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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 55 records · Page 3
All sourcesNASA NTRSDOE OSTI
NASA NTRS1989

Total hemispherical emittance measured at high temperatures by the calorimetric method

A calorimetric vacuum emissometer (CVE) capable of measuring total hemispherical emittance of surfaces at elevated temperatures was designed, built, and tested. Several materials with a wide range of emittances were measured in the CVE between 773 to 923 K. These results were compared to values calculated from spectral emittance curves measured in a room temperature Hohlraum reflectometer and in an open-air elevated temperature emissometer. The results differed by as much as 0.2 for some materials but were in closer agreement for the more highly-emitting, diffuse-reflecting samples. The differences were attributed to temperature, atmospheric, and directional effects, and errors in the Hohlraum and emissometer measurements (plus or minus 5 percent). The probable error of the CVE measurements was typically less than 1 percent.

Difilippo, Frank↗
NASA NTRS1987

Exposure time considerations in high temperature low cycle fatigue

The Conventional Strainrange Partitioning (CSRP) method for High-Temperature, Low-Cycle Fatigue (HTLCF) life prediction has its origins in the modeling of first-order, creep-fatigue waveform effects while treating as second-order effects, the influence of metallurgical or environmental time dependencies. Procedures are proposed to include the latter explicitly in the inelastic strainrange--life relations. For brevity, only the CP life relation will be presented in detail. The exposure-time effect within the CP inelastic strainrange (tensile creep reversed by compressive plasticity) was determined by tensile stresshold-time experiments for 316 SS at 816 C. Reductions in CP cyclic life of a factor of about two were observed with an increase in exposure time or a corresponding decrease in creep rate by a factor of about 100. The CP life relation has been modified to be expressed in terms of either Steady State Creep Rate (SSCR) or Exposure Time (ET). The applicability and accuracy of the time-dependent CP life relations is demonstrated by conducting verification experiments involving complex hysteresis loops. Metallographic examination revealed time-dependent degradation attributable to oxide formation and precipitation of carbides along grain boundaries.

Kalluri, S.↗
NASA NTRS1988

Exposure time considerations in high temperature low cycle fatigue

The Conventional Strainrange Partitioning (CSRP) method for High-Temperature, Low-Cycle Fatigue (HTLCF) life prediction has its origins in the modeling of first-order, creep-fatigue waveform effects while treating as second-order effects, the influence of metallurgical or environmental time dependencies. Procedures are proposed to include the latter explicitly in the inelastic strainrange-life relations. For brevity, only the CP life relation will be presented in detail. The exposure-time effect within the CP inelastic strainrange (tensile creep reversed by compressive plasticity) was determined by tensile stresshold-time experiments for 316 SS at 816 C. Reductions in CP cyclic life of a factor of about two were observed with an increase in exposure time or a corresponding decrease in creep rate by a factor of about 100. The CP life relation has been modified to be expressed in terms of either Steady State Creep Rate (SSCR) or Exposure Time (ET). The applicability and accuracy of the time-dependent CP life relations is demonstrated by conducting verification experiments involving complex hysteresis loops. Metallographic examination revealed time-dependent degradation attributable to oxide formation and precipitation of carbides along grain boundaries.

Kalluri, S.↗
NASA NTRS1950

Fundamental Effects of Aging on Creep Properties of Solution-Treated Low-Carbon N-155 Alloy

A method is developed whereby the fundamental mechanisms are investigated by which processing, heat treatment, and chemical composition control the properties of alloys at high temperatures. The method used metallographic examination -- both optical and electronic --studies of x-ray diffraction-line widths, intensities, and lattice parameters, and hardness surveys to evaluate fundamental structural conditions. Mechanical properties at high temperatures are then measured and correlated with these measured structural conditions. In accordance with this method, a study was made of the fundamental mechanism by which aging controlled the short-time creep and rupture properties of solution-treated low-carbon n-155 alloy at 1200 degrees F.

Frey, D N↗
NASA NTRS2001

High Temperature Fatigue Crack Growth Behavior of Alloy 10

Methods to improve the high temperature, dwell crack growth resistance of Alloy 10, a high strength, nickel-base disk alloy, were studied. Two approaches, heat treat variations and composition modifications, were investigated. Under the heat treat approach, solution temperature, cooling rates, and stabilization, were studied. It was found that higher solution temperatures, which promote coarser grain sizes, coupled with a 1550 F stabilization treatment were found to significantly reduce dwell crack growth rates at 1300 F Changes in the niobium and tantalum content were found to have a much smaller impact on crack growth behavior. Lowering the niobium:tantalum ratio did improve crack growth resistance and this effect was most pronounced for coarse grain microstructures. Based on these findings, a coarse grain microstructure for Alloy 10 appears to be the best option for improving dwell crack growth resistance, especially in the rim of a disk where temperatures can reach or exceed 1300 T. Further, the use of advanced processing technologies, which can produce a coarse grain rim and fine grain bore, would be the preferred option for Alloy 10 to obtain the optimal balance between tensile, creep, and crack growth requirements for small gas turbine engines.

Gayda, John↗
NASA NTRS2014

Experimental and Theoretical Study of Thermodynamics of the Reaction of Titania and Water at High Temperatures

The transpiration method was used to determine the volatility of titanium dioxide (TiO2) in water vapor-containing environments at temperatures between 1473 and 1673 K. Water contents ranged from 0 to 76 mole % in oxygen or argon carrier gases for 20 to 250 hr exposure times. Results indicate that oxygen is not a key contributor to volatilization and the primary reaction for volatilization in this temperature range is: TiO2(s) + H2O(g) = TiO(OH)2(g). Data were analyzed with both the second and third law methods to extract an enthalpy and entropy of formation. The geometry and vibrational frequencies of TiO(OH)2(g) were computed using B3LYP density functional theory, and the enthalpy of formation was computed using the coupled-cluster singles and doubles method with a perturbative correction for connected triple substitutions [CCSD(T)]. Thermal functions are calculated using both a structure with bent and linear hydroxyl groups. Calculated second and third heats show closer agreement with the linear hydroxyl group, suggesting more experimental and computational spectroscopic and structural work is needed on this system.

equilibrium↗
NASA NTRS1991

Structural characterization of high temperature composites

Glass, ceramic, and carbon matrix composite materials have emerged in recent years with potential properties and temperature resistance which make them attractive for high temperature applications such as gas turbine engines. At the outset of this study, only flexural tests were available to evaluate brittle matrix composites at temperatures in the 600 to 1000 C range. The results are described of an ongoing effort to develop appropriate tensile, compression, and shear test methods for high temperature use. A tensile test for unidirectional composites was developed and used to evaluate the properties and behavior of ceramic fiber reinforced glass and glass-ceramic matrix composites in air at temperatures up to 1000 C. The results indicate generally efficient fiber reinforcement and tolerance to matrix cracking similar to polymer matrix composites. Limiting properties in these materials may be an inherently very low transverse strain to failure, and high temperature embrittlement due to fiber/matrix interface oxidation.

Mandell, J. F.↗
NASA NTRS1970

Ultrasonic propagation in gases at high temperatures

Ultrasonic pulse method /1 to 3 MHz/ measures both sound speed and absorption in monatomic and polyatomic gases in a temperature range of 300 to 20000 degrees K at atmospheric pressure. Helium, nitrogen, oxygen, and argon are investigated.

Carey, C.↗
NASA NTRS1982

HOST high temperature crack propagation

Methods for characterizing and predicting crack growth at elevated temperatures are discussed. Nonlinear behavior, thermal gradients, and thermomechanical cycling are discussed.

Orange, T. W.↗
NASA NTRS2003

CVD aluminiding process for producing a modified platinum aluminide bond coat for improved high temperature performance

A method of depositing by chemical vapor deposition a modified platinum aluminide diffusion coating onto a superalloy substrate comprising the steps of applying a layer of a platinum group metal to the superalloy substrate; passing an externally generated aluminum halide gas through an internal gas generator which is integral with a retort, the internal gas generator generating a modified halide gas; and co-depositing aluminum and modifier onto the superalloy substrate. In one form, the modified halide gas is hafnium chloride and the modifier is hafnium with the modified platinum aluminum bond coat comprising a single phase additive layer of platinum aluminide with at least about 0.5 percent hafnium by weight percent and about 1 to about 15 weight percent of hafnium in the boundary between a diffusion layer and the additive layer. The bond coat produced by this method is also claimed.

Nagaraj, Bangalore A.↗
NASA NTRS2010

Titanium Hydroxide - a Volatile Species at High Temperature

An alternative method of low-temperature plasma functionalization of carbon nanotubes provides for the simultaneous attachment of molecular groups of multiple (typically two or three) different species or different mixtures of species to carbon nanotubes at different locations within the same apparatus. This method is based on similar principles, and involves the use of mostly the same basic apparatus, as those of the methods described in "Low-Temperature Plasma Functionalization of Carbon Nanotubes" (ARC-14661-1), NASA Tech Briefs, Vol. 28, No. 5 (May 2004), page 45. The figure schematically depicts the basic apparatus used in the aforementioned method, with emphasis on features that distinguish the present alternative method from the other. In this method, one exploits the fact that the composition of the deposition plasma changes as the plasma flows from its source in the precursor chamber toward the nanotubes in the target chamber. As a result, carbon nanotubes mounted in the target chamber at different flow distances (d1, d2, d3 . . .) from the precursor chamber become functionalized with different species or different mixtures of species.

Nguyen, QuynhGiao N.↗
NASA NTRS1998

Method Developed for the High-Temperature Nondestructive Evaluation of Fiber-Reinforced Silicon Carbide Ceramic Matrix Composites

Ceramic matrix composites have emerged as candidate materials to allow higher operating temperatures (1000 to 1400 C) in gas turbine engines. A need, therefore, exists to develop nondestructive methods to evaluate material integrity at the material operating temperature by monitoring thermal and mechanical fatigue. These methods would also have potential as quality inspection tools. The goal of this investigation at the NASA Lewis Research Center is to survey and correlate the temperature-dependent damping and stiffness of advanced ceramic composite materials with imposed thermal and stress histories that simulate in-service turbine engine conditions. A typical sample size of 100 by 4 by 2 cubic millimeters, along with the specified stiffness and density, placed the fundamental vibration frequencies between 100 and 2000 Hz. A modified Forster apparatus seemed most applicable to simultaneously measure both damping and stiffness. Testing in vacuum reduced the effects of air on the measurements. In this method, a single composite sample is vibrated at its fundamental tone; then suddenly, the mechanical excitation is removed so that the sample's motion freely decays with time. Typical results are illlustrated in this paper.

Goldsby, Jon C.↗
NASA NTRS1982

Bipulsating Technique for Silicon Production

Method controls reaction temperature and rate of reaction of sodium and silicon tetrafluoride by alternately adding measured amounts of reactants. Technique used in large reactor, where heat dissipation becomes serious problem, to control reactor temperatures. Highly efficient method, which would utilize almost 100 percent of raw materials.

Sanjurjo, A.↗
NASA NTRS2019

High temperature electric arc furnace and method

An apparatus and process for improving the microstructure of electrically conducting materials is disclosed by the present invention. A revolving heat source applies heat to the surface of the material evenly and quickly. One or more heat sinks quickly cool the material. In the preferred embodiment, the cooling may be done in such a way as to promote as high a degree of directional grain growth as desired or completely nondirectional grain growth.

Richard M Poorman↗
NASA NTRS1976

High Temperature Strain Gage Calibration Fixture

An apparatus and method are described for calibrating high temperature strain gases which serve for both dead weight and constant deflection measurements. A cantilever support arm allows the test unit to slide into a furnace while one end is subjected to bending strain either by hanging weights upon it or by deflecting it with a push rod. The dual nature of the fixture permits both tests to be run without change of the test specimen or removal from the furnace.

Vranas, T.↗
NASA NTRS1975

Creep analysis capability for stiffened panel structures

A method of analysis developed for predicting permanent cyclic creep deflections in stiffened panel structures is presented. The resulting computer program (TPSC, for Thermal Protection System Creep) applies either the time hardening or strain hardening theories of creep accumulation, using iterative techniques to determine structural rotations, creep strains, and stresses as a function of time. Deflections are determined by numerical integration of structural rotations along the panel length. The analytical approach was developed for purposes of analyzing thin gage entry vehicle metallic thermal protection system panels subjected to cyclic bending loads at high temperatures. The method is applicable to any panel subjected to bending loads. Predicted panel creep deflections are compared with results from cyclic tests of subsize and full size corrugation and rib stiffened panels. Empirical equations used in the analysis were developed for each material based on correlation with tensile cyclic creep data.

Cramer, B. A.↗