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NASA NTRS1995

High Modulus and High T(sub g) Thermally Stable Polymers from p-Ethynyl-Terminated Rigid-Rod Monomers

Novel p-ethynyl-substituted rigid rod monomers were studied by pressure Differential Scanning Calorimetry (DSC), ThermoGravimetric Analysis (TGA), IsothermoGravimetric Analysis (IGA), and TGA-IR. These monomers, 4,4'-bis(((4-ethynylphenyl)carbonyl)oxy)biphenyl, designated 1, 1,5-bis-(((4-ethynylphenyl)carbonyl)oxy)naphthalene, designated 2, and bis(4-ethynylphenyl)pyromellitimide, designated 3, were polymerized in the solid state. Thermal polymerization in N2 or air produced highly cross-linked resins with polymerization exotherms centered between 212 and 276 C. The (delta)H's of polymerization of these resins in air were found to be double those in N2. When monomers 1 and 2 were heated in air from 23 to 750 C at 10 C/min, the main decomposition product was carbon dioxide, evolving at a maximum rate between 500 and 600 C; water was also detected as a decomposition product. Void-free neat resin moldings, designated lp to 3p, were made by compression molding the monomers and then heating them. The resulting polymers were highly cross-linked, and their glass transition temperatures (T(sub g)) were much higher than their polymerization temperatures. Using ThermoMechanical Analysis (TMA), we found that polymers lp to 3p had T(sub g)'s of 422, 329, and 380 C, respectively. The thermal and thermooxidative stabilities improved when lp to 3p were postcured in N2 (the postcured polymers were designated 1pp to 3pp). The Linear Thermal Expansions (LTE) for lp and 3p were 1% between 23 and 420 C. Using rheological analysis, we could not clearly detect the T(sub g)'s of lp to 3p because their moduli dropped only slightly between 23 and 490 C and the changes in tan beta were very low. Because of high cross-link density, their moduli changed little as the resins went from a glassy to a rubbery state. Their shear storage moduli in air ranged from 0.82 (3p, 3pp) to 1.6 GPa (lpp) at 23 C, from 0.16 (2p) to 0.7GPa(lpp) at 380 C, and from 0.18(lpp)to 0.6GPa(2p) at 490 C. Finally, these novel-p-ethynyl polymers exhibited an excellent combination of high T(sub g), low LTE, and high thermooxidative stability. Most notably, 3pp lost only 3% of its initial weight when it was aged for 500 h at 288 C in air.

Melissaris, Anastasios P.↗

NASA NTRS1999

The Lunar Prospector Mission: Final Results of Trajectory Design, Quasi-Frozen Orbits, Extended Mission Targeting, and Lunar Topography and Potential Models

The National Aeronautics and Space Administration (NASA) selected Lunar Prospector (LP) as one of the discovery missions to conduct solar system exploration science investigations. The mission was NASA's first lunar voyage to investigate key science objectives since Apollo and was launched in January 1998. In keeping with discovery program requirements to reduce total mission cost and utilize new technology, Lunar Prospector's mission design and control will focus on the use of innovative and proven trajectory analysis programs. As part of this effort, the Goddard Space Flight Center and the Ames Research Center became partners in the Lunar Prospector trajectory team to provide the trajectory analysis and orbit determination support. At the end of 1998, Lunar Prospector completed its one-year primary mission at 100-km altitude above the lunar surface. On December 19, 1998, Lunar Prospector entered its extended mission phase. The mission orbit was lowered from 100 km to a mean altitude of 40 km. Due to lunar potential effects, the altitude of Lunar Prospector varied from 25 to 55 km above the mean lunar geoid. After one month at 40 km, the lunar potential model was updated based upon the new tracking data at 40 km. On January 15, 1999, the altitude was lowered again to a mean altitude of 30 km. The spherical altitude varied between 15 km and 45 km above the mean lunar geoid while the topographical altitude varied between 10 km and 50 km. Various means were employed to get accurate lunar surface elevation including Clementine altimetry and LOS analysis. Based upon the best available terrain maps, Lunar Prospector reached actual altitudes of 8 km above lunar mountains in the southern polar region. This extended mission phase of six months will enable LP to obtain science data up to 3 orders of magnitude better than at the mission orbit. At the end of the operations mission, LP was targeted for impact at a chosen location that allowed optical observation of the lunar ejecta as LP ended its mission at 1.6 km/sec. This paper details the trajectory design and orbit determination planning and actual results of the Lunar Prospector nominal and extended mission including maneuver design, eccentricity vs. argument of perigee evolution, topographical altitude estimation, and lunar potential modeling. This paper provides understanding of the quasi-frozen orbit design of the LP mission, the optimization process of lunar orbit targets, the impacts that the selected lunar potential models play, and discusses the feasibility of meeting the mission goals. Observed evolution of the Keplerian orbit elements are compared to the theoretical predictions using the latest lunar potential model available which incorporates the Lunar Prospector Doppler data. Mapping orbit maintenance maneuver design along with results of the actual maneuvers to maintain the orbital requirements are also presented.

Folta, David↗

NASA NTRS2004

Revisiting the Interpretation of Thorium Abundances at Hansteen Alpha

Hansteen Alpha is one of the few remaining locations on the Moon thought to be formed by highlands volcanism. Hansteen Alpha is a triangular shaped feature located in the southern portion of Oceanus Procellarum (12 degrees W, 50 degrees S) and its size is approximately 25 km on each side. As described by Hawke et al., there is clear evidence that: 1) Hansteen Alpha was emplaced by extrusive volcanic processes; and 2) it was formed by a viscous lava that should be enriched in Th. However, in the study of Hawke et al. using available Lunar Prospector (LP) Th data, it was concluded that the Hansteen Alpha region was not greatly enriched in Th as would be expected for a highly evolved, viscous lava. It was further concluded based on other compositional data that the magma that formed Hansteen Alpha did not correspond to any known rock type. Here we revisit the interpretation of Th abundances at Hansteen Alpha for a couple of reasons. First, the size of Hansteen Alpha is smaller than the spatial resolution of the LP Gamma-ray Spectrometer (LP-GRS) from which the Th abundances were derived. Therefore, the LP-GRS pixels covering Hansteen Alpha may not truly represent the Th abundance of the Hansteen Alpha feature. Second, recent work has led to a much greater understanding of the Th spatial distribution for small-area features on the lunar surface. In particular, using forward modeling techniques, we have developed the ability to obtain information about Th abundances for features that are at or smaller than the FWHM spatial resolution (approximately [80 square kilometers]) of the LP-GRS data.

Lawrence, D. J.↗

NASA NTRSDate not supplied

Ten Year Ozone Profile Record From Suomi NPP OMPS Limb Profiler

In this study, we evaluate a decadal ozone profile record derived from Suomi NPP Ozone Mapping and Profiler Suite (OMPS) Limb Profiler (LP). The data from OMPS LP were re-processed with the new retrieval algorithm from 2012 to present. The new reprocessing includes adjustments in both Level 1 and Level 2 algorithms. The sensor’s altitude registration, updates in radiometric calibrations, under-sampling and stray light corrections were addressed in Level 1 processing. The new retrieval algorithm (version 2.7) combines measurements from UV and VIS parts of the spectra to retrieve a single vertical ozone profile between 12.5 km (or cloud tops) and 57.5 km, unlike to previous version 2.5 where ozone profiles were retrieved independently from UV and VIS. To improve ozone retrievals in the Upper Troposphere Lower Stratosphere (UTLS) region, we implemented a new aerosol correction that assumes a gamma-function particle size distribution. In addition, ozone and nitrogen dioxide cross sections and climatologies were updated. We discuss sensitivity of the ozone retrievals to implemented changes in Level 1 and Level 2 algorithms. We focus our analysis on evaluation of the stability of the 10-year record from OMPS LP. We show results from the internal methods for characterizing the stability of the LP altitude registration and compare the LP reflectivity and ozone with the similar quantities measured by OMPS nadir sensors. Finally, we will show results from comparisons with independent satellite (MLS and SAGE III) and ozone sonde measurements.

Ozone↗

NASA NTRSDate not supplied

Comparisons of ozone profile retrievals from the OMPS Limb Profiler and ACE-FTS

The OMPS Limb Profiler (OMPS LP) was launched in October 2011, and has more than 10 years of overlap with ACE-FTS. Therefore, ACE-FTS offers an excellent opportunity to obtain independent ozone profile data with which to validate OMPS LP ozone retrievals. In this study we utilize ACE-FTS ozone retrievals to evaluate 10 years of OMPS LP profile measurements processed with the new NASA GSFC version 2.6 retrieval algorithm. The OMPS LP is a solar scattering instrument that makes observations in the sunlit portion of the Earth, whilst ACE-FTS is a solar occultation instrument that measures ozone only at sunrise and sunset. To account for these differences in measurement times we use the Goddard Diurnal Ozone Climatology (GDOC). Diurnal adjustments using this climatology have been shown to help reduce biases above 30 km. Our analysis shows that biases between OMPS LP v2.6 and ACE-FTS v5.2 are <10% between 18 and 45 km, and increase above and below these altitudes. The vertical patterns of the differences are similar across different latitudes and seasons, with larger seasonal variations observed in the Northern Hemisphere. We also analyze ozone time series from the two instruments.

Atmospheric Science, Stratospheric Ozone↗

NASA NTRSDate not supplied

Process Development and Hot-fire Testing of Additively Manufactured NASA HR-1 for Liquid Rocket Engine Applications

Additive manufacturing (AM) has provided new design and manufacturing opportunities to reduce cost and schedules, consolidate parts, and optimize performance. One technique being evaluated is Laser Powder Directed Energy Deposition (LP-DED), which provides a significant increase in scale compared to Laser Powder Bed Fusion (L-PBF). NASA along with industry partners have been developing the LP-DED process to demonstrate internal channel geometry and development components for use in liquid rocket engine channel cooled nozzles. Optimized materials in the extreme high pressure and hydrogen environment for liquid rocket engines remains a key challenge. NASA has advanced an enabling material called NASA HR-1 (Hydrogen Resistant -1) as a solution using AM techniques. NASA HR-1 is a high-strength Fe-Ni superalloy designed to resist high pressure, hydrogen environment embrittlement, oxidation, and corrosion. NASA HR-1 meets materials requirements for liquid rocket engine components, including good hydrogen resistance, high conductivity, good low cycle fatigue performance, and high elongation and strength for components in high heat flux environments. Material properties and process characterization have been completed on the high density thin-wall material in addition to advancements of the supply chain. NASA has also completed fabrication of several subscale and full-scale channel wall nozzles in LP-DED NASA HR-1 and completed hot-fire testing. This includes refinement of the process to produce thin-walls and various channel geometries to meet the requirements for channel wall nozzle applications. This paper will provide an overview of the LP-DED process development, material characterization and properties, component manufacturing, and hot-fire testing. Hot-fire testing was completed for a lander-class 7K-lbf thrust chamber using Liquid Oxygen (LOX)/Methane. The design overview and results from hot-fire testing will be presented in addition to hardware development for future testing on 2K-lbf and 35k-lbf thrust chambers and large-scale manufacturing technology demonstrators.

DED↗

NASA NTRSDate not supplied

Process Development and Hot-fire Testing of Additively Manufactured NASA HR-1 for Liquid Rocket Engine Applications

Additive Manufacturing↗

NASA NTRSDate not supplied

Experimental Characterization of Surface Roughness and Geometric Evaluations of Thin-Wall Laser Powder Directed Energy Deposition

Additive Manufacturing (AM) has offered many new design and manufacturing opportunities for components across various industries. As AM evolves there is a need to better understand outputs of the process including geometric limitations and surface roughness based on specific application requirements. One possible application area of AM are components using thin-wall (<2 mm) microchannel heat exchangers for subsystems across aerospace, and industrial applications. AM offers the opportunity to significantly reduce the cost and lead time associated with fabricating these complex parts with internal features such as an array of cooling channels. Laser Powder Bed Fusion (L-PBF) has been continuously demonstrated as a technique to fabricate heat exchangers with internal geometric complexities. However, L-PBF is limited in the scale at which parts can be fabricated. Laser Powder Directed Energy Deposition (LP-DED) has been demonstrated as an AM technology to significantly increase the scale of which thin-wall microchannel heat exchangers could be manufactured. Successful deployment of the LP-DED technology requires critical understanding of the resulting features from the build process. Surface roughness is one of the critical areas that effects the friction factor and pressure drop within a heat exchanger and must be well understood. This presentation will provide an overview of the characterization work completed to understand the LP-DED process for thin-walls representative of hydrogen resistant alloy NASA HR-1 that would be used in a Hydrogen-environment application. An overview of the experiments conducted with varying LP-DED parameters, evaluation of various geometric channel and geometric build features and resulting surface finish will be provided along with a summary of conclusions from these experiments. Results indicate that powder size is a major contributor and surface roughness varies between closed channel shapes and external surfaces.

Directed Energy Deposition↗

NASA NTRS1991

Evaluation of the minority carrier diffusion length and surface-recombination velocity in GaAs p/n solar cells

The minority carrier diffusion length (Lp) and the surface recombination velocity (Vs) were measured as a function of distance (x) from the p-n junction in GaAs p/n concentrator solar cells. The measured Vs values were used in a theoretical expression for the normalized electron-beam-induced current. A fitting procedure was then used to fit this expression with experimental values to obtain Lp. The results show that both Vs and Lp vary with x. Lp measured in irradiated cells showed a marked reduction. These values were compared to those measured previously which did not account for Vs.

Hakimzadeh, Roshanak↗

NASA NTRS1995

Can standard cosmological models explain the observed Abell cluster bulk flow?

Lauer and Postman (LP) observed that all Abell clusters with redshifts less than 15,000 km/s appear to be participating in a bulk flow of 689 km/s with respect to the cosmic microwave background. We find this result difficult to reconcile with all popular models for large-scale structure formation that assume Gaussian initial conditions. This conclusion is based on Monte Carlo realizations of the LP data, drawn from large particle-mesh N-body simulations for six different models of the initial power spectrum (standard, tilted, and Omega(sub 0) = 0.3 cold dark matter, and two variants of the primordial baryon isocurvature model). We have taken special care to treat properly the longest-wavelength components of the power spectra. The simulations are sampled, 'observed,' and analyzed as identically as possible to the LP cluster sample. Large-scale bulk flows as measured from clusters in the simulations are in excellent agreement with those measured from the grid: the clusters do not exhibit any strong velocity bias on large scales. Bulk flows with amplitude as large as that reported by LP are not uncommon in the Monte Carlo data stes; the distribution of measured bulk flows before error bias subtraction is rougly Maxwellian, with a peak around 400 km/s. However the chi squared of the observed bulk flow, taking into account the anisotropy of the error ellipsoid, is much more difficult to match in the simulations. The models examined are ruled out at confidence levels between 94% and 98%.

Strauss, Michael A.↗

NASA NTRS1998

A Low Precipitation Supercell over the Southeast US: A Case Study

On 28 March 1997 a low precipitation supercell storm was observed 125 km east of Memphis, TN. The storm exhibited a visual appearance similar to that of Great Plains low precipitation (LP) supercells while it was being video typed for 35 min. beginning at 2335 UTC. While the storm produced hailstones up to 4.5 cm in diameter, and had a 4 hour lifetime, tornadoes were absent. However, over 20 tornadoes were produced in Kentucky and Tennessee (TN) by other thunderstorms during that afternoon and evening. The purpose of this paper is to document this LP supercell that occurred in the Southeastern US. To the authors' knowledge an LP storm has not yet been documented in the Southeastern US. This paper presents a detailed overview of the LP supercell, including synoptic conditions, radar observations, lightning data and visual observations of the storm.

Robert, Barry C.↗

NASA NTRS1999

Lunar Prospector Orbit Determination Uncertainties Using the High Resolution Lunar Gravity Models

The Lunar Prospector (LP) mission began on January 6, 1998, when the LP spacecraft was launched from Cape Canaveral, Florida. The objectives of the mission were to determine whether water ice exists at the lunar poles, generate a global compositional map of the lunar surface, detect lunar outgassing, and improve knowledge of the lunar magnetic and gravity fields. Orbit determination of LP performed at the Jet Propulsion Laboratory (JPL) is conducted as part of the principal science investigation of the lunar gravity field. This paper will describe the JPL effort in support of the LP Gravity Investigation. This support includes high precision orbit determination, gravity model validation, and data editing. A description of the mission and its trajectory will be provided first, followed by a discussion of the orbit determination estimation procedure and models. Accuracies will be examined in terms of orbit-to-orbit solution differences, as a function of oblateness model truncation, and inclination in the plane-of-sky. Long term predictions for several gravity fields will be compared to the reconstructed orbits to demonstrate the accuracy of the orbit determination and oblateness fields developed by the Principal Gravity Investigator.

Carranza, Eric↗

NASA NTRS2009

The OMPS Limb Profiler Instrument: An Alternative Data Analysis and Retrieval Algorithm

The upcoming Ozone Mapper and Profiler Suite (OMPS), which will be launched on the NPOESS Preparatory Project (NPP) platform in early 2011, will continue monitoring the global distribution of the Earth's middle atmosphere ozone and aerosol. OMPS is composed of three instruments, namely the Total Column Mapper (heritage: TOMS, OMI), the Nadir Profiler (heritage: SBUV) and the Limb Profiler (heritage: SOLSE/LORE, OSIRIS, SCIAMACHY, SAGE III). The ultimate goal of the mission is to better understand and quantify the rate of stratospheric ozone recovery. The focus of the paper will be on the Limb Profiler (LP) instrument. The LP instrument will measure the Earth fs limb radiance (which is due to the scattering of solar photons by air molecules, aerosol and Earth surface) in the ultra-violet (UV), visible and near infrared, from 285 to 1000 nm. The LP simultaneously images the whole vertical extent of the Earth's limb through three vertical slits, each covering a vertical tangent height range of 100 km and each horizontally spaced by 250 km in the cross-track direction. The focal plane of the LP spectrometer is a two ]dimensional CCD array comprised of 340 x 740 pixels. Several data analysis tools are presently being constructed and tested to retrieve ozone and aerosol vertical distribution from limb radiance measurements. The primary NASA algorithm is based on earlier algorithms developed for the SOLSE/LORE and SAGE III limb scatter missions. The paper will describe an alternative algorithm which will retrieve ozone density and aerosol extinction directly from radiance data collected on individual CCD pixels. This alternative method uses an optimal estimation approach to retrieve ozone and aerosol in the 10-60 km range from the information contained within an ensemble of about 50000 down-linked pixels. Tangent height registration is performed using the Rayleigh Scattering Attitude Sensor (RSAS) technique applied to columns of pixels in the 340-360 nm range. Cloud height is determined by analyzing the radiance first derivative along pixel columns at longer wavelengths. Wavelength registration is performed using rows of pixels and identifying Fraunhofer solar lines within the measured spectra. Special attention is given to stray-light decontamination and modeling of the measured finite spectral/spatial line shape functions.

Rault, Didier F.↗

NASA NTRS2014

Release 2 data products from the Ozone Mapping and Profiler Suite (OMPS) Limb Profiler

The OMPS Limb Profiler (LP) was launched on board the NASA Suomi National Polar-orbiting Partnership (SNPP) satellite in October 2011. OMPS-LP is a limb-scattering hyperspectral sensor that provides ozone profiling capability at 1.5 km vertical resolution from cloud top to 60 km altitude. The use of three parallel slits allows global coverage in approximately four days. We have recently completed a full reprocessing of all LP data products, designated as Release 2, that improves the accuracy and quality of these products. Level 1 gridded radiance (L1G) changes include intra-orbit and seasonal correction of variations in wavelength registration, revised static and intra-orbit tangent height adjustments, and simplified pixel selection from multiple images. Ozone profile retrieval changes include removal of the explicit aerosol correction, exclusion of channels contaminated by stratospheric OH emission, a revised instrument noise characterization, improved synthetic solar spectrum, improved pressure and temperature ancillary data, and a revised ozone climatology. Release 2 data products also include aerosol extinction coefficient profiles derived with the prelaunch retrieval algorithm. Our evaluation of OMPS LP Release 2 data quality is good. Zonal average ozone profile comparisons with Aura MLS data typically show good agreement, within 5-10% over the altitude range 20-50 km between 60 deg S and 60 deg N. The aerosol profiles agree well with concurrent satellite measurements such as CALIPSO and OSIRIS, and clearly detect exceptional events such as volcanic eruptions and the Chelyabinsk bolide in February 2013.

Limb scatter↗

NASA NTRS2018

Improvement of Stratospheric Aerosol Extinction Retrieval from OMPS/LP Using a New Aerosol Model

The Ozone Mapping and Profiler Suite Limb Profiler (OMPS/LP) has been flying on the Suomi National Polar-orbiting Partnership (S-NPP) satellite since October 2011. It is designed to produce ozone and aerosol vertical profiles at 2-kilometer vertical resolution over the entire sunlit globe. Aerosol extinction profiles are computed with Mie theory using radiances measured at 675 nanometers. The operational Version 1.0 (V1.0) aerosol extinction retrieval algorithm assumes a bimodal lognormal aerosol size distribution (ASD) whose parameters were derived by combining an in situ measurement of aerosol microphysics with the Stratospheric Aerosol and Gas Experiment (SAGE II) aerosol extinction climatology. Internal analysis indicates that this bimodal lognormal ASD does not sufficiently explain the spectral dependence of LP-measured radiances. In this paper we describe the derivation of an improved aerosol size distribution, designated Version 1.5 (V1.5), for the LP retrieval algorithm. The new ASD uses a gamma function distribution that is derived from Community Aerosol and Radiation Model for Atmospheres (CARMA)-calculated results. A cumulative distribution fit derived from the gamma function ASD gives better agreement with CARMA results at small particle radii than bimodal or unimodal functions. The new ASD also explains the spectral dependence of LP-measured radiances better than the V1.0 ASD. We find that the impact of our choice of ASD on the retrieved extinctions varies strongly with the underlying reflectivity of the scene. Initial comparisons with collocated extinction profiles retrieved at 676 nanometers from the SAGE III instrument on the International Space Station (ISS) show a significant improvement in agreement for the LP V1.5 retrievals. Zonal mean extinction profiles agree to within 10 percent between 19 and 29 kilometers, and regression fits of collocated samples show improved correlation and reduced scatter compared to the V1.0 product. This improved agreement will motivate development of more sophisticated ASDs from CARMA results that incorporate latitude, altitude and seasonal variations in aerosol properties.

Ozone Mapping Profiler Suite Limb Profiler (OMPS/L↗

NASA NTRS2019

Joint Assimilation of the Aura Microwave Limb Sounder and Ozone Mapping and Profiler Suite Limb Profiler Data: Towards a Reanalysis of Stratospheric Ozone for Trend Studies

The future trajectory of the stratospheric ozone recovery will be sensitive to greenhouse gas concentrations through thermal control of chemical loss and via stratospheric circulation changes. The latter in particular is subject to considerable uncertainty meriting continuing monitoring of the evolution of ozone throughout the depth of the stratosphere. Atmospheric reanalyses utilize the data assimilation methodology to obtain comprehensive representations of the state of the atmosphere, including its composition, on multidecadal scales by combining diverse measurements from satellite-borne and conventional data sources. Systematic biases among these various data types pose a challenge for assimilation by introducing spurious discontinuities that affect the utility of reanalyses for studies of long-term variability and trends.In this presentation we will outline an approach, developed at NASA's Global Modeling and Assimilation Office (GMAO), that allows joint assimilation of stratospheric ozone profiles from the Microwave Limb Sounder (MLS) on EOS Aura and the Ozone Mapping and Profiler Suite Limb Profiler (OMPS-LP) currently flying on the Suomi-NPP satellite with future missions projected into the 2030s. We will demonstrate that a simple offline correction significantly reduces biases between MLS and OMPS-LP ozone data providing a strategy for generating a long-term vertically resolved homogenized representation of stratospheric ozone in future reanalyses. One novel element of our approach compared to previous GMAO reanalysis is the use of a version of the Goddard Earth Observing System model with full stratospheric chemistry. We will show selected comparisons of MLS and OMPS-LP assimilation experiments with independent ozonesonde and satellite data as well as two examples of process-based evaluation focused on the 2016 QBO disruption and Arctic winter ozone loss focusing on the relative performance of the MLS and OMPS-LP analyses.

Wargan, K.↗

NASA NTRSDate not supplied

Hot-Fire Testing Results of Additively Manufactured NASA HR-1 towards Large Scale Implementation of Channel Wall Nozzles

Additive manufacturing (AM) has provided new design and manufacturing opportunities to reduce cost and schedules, consolidate parts, and optimize performance. One technique being evaluated is Laser Powder Directed Energy Deposition (LP-DED), which provides a significant increase in scale compared to Laser Powder Bed Fusion (L-PBF). NASA along with industry partners have been developing the LP-DED process to demonstrate internal channel geometry and development components for use in liquid rocket engine channel cooled nozzles. One material that has been the focus of this development is NASA HR-1, an Iron-Nickel based superalloy optimized for use in high pressure hydrogen environments. Material properties and process characterization has been completed on the high density thin-wall material in addition to advancements of the supply chain. NASA has also completed fabrication of several subscale and full scale channel wall nozzles in LP-DED NASA HR-1 and completed hot-fire testing. This includes refinement of the process to produce thin-walls and various channel geometries to meet the requirements for channel wall nozzle applications. This paper will provide an overview of the LP-DED process development, material characterization and properties, component manufacturing, and hot-fire testing. Hot-fire testing was completed for a lander-class 7K-lbf thrust chamber using Liquid Oxygen (LOX)/Methane. The design overview and results from hot-fire testing will be presented in addition to hardware development for future testing on 2K-lbf and 35k-lbf thrust chambers and large-scale manufacturing technology demonstrators.

Paul Gradl↗

NASA NTRSDate not supplied

Effect of Heat Treatments on the Tensile Properties of Additively Manufactured 15-5 Ph Stainless Steel

This study investigated the effect of post-manufacture heat treatments on the microstructure and mechanical properties of 15-5 PH stainless steel (SS) fabricated by laser powder-directed energy deposition (LP-DED). Various heat treatment procedures (CA-H900 and CA-H1150) were conducted to evaluate their effects on the tensile behavior of LP-DED 15-5 PH SS. Scanning electron microscopy was used to characterize the microstructural features and the fracture surfaces. Tensile tests were performed to evaluate the mechanical properties at cryogenic and room temperatures. Reduction in area of CA-H1150 treated specimens after tensile tests was significantly higher than CA-H900 ones, while the ultimate tensile and yield strengths of CA-H900 specimens were higher compared to the CA-H1150 ones. The mechanical behavior of the LP-DED 15-5 PH SS in various heat treatment conditions is discussed based on their microstructures and fracture surfaces.

Laser powder directed energy deposition (LP-DED)↗