutive equations were determined that describe flow over a wide ranged of stress, strain rate, grain size and temperature. In the case of ice, three creep regimes were delineate. Extrapolation demonstrates that dislocation glide and grain boundary sliding processes dominate flow in ice I under planetary conditions and that diffusion creep is not an important deformation mechanism either in the laboratory or on icy satellites. These results have already been incorporated by other investigators into models describing, for example, the thickness and stability of the ice shell on Europa and to unravel long-standing discrepancies between field observations on glaciers and laboratory results.

Kohlstedt, David L.↗

Prioritizing Scientific Data for Transmission

A software system has been developed for prioritizing newly acquired geological data onboard a planetary rover. The system has been designed to enable efficient use of limited communication resources by transmitting the data likely to have the most scientific value. This software operates onboard a rover by analyzing collected data, identifying potential scientific targets, and then using that information to prioritize data for transmission to Earth. Currently, the system is focused on the analysis of acquired images, although the general techniques are applicable to a wide range of data modalities. Image prioritization is performed using two main steps. In the first step, the software detects features of interest from each image. In its current application, the system is focused on visual properties of rocks. Thus, rocks are located in each image and rock properties, such as shape, texture, and albedo, are extracted from the identified rocks. In the second step, the features extracted from a group of images are used to prioritize the images using three different methods: (1) identification of key target signature (finding specific rock features the scientist has identified as important), (2) novelty detection (finding rocks we haven t seen before), and (3) representative rock sampling (finding the most average sample of each rock type). These methods use techniques such as K-means unsupervised clustering and a discrimination-based kernel classifier to rank images based on their interest level.

Castano, Rebecca↗

Connecting Community Scientific Hypotheses to Mars Sample Science

The proposed Mars Sample Return (MSR) program seeks to bring back to Earth a set of specially curated samples from the surface of Mars. The first segment of the MSR program is presently under-way; the Mars 2020 rover Perseverance has, to date, collected 24 samples of martian rock, regolith, and at-mosphere within Jezero crater. Its geologically diverse rock sample set can provide insight into the time evolu-tion of the Jezero environment, including the possible preservation of ancient biosignatures. Presently, a cache of 10 samples has been deposited in the Three Forks region on the floor of Jezero crater. These sam-ples, deemed scientifically return worthy by the Mars science community [1], are intended as a contingency sample set, as Perseverance has subsequently obtained more samples, and is therefore storing a more compre-hensive and scientifically valuable set of samples that will grow as the rover ascends to the rim of Jezero crater. The return of samples from Mars has been identi-fied as the highest priority planetary mission in the past three National Academies Decadal Surveys [2-4]. Sub-stantial work has gone into establishing science objec-tives for an MSR program, an overall framework for sample retrieval and analysis, and the expected impact on future Mars science and exploration (e.g., [5]). These objectives have been established at a relatively high level, e.g., “Interpret the primary geologic pro-cesses and history that formed the martian geologic rec-ord, with an emphasis on the role of water.” (Objective 1 in [5]) and are designed to encapsulate the broad sci-entific priorities of, and lay the groundwork for, inves-tigation strategies and measurements to be conducted by a future MSR program. It is from this overarching framework that the Connecting Community Scientific Hypotheses to Mars Sample Science workshop (‘The Workshop’) was conceived, with the purpose of distil-ling these high-level scientific objectives into discrete, testable hypotheses across a range of scientific disci-plines. The output of the workshop is meant to be a ‘hy-pothesis document’ serving as a starting point for cata-loging and condensing specific hypotheses for consid-eration by the scientific community. The template for this approach is based on the “driving hypotheses” de-veloped by the OSIRIS-REx team as part of their Sam-ple Analysis Plan [6].

Michael A Mischna↗

Microwave dielectric properties of dry rocks

A combination of techniques was used to measure the dielectric properties of 80 rock samples in the microwave region. The real part (RP) of the relative dielectric constant was measured in 0.1-GHz steps from 0.5 to 18 GHz, and the imaginary part (IP) was measured at five frequencies between 1.6 and 16 GHz. The bulk density rho(b) was also measured for all the samples, and the bulk chemical composition (BCC) was determined for 56 of the samples. RP is found to be frequency-independent at 0.5-18 GHz for all samples, and rho(b) accounts for about 50 percent of the observed variance. For silicate rocks, as much as 78 percent of the variance is explained by the combination of rho(b) and the fractional contents of oxides when the silicates are subgrouped by genesis. In contrast, IP decreases with increasing frequency for most rock samples, and no statistically significant relationships are found between IP and rho(b). For subgrouped silicate rocks, 60 percent of the variance in IP can be explained by BCC.

Ulaby, Fawwaz T.↗

Beagle 2: The Next Exobiology Mission to Mars

Beagle 2 is a 60 kg probe (with a 30 kg lander) developed in the United Kingdom for inclusion on the European Space Agency's 2003 Mars Express. Beagle 2 will deliver to the Martian surface a payload which consists of a high percentage of science instruments to landed spacecraft mass. Beagle 2 will be launched in June, 2003 with Mars Express on a Soyuz-Fregat rocket from the Baikonur Cosmodrome in Kazakhstan. Beagle 2 will land on Mars on December 26, 2003 in the Isidis Planitia basin (approximately 10 degrees N and 275 degrees W), a large sedimentary basin that overlies the boundary between ancient highlands and northern plains. Isidis Planitia, the third largest basin on Mars, which is possibly filled with sediment deposited at the bottom of long-standing lakes or seas, offers an ideal environment for preserving traces of life. Beagle 2 was developed to search for organic material and other volatiles on and below the surface of Mars in addition to the study of the inorganic chemistry and mineralogy. Beagle 2 will utilize a mechanical mole and grinder to obtain samples from below the surface, under rocks and inside rocks. A pair of stereo cameras will image the landing site along with a microscope for examination of surface and rock samples. Analyses will include both rock and soil samples at various wavelengths, X-ray spectrometer and Mossbauer spectrometer as well as a search for organics and other light element species (e.g. carbonates and water) and measurement of their isotopic compositions. Beagle 2 has as its focus the goal of establishing whether evidence for life existed in the past on Mars at the Isidis Planitia site or at least establishing if the conditions were ever suitable. Carbonates and organic components were first recognized as existing on Mars when they were found in the Martian meteorite Nakhla. Romanek et al showed the carbonates in ALH84001 were formed at low temperatures. McKay et al noted possible evidence of early life on Mars within the ALH84001 meteorite. Thomas-Keprta et al showed the magnetite biomarkers in ALH84001's carbonates are indistinguishable from those formed by magnetotactic bacteria found on Earth. Gibson et al showed there was significant evidence for liquid water and biogenic products present on Mars across a 3.9 billion year period. A mechanical arm (PAW) operates from the lander and is used for science operations along with sample acquisition. Instruments attached to the PAW include: stereo cameras, Mossbauer instrument, X-ray fluorescence instrument, microscope, environmental sensors, rock corer/grinder, a spoon, mirror, brushes, a mole attachment for acquisition of subsurface to depths of 1 to 2 meters and an illumination device. Each camera has 14 filters which have been optimized for mineralogy composition, dust and water vapor detection. The microscope's camera is designed for viewing the size and shape of dust particles, rock surfaces, microfossils, and characteristics of the samples prior to introduction into the gas analysis package (GAP). The camera has a resolution of 4 microns/pixel, features four color capability (red, green, blue and UV (ultraviolet) fluoresence), a depth of focus of 40 micrometers and translation stage of +3 millimeters. The heart of the Beagle 2's life detection package is the gas analysis package (GAP), which consists of a mass spectrometer with collectors at fixed masses for precise isotopic ratio measurements and voltage scanning for spectral analysis. Primary aim of the GAP is to search for the presence of bulk constituents, individual species, and isotopic fractionations for both extinct and extent life along with studying the low-temperature geochemistry of the hydrogen, carbon, nitrogen and oxygen components on Mars from both the surface and atmosphere. GAP is a magnetic sector mass spectrometer with the range of 1 to 140 amu which can be operated in both the static and dynamic modes. A triple Faraday collector array will be used for C, N and O ratios along with a double Faraday array for H/D. Pulse counting electron multiplier will be utilized for noble gases and selected organics. Anticipated detection limits are at the picomole level for operation in the static mode of operation and high precision isotopic measurements will be made in the dynamic mode. Sample processing and preparation system consists of reaction vessels along with references. Sample ovens capable of being heated are attached to the manifold for sample combustion. Surface, subsurface materials and interior rock specimens will be combusted in pure oxygen gas at various temperature intervals to release organic matter and volatiles. Combustion process will permit detection of all forms and all atoms of carbon present in the samples. A chemical processing system is capable of a variety of conversion reactions. Gases are manipulated either by cryogenic or chemical reactions and passed through the gas handling portion of the vacuum system. There are two modes of operation: quantitative analysis and precise isotopic measurements. Additional information is contained in the original extended abstract.

Gibson, Everett K., Jr.↗