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Vacuum resonant-cavity dielectrometer for in situ measurements of complex permittivity in simulated space environment
Work performed on the permittivity of seawater and ice at 100 GHz was described. Measurements on water covered the temperature range from 0 to 50 C, while the measurements on ice were taken near - 10 C. In addition, a small number of measurements were made on the reflectivity of absorber materials used in a previous program on research in millimeter wave techniques. Normal incidence reflectivity was measured, and the result was used to obtain the index of refraction. For the case of normal incidence, reflectivity at a fixed temperature was reproducible to 1% for values near 40%. For reflectivity measurements on ice, the lack of attenuation leads to reflection from the back surface of the sample; this complication was circumvented by using a wedge shaped sample and freezing the water in a container lined with absorber material.
Two-coupler microwave technique measures complex permittivity utilizing waveguide which encloses gas or aerosol. Using technique, blower continuously circulates substances to keep them homogeneous.
A spectral-domain Galerkin method is used to calculate the dispersion characteristics of wide slotlines on low-permittivity substrates that are electrically thin. The range of parameters covered are d/lambda sub 0 = 0.006-0.06, W/lambda sub 0 = 0.005-2.0, and epsilon sub r = 2.22, 3.0, 3.8, and 9.8. The choice of expansion and testing functions makes possible the extraction of the asymptotic form of the infinite integrals, resulting in a computationally efficient solution. The agreement between calculated and measured slot wavelengths on narrow and wide slots is generally within 2.0 percent over 2-6 GHz.
Causal solutions for effective relative complex permittivities of plasmas are derived. Both lossless and lossy plasmas are considered.
The causality of the complex permittivity for a plasma model in which both loss and restoring terms are included is shown. Discussions as to what occurs in this causality property when the loss and restoring terms vanish are presented. Results are shown to agree with earlier work.
Complex refractive index and dielectric permittivity studies of presently used Space Shuttle tile materials at millimeter wavelengths reveal these tiles to exhibit similar absorption characteristics to those of fused silica materials. This absorption is mainly related to the water content in the specimen. A strong birefringence is observed at least in one of these fibrous refractory composite materials.
This paper presents a measurement system used for w-band complex permittivity measurements performed in NASA Langley Research Center's Electromagnetics Research Branch. The system was used to characterize candidate radome materials for the passive millimeter wave (PMMW) camera experiment. The PMMW camera is a new technology sensor, with goals of all-weather landings of civilian and military aircraft. The sensor is being developed under a NASA Technology Reinvestment program with TRW, McDonnell- Douglas, Honeywell, and Composite Optics, Inc. as participants. The experiment is scheduled to be flight tested on the Air Force's 'Speckled Trout' aircraft in late 1997. The camera operates at W-band, in a radiometric capacity and generates an image of the viewable field. Because the camera is a radiometer, the system is very sensitive to losses. Minimal transmission loss through the radome at the operating frequency, 89 GHz, was critical to the success of the experiment. This paper details the design, set-up, calibration and operation of a free space measurement system developed and used to characterize the candidate radome materials for this program.
Ferroelectric liquid crystalline polymers (LCPs) with a high spontaneous polarization (P s ) are of great interest for the fabrication of advanced electronic devices. However, conventional ferroelectric LCPs typically exhibit low spontaneous polarization, only around 1 mC/m 2 . To increase the orientational polarization for ferroelectric LCPs, in this work, we designed mesogen-free comb-shaped LCPs based on isotactic polyepichlorohydrin, which contained highly dipolar sulfonyl groups (dipole moment of 4.5 Debye) in the side chains. The goal was to increase dipole density and induce ferroelectric switching. In this new series of mesogen-free LCPs, the sulfonyl groups were first moved away from the main chain to mitigate strong dipole–dipole interactions. Second, methyl-branched alkyl side chains were implemented to decrease the crystallizability and induce the Smectic C (SmC) self-assembly. Intriguingly, these SmC samples, for the first time, exhibited typical paraelectric behavior (i.e., slim S-shaped single hysteresis loops) with a high dielectric constant in the range of 20–30. Finally, learning from the knowledge obtained from this study, we will be able to design new mesogen-free LCPs with tailor-made dipole–dipole interactions and realize ferroelectricity.
Sulfonated polysulfone is a promising membrane material for separation and energy generation processes that rely on membranes to control the rates of small-molecule (e.g., water and ions) transport. The interactions among water molecules, ions, and the sulfonate groups in these polymers play a key role in controlling these rates of transport, but much remains unknown about these fundamental interactions in sulfonated polymers. In this study, we used dielectric relaxation spectroscopy to characterize water molecule dynamics in sulfonated polysulfone and Nafion. We found that the charged sulfonate groups contribute to a restriction of water molecule dynamics (i.e., a reduction in the characteristic time scale of dipolar motions) in a manner that is governed by the concentration and nature (i.e., conjugate base strength) of the sulfonate group. Additionally, we develop strategies to use these data to aid in modeling ion transport in sulfonated polysulfone. These results may be useful to guide engineering strategies for polymeric membranes.
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The relative dielectric constant and loss tangent of lunar sample 14163,164 (fine dust) were determined as a function of density at 9.375, 24, 35, and 60 GHz. In addition, such measurements have also been performed on lunar sample 14310,74 (solid rock) at 9.375 GHz. The loss tangent was found to be frequency independent at these test frequencies and had a value of 0.015 for the lunar dust sample.
The research performed and the data obtained on candidate space shuttle antenna window and heat shield materials are presented. The measurement technique employs a free-space focused beam microwave bridge for obtaining RF transmission data, and a device which rotates a sample holder which is heated on one side by natural gas-air flames. The surface temperature of each sample is monitored by IR pyrometry; embedded and rear surface thermocouples are also used in obtaining temperature data. The surface of the sample undergoing test is subjected to approximately the same temperature/time profile that occurs at a proposed antenna position on the space shuttle as it re-enters. The samples are cycled through ten of these temperature profiles to determine the recycling effects. Very little change was noted in the materials due to the recycling.
The recent measurements on the dielectric properties of soils shows that the variation of dielectric constant with moisture content depends on soil types. The observed dielectric constant increases only slowly with moisture content up to a transition point. Beyond the transition it increases rapidly with moisture content. The moisture value of transition region was found to be higher for high clay content soils than for sandy soils. Many mixing formulas were compared with, and were found incompatible with, the measured dielectric variations of soil-water mixtures. A simple empirical model was proposed to describe the dielectric behavior of ths soil-water mixtures. The relationship between transition moisture and wilting point provides a means of estimating soil dielectric properties on the basis of texture information.
Measurements of reflectivity of water and ice at 100 GHz, 140 GHz, and 180 GHz are reported. Measurements on water covered the temperature range 0 C to 50 C. No anomalies in the dielectric properties of water due to the presence of either salts or organic matter were found. The reflectivity of water and its temperature dependence are consistent with recent dielectric property models derived from data at other wavelengths. The index of refraction of fresh ice is constant at 1.78 throughout this regions.
Recent measurements on the dielectric properties of soils have shown that the variation of dielectric constant with moisture content depends on soil types. The observed dielectric constant increases only slowly with moisture content up to a transition point. Beyond the transition it increases rapidly with moisture content. The moisture value at transition region was found to be higher for high clay content soils than for sandy soils. Many mixing formulas reported in the literature were compared with, and were found incompatible with, the measured dielectric variations of soil-water mixtures. A simple empirical model was proposed to describe the dielectric behavior of the soil-water mixtures. This model employs the mixing of either the dielectric constants or the refraction indices of ice, water, rock, and air, and treats the transition moisture value as an adjustable parameter. The calculated mixture dielectric constants from the model were found to be in reasonable agreement with the measured results over the entire moisture range of 0-0.5 cu cm/cu cm. The transition moistures derived from the model range from 0.16 to 0.33 and are strongly correlated with the wilting points of the soils estimated from their textures. This relationship between transition moisture and wilting point provides a means of estimating soil dielectric properties on the basis of texture information.
An attempt is made to draw some quantitative conclusions regarding the anisotropy of the clear-air back-scattering mechanism based on the measured variation of echo power with zenith angle. The measurements were made by the SOUSY group of the Max Planck Institute for Aeronomy at Lindau, FRG. They installed their 47-MHz transmitter and antenna feed in the 300-meter diameter reflector at Arecibo. The resulting 1.7-degree beam was stepped successively through seven 1.7-degree intervals from 1.7 to 11.7 degrees in zenith angle, obtaining about four minutes of data at each setting. This procedure was carried out in an eastward pointing azimuth and in a northward pointing azimuth, the entire set of measurements consuming an hour and twenty minutes. Range resolution was 150 meters.