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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3
All sourcesNASA NTRSDOE OSTI
DOE OSTI2020

Ceramic encapsulated metal phase change material for high temperature thermal energy storage

Thermal energy storage (TES) is a broad-based technology for reducing CO₂ emissions and advancing concentrating solar, fossil, and nuclear power through improvements in efficiency and economics. Phase change materials (PCMs) are of interest as TES media because of their ability to store large amounts of heat in relatively small volumes. The volume expansion during a phase change, typically between a solid and liquid, can cause breakage of protective coatings. This paper reports on the fabrication of a ceramic encapsulated metal (CEM) high temperature TES technology using a rotary calcining furnace and a fluidized bed chemical vapor deposition coating technique. Aluminum beads were chosen as the PCM because Al has a high melting point (660 °C), low cost, high heat of fusion, and an ability to form a thin, strong alumina layer capable of supporting the Al melt for subsequent processing. Quite remarkably, this study shows that 1 mm diameter Al can be fluidized up to at least 1500 °C in an appropriate atmosphere while maintaining a spheroid geometry. This allowed for producing a first of a kind CEM whereby Al particles were encapsulated in pyro-carbon (PyC) and high purity, dense chemical vapor deposited SiC. The CEM with a PyC only coating was exposed to thermal cycling to test the performance with a differential scanning calorimeter; the melting point and latent heat were measured to be 648.4 ± 2.8 °C and 293.3 ± 6.2 J/g respectively. It was demonstrated that the CEM design is possible to produce, laying the foundation for manufacturing of high temperature, tunable, TES media.

25 ENERGY STORAGE↗
NASA NTRS1977

Thermodynamic property determination in low gravity

Techniques for determining heat capacities and other properties of molten metals were investigated and critically evaluated. Precisely determining heat capacities calorimetrically in space poses several problems. The weight of a drop calorimeter block along with the necessity of obtaining a large number of data points tend to make traditional approaches appear infeasible. However, for many substances exhibiting sufficiently high thermal conductivities and with known emissivities, it appears possible to investigate their properties by observing the rate of cooling of a levitated sphere which is initially at a uniform temperature above the melting point. A special advantage of the levitation method is that considerable supercooling is expected, making the study of the heat capacities of molten metals both above and below their melting points possible.

Margrave, J. L.↗
NASA NTRS1994

Heat capacity and thermal relaxation of bulk helium very near the lambda point

In October 1992 a low temperature experiment was flown on the Space Shuttle in low Earth orbit. The objective of the mission was to measure the heat capacity and thermal conductivity of helium very close to the lambda point with the smearing effect of gravity removed. We report preliminary results from the experiment, and compare them with related measurements performed on the ground. The sample was s sphere of helium 3.5 cm in diameter contained within a copper calorimeter of vey high thermal conductivity. The calorimeter was attached to a pair of high resolution paramagnetic salt thermometers with noise levels in the 10(exp -10) K range and suspended from a high stability thermal isolation system. During the mission we found that the resolution of the thermometers was degraded somewhat due to the impact of charged particles. This effect limited the useful resolution of the measurements to about two nanokelvins from the lambda point. The results reported here are limited to about ten nanokelvins from the transition.

Lipa, John A.↗
DOE OSTI2024

Aluminum relaxation as the source of excess low energy events in low threshold calorimeters

A previously unexplained background called the Low Energy Excess has negatively impacted the reach of a variety of low threshold calorimeters including light dark matter direct detection and coherent elastic neutrino-nucleus scattering experiments. The relaxation of stressed aluminum films as mediated by the motion of dislocations may account for these observations.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS2017

Characterization of a 50kW Inductively Coupled Plasma Torch for Testing of Ablative Thermal Protection Materials

With the development of new manned spaceflight capabilities including NASA's Orion capsule and the Space-X Dragon capsule, there is a renewed importance of understanding the dynamics of ablative thermal protection systems. To this end, a new inductively coupled plasma torch facility is being developed at UT-Austin. The torch operates on argon and/or air at plasma powers up to 50 kW. In the present configuration the flow issues from a low-speed subsonic nozzle and the hot plume is characterized using slug calorimetry and emission spectroscopy. Preliminary measurements using emission spectroscopy have indicated that the torch is capable of producing an air plasma with a temperature between 6,000 K and 8,000 K depending on the power and flow settings and an argon plasma with a temperature of approximately 12,000 K. The operation envelope was measured, and heat flux measured for every point within the envelope using both a slug calorimeter and a Gardon gauge heat flux sensor. The torch was found to induce a stagnation point heat flux of between 90 and 225 W/sq cm.

Greene, Benton R.↗
DOE OSTI2024

ANALYSIS OF SUITABLE METHODOLOGIES FOR COMPRESSOR MASS FLOW RATE CORRECTION TO OTHER SUPERHEAT LEVELS AND REFRIGERANTS

This paper investigates the impact of suction conditions and refrigerant on scroll compressor mass flow rate by using calorimeter tests from AHRI-11 and AHRI-21 reports, published by AHRI's Low-GWP Alternative Refrigerants Evaluation program. Two Copeland scroll compressors (20 and 51 cm3) have been analyzed including different suction conditions (SH = 11K, SH = 22K, Ti = 18ºC) and several refrigerants (R134a, R32, R410A, R404A, etc.). Previous studies have explored response surfaces for energy consumption and mass flow rate variables. This study aims to expand the analysis by identifying the optimal approach to extrapolate mass flow rate from specific suction conditions to others SH or suction temperature levels and refrigerants. The current compressor characterization standard relies on the 1981 Dabiri correlation to correct compressor mass flow rate with suction conditions. Thus, this study aims to assess the adequacy of this correction and explore alternative correction methods for improved results.

Marchante Avellaneda, Javier↗
NASA NTRS1981

Undercooling measurement in a low-gravity containerless environment

A technique is described for measuring the amount of undercooling for samples processed in a low-gravity containerless environment. The time of undercooling is determined by measuring the time of cooling before nucleation and recalescence by two infrared detectors. Once the cooling curve for each drop is calculated, the amount of undercooling can then be found. The technique is demonstrated by measuring the amount of undercooling for drops of pure niobium and select compositions of the niobium-germanium alloy system while free falling in a 32 n evacuated drop tube. The total hemispherical emissivities and specific heats for these materials were measured using a high-temperature containerless calorimeter. An overview of the effect of undercooling on drops of niobium and niobium-germanium is given.

Robinson, M. B.↗
DOE OSTI2021

Low Temperature Microcalorimeters for Decay Energy Spectroscopy

Low Temperature Detectors have been used to measure embedded radioisotopes in a measurement mode known as Decay Energy Spectroscopy (DES) since 1992. DES microcalorimeter measurements have been used for applications ranging from neutrino mass measurements to metrology to measurements for safeguards and medical nuclides. While the low temperature detectors have extremely high intrinsic energy resolution (several times better than semiconductor detectors), the energy resolution achieved in practice is strongly dependent on factors such as sample preparation method. This review seeks to present the literature consensus on what has been learned by looking at the energy resolution as a function of various choices of detector, absorber, and sample preparation methods.

47 OTHER INSTRUMENTATION↗
DOE OSTI2022

Silicon alloying enhances fast heating rate combustion of aluminum particles

Alloys and composites of aluminum (Al) have shown promise in regulating and enhancing particle combustion for energy generation applications. Recent work on aluminum-silicon (Al-Si) spherical alloy particles has shown improved combustion at low heating rates through enhanced diffusion accompanying a lower melting temperature. This study extends reactivity analysis to higher heating rates, comparing oxidation of Al-Si with Al. Flame speeds of Al-Si powder mixed with molybdenum trioxide (MoO 3 ) powder (Al-Si+MoO 3 ) exhibited a faster transition to steady propagation relative to Al+MoO 3 . Bomb calorimetry experiments revealed up to 5.8% greater early temperature rise for Al-Si powder. Rapid steady propagation for Al-Si mixture and faster temperature rise for Al-Si particles were attributed to accelerated kinetics evidenced in thermal equilibrium analysis of the mixtures using a differential scanning calorimeter (DSC). Larger DSC exotherms in the early stages of oxidation (i.e., 480–720 °C) correlated with early heat release and promoted steady flame propagation for Al-Si+MoO 3 compared with Al+MoO 3 . Furthermore, in multiple heating rate DSC studies, Al-Si+MoO 3 ignited at a lower heating rate (i.e., 15 ⁰C/min) than Al+MoO 3 (i.e., 20 ⁰C/min). Both mixtures ignited at temperatures less than 625 °C which is above the melting temperature of Al-Si (574 °C) and below Al (659 °C). Thus, alloy particle fuels with enhanced diffusion-controlled kinetics promote steady flame propagation and show promise for energy generation applications. This is especially promising for technologies driven by enhanced condensed phase combustion such as some propellant additives or applications dependent on reliable burn rates such as pyrotechnic time delay formulations and primers.

36 MATERIALS SCIENCE↗
DOE OSTI2025

Heating effects on jack pine pyrogenic organic matter properties from a pyrocosm study in 2022

This dataset contains data associated with the preprint “Fire removes preexisting pyrogenic organic matter from the ecosystem through the mechanisms of both direct combustion and increasing mineralizability” (Luo et al., 2025b), which is the complementary study to the published paper “Reburning pyrogenic organic matter: a laboratory method for dosing dynamic heat fluxes from above” (Luo et al., 2025a). We designed a full-factorial experiment with different burial depths of jack pine (Pinus banksiana Lamb) pyrogenic organic matter (PyOM) (Surface, 1 cm, and 5 cm) and different heat-flux profiles (High, Low, and Control) to examine how subsequent fires affect the properties of preexisting PyOM. We measured total carbon (C), pH, dissolved organic carbon (DOC), dissolved inorganic carbon (DIC), and mineralized C (as CO₂-C, from a 12-week incubation).We found that high heat flux and/or surface placement resulted in substantial direct C losses through combustion. Intermediate heat exposure produced both combustion losses and increases in DOC and mineralizability, which may have complex long-term implications: an increased dissolved fraction of PyOM may promote downward transport into mineral soils and potentially contribute to deeper, longer-term C storage, but it may also make PyOM more susceptible to microbial decomposition. Under the lowest heat flux and deepest burial, most PyOM was retained, and changes in DOC and C mineralization were minimal. Finally, PyOM pH, an important chemical property, decreased under low-temperature heating but increased under higher temperatures.We uploaded pH data for all samples (“pH_of_all_samples.csv”); pH and temperature-related data (peak temperature and degree hours) for samples in High and Low heat-flux treatments (“pH_vs_peakT_and_degree_hours_only_for_heated_samples.csv”); total C data (“CN_pct_C_stock_C_loss_in_samples.csv”); DOC and DIC data (“doc_dic.csv”); and mineralized C (CO₂-C) data (“CO2-C_all_original.csv”). Additional details can be found in the Methods & Sampling section.All datasets uploaded to ESS-DIVE are clearly labeled, cleaned, and include both raw and derived data, ready for reuse in other analyses. All analysis code and raw datasets are also available on GitHub: https://github.com/MengmengLuo/Fire-removes-preexisting-pyrogenic-organic-matter-from-the-ecosystem.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1983

SSME main combustion chamber life prediction

Typically, low cycle fatigue life is a function of the cyclic strain range, the material properties, and the operating temperature. The reusable life is normally defined by the number of strain cycles that can be accrued before severe material degradation occurs. Reusable life is normally signified by the initiation or propagation of surface cracks. Hot-fire testing of channel wall combustors has shown significant mid-channel wall thinning or deformation during accrued cyclic testing. This phenomenon is termed cyclic-creep and appears to be significantly accelerated at elevated surface temperatures. This failure mode was analytically modelled. The cyclic life of the baseline SSME-MCC based on measured calorimeter heat transfer data, and the life sensitivity of local hot spots caused by injector effects were determined. Four life enhanced designs were assessed.

Cook, R. T.↗
NASA NTRS1999

Thermal Performance of the XRS Helium Insert

The X-Ray Spectrometer (XRS) is an instrument on the Japanese Astro-E satellite, scheduled for launch early in the year 2000. The XRS Helium Insert comprises a superfluid helium cryostat, an Adiabatic Demagnetization Refrigerator (ADR), and the XRS calorimeters with their cold electronics. The calorimeters are capable of detecting X-rays over the energy range 0.1 to 10 keV with a resolution of 12 eV. The Helium Insert completed its performance and verification testing at Goddard in January 1999. It was shipped to Japan, where it has been integrated with the neon dewar built by Sumitomo Heavy Industries. The Helium Insert was given a challenging lifetime requirement of 2.0 years with a goal of 2.5 years. Based on the results of the thermal performance tests, the predicted on-orbit lifetime is 2.6 years with a margin of 30%. This is the result of both higher efficiency in the ADR cycle and the low temperature top-off, more than compensating for an increase in the parasitic heat load. This paper presents a summary of the key design features and the results of the thermal testing of the XRS Helium Insert.

Breon, Susan R.↗
NASA NTRS1996

Emulsion Chamber Technology Experiment (ECT)

The experimental objective of Emulsion Chamber Technology (ECT) was to develop space-borne emulsion chamber technology so that cosmic rays and nuclear interactions may subsequently be studied at extremely high energies with long exposures in space. A small emulsion chamber was built and flown on flight STS-62 of the Columbia in March 1994. Analysis of the several hundred layers of radiation-sensitive material has shown excellent post-flight condition and suitability for cosmic ray physics analysis at much longer exposures. Temperature control of the stack was 20 +/-1 C throughout the active control period and no significant deviations of temperature or pressure in the chamber were observed over the entire mission operations period. The unfortunate flight attitude of the orbiter (almost 90% Earth viewing) prevented any significant number of heavy particles (Z greater than or equal to 10) reaching the stack and the inverted flow of shower particles in the calorimeter has not allowed evaluation of absolute primary cosmic ray-detection efficiency nor of the practical time limits of useful exposure of these calorimeters in space to the level of detail originally planned. Nevertheless, analysis of the observed backgrounds and quality of the processed photographic and plastic materials after the flight show that productive exposures of emulsion chambers are feasible in low orbit for periods of up to one year or longer. The engineering approaches taken in the ECT program were proven effective and no major environmental obstacles to prolonged flight are evident.

Gregory, John C.↗
NASA NTRS2001

Overall Thermal Performance of Flexible Piping Under Simulated Bending Conditions

Flexible, vacuum-insulated transfer lines for low-temperature applications have higher thermal losses than comparable rigid lines. Typical flexible piping construction uses corrugated tubes, inner and outer, with a multilayer insulation (MLI) system in the annular space. Experiments on vacuum insulation systems in a flexible geometry were conducted at the Cryogenics Test Laboratory of NASA Kennedy Space Center. The effects of bending were simulated by causing the inner tube to be eccentric with the outer tube. The effects of spacers were simulated in a controlled way by inserting spacer tubes for the length of the cylindrical test articles. Two material systems, standard MLI and a layered composite insulation (LCI), were tested under the full range of vacuum levels using a liquid nitrogen boiloff calorimeter to determine the apparent thermal conductivity (k-value). The results indicate that the flexible piping under simulated bending conditions significantly degrades the thermal performance of the insulation system. These data are compared to standard MLI for both straight and flexible piping configurations. The definition of an overall k-value for actual field installations (k(sub oafi)) is described for use in design and analysis of cryogenic piping systems.

Fesmire, James E.↗
NASA NTRS2019

Magnetic Calorimeter Option for the Lynx X-Ray Microcalorimeter

One option for the detector technology to implement the Lynx x-ray microcalorimeter (LXM) focal plane arrays is the metallic magnetic calorimeter (MMC). Two-dimensional imaging arrays of MMCs measure the energy of x-ray photons by using a paramagnetic sensor to detect the temperature rise in a microfabricated x-ray absorber. While small arrays of MMCs have previously been demonstrated that have energy resolution better than the 3 eV requirement for LXM, we describe LXM prototype MMC arrays that have 55,800 x-ray pixels, thermally linked to 5688 sensors in “hydra” configurations, and that have sensor inductance increased to avoid signal loss from the stray inductance in the large-scale arrays when the detectors are read out with microwave superconducting quantum interference device multiplexers, and that use multilevel planarized superconducting wiring to provide low-inductance, low-crosstalk connections to each pixel. We describe the features of recently tested MMC prototype devices and simulations of expected performance in designs opti- mized for the three subarray types in LXM.

Stevenson, Thomas R.↗
NASA NTRS2013

Future Development Trajectories for Imaging X-rays Spectrometers Based on Microcalorimeters

Future development trajectories for imaging x-ray spectrometers based on microcalorimeters. Since their invention 30 years ago, the capability of X-ray microcalorimeters has increased steadily, with continual improvements in energy resolution, speed, and array size. Arrays of up to 1024 pixels have been produced, and resolution better than 1 eV at 1.5 keV has been achieved. These detectors can be optimized for the highest priority science, such as designing for the highest resolving power at low energies at the expense of dynamic range, or the greatest focal-plane coverage at the expense of speed. Three types of X-ray microcalorimeters presently dominate the field, each characterized by the thermometer technology. The first two types use temperature-sensitive resistors: semiconductors in the metal-insulator transition and superconductors operated in the superconducting-normal transition. The third type uses a magnetically coupled thermometer, and is at an earlier stage of development than the other two. The Soft X-ray Spectrometer (SXS) on Astro-H, expected to launch in 2015, will use an array of silicon thermistors with HgTe X-ray absorbers that will operate at 50 mK. Both the semiconductor and superconductor calorimeters have been implemented in small arrays. Kilopixel arrays of the superconducting calorimeters are being produced, and much larger arrays may require the non-dissipative advantage of magnetically coupled thermometers. I will project the development trajectories of these detectors and their read-out technologies and assess what their capabilities and limitations will be 10 - 20 years from now.

Kilbourne, Caroline A.↗
NASA NTRS2011

Ares I-X Ascent Base Environments

Plume induced base heating environments were measured during the flight of the NASA Constellation Ares I-X developmental launch vehicle, successfully flown on October 28, 2009. The Ares IX first stage is a four segment Space Shuttle derived booster with base consisting of a flared aft skirt, deceleration and tumble motors, and a thermal curtain surrounding the first stage 7.2 area ratio nozzle. Developmental Flight Instrumentation (DFI) consisted of radiometers, calorimeters, pressure transducers and gas temperature probes installed on the aft skirt and nozzle to measure the base environments. In addition, thermocouples were also installed between the layers of the flexible thermal curtain to provide insight into the curtain response to the base environments and to assist in understanding curtain failure during reentry. Plume radiation environment predictions were generated by the Reverse Monte Carlo (RMC) code and the convective base heating predictions utilized heritage MSFC empirical methods. These predictions were compared to the DFI data and results from the flight videography. Radiation predictions agreed with the flight measured data early in flight but gauge failures prevented high altitude comparisons. The convective environment comparisons demonstrated the need to improve the prediction methodology; particularly for low altitude, local plume recirculation. The convective comparisons showed relatively good agreement at altitudes greater than 50,000 feet.

Mobley, B. L.↗
NASA NTRS2015

Study of the Residual Background Events in Ground Data from the ASTRO-HSXS Microcalorimeter

The measured instrumental background of the XRS calorimeter spectrometer of Suzaku had several sources, including primary cosmic rays and secondary particles interacting with the pixels and with the silicon structure of the array. Prior to the launch of Suzaku, several data sets were taken without x-ray illumination to study the characteristics and timing of background signals produced in the array and anti-coincidence detector. Even though the source of the background in the laboratory was different from that in low-earth orbit (muons and environmental gamma-rays on the ground versus Galactic cosmic-ray (GCR) protons and alpha particles in space), the study of correlations and properties of populations of rare events was useful for establishing the preliminary screening parameters needed for selection of good science data. Sea-level muons are singly charged minimum-ionizing particles, like the GCR protons, and thus were good probes of the effectiveness of screening via the signals from the anti-coincidence detector. Here we present the first analysis of the on-ground background of the SXS calorimeter of Astro-H. On XRS, the background prior to screening was completely dominated by coincident events on many pixels resulting from the temperature pulse arising from each large energy deposition (greater than 200 keV) into the silicon frame around the array. The improved heat-sinking of the SXS array compared with XRS eliminated these thermal disturbances, greatly reducing the measured count rate in the absence of illumination. The removal of these events has made it easier to study the nature of the residual background and to look for additional event populations. We compare the SXS residual background to that measured in equivalent ground data for XRS and discuss these preliminary results.

ASTRO-H↗