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All sources NASA NTRS DOE OSTI

NASA NTRS1982

Silicon crystal growth in vacuum

The most developed process for silicon crystal growth is the Czochralski (CZ) method which was in production for over two decades. In an effort to reduce cost of single crystal silicon for photovoltaic applications, a directional solidification technique, Heat Exchanger Method (HEM), was adapted. Materials used in HEM and CZ furnaces are quite similar (heaters, crucibles, insulation, etc.). To eliminate the cost of high purity argon, it was intended to use vacuum operation in HEM. Two of the major problems encountered in vacuum processing of silicon are crucible decomposition and silicon carbide formation in the melt.

Khattak, C. P.↗

NASA NTRS1984

Remanent magnetization of a 'paramagnetic' composition in the ilmenite-hematite solid solution stress

In the ilmenite-hematite solid solution series, compositions more ilmenite-rich than Ilm(73)Hem(27) are classically thought to be paramagnetic at room temperature. Ilm(80)Hem(20) samples have nevertheless been synthesized that acquire hard saturation remanent and thermoremanent moments. From analysis of AC demagnetization data, the source of the measured remanence is believed to be a single-domain (SD) like material within the IlM(80)Hem(20) grains themselves. On the basis of transmission electron microscope observations, it is suggested that transformation-induced domain boundaries, which in part are enriched in hematite component relative to the bulk composition of the grains, could act as the magnetic carrier of the SD-like remanence.

Lawson, C. A.↗

NASA NTRS2010

Astrobiology and the Human Exploration of Mars

In March 2007, the Mars Exploration Program Analysis Group (MEPAG) chartered the Human Exploration of Mars Science Analysis Group (HEM-SAG), co-chaired by J. B. Garvin and J. S. Levine and consisting of about 30 Mars scientists from the U.S. and Europe. HEM-SAG was one of a half dozen teams charted by NASA to consider the human exploration of Mars. Other teams included: Mars Entry, Descent and Landing, Human Health and Performance, Flight and Surface Systems, and Heliospheric/Astrophysics. The results of these Mars teams and the development of an architecture for the human exploration of Mars were summarized in two recent publications: Human Exploration of Mars Design Reference Architecture 5.0, NASA Special Publication-2009-566 (B. G. Drake, Editor), 100 pages, July 2009 and Human Exploration of Mars Design Reference Architecture 5.0, NASA Special Publication-2009-566 Addendum (B. G. Drake, Editor), 406 pages, July 2009. This presentation summarizes the HEM-SAG conclusions on astrobiology and the search for life on Mars by humans.

Levine, Joel S.↗

DOE OSTI2025

Optimizing Bendability and Hardness of Age-Hardenable Aluminum Sheets through Local Thermo-Mechanical Processing

This paper introduces a novel thermo-mechanical process to modify the local mechanical properties of 6xxx aluminum (Al-Mg-Si-Cu) alloy sheets. In this process, two pairs of rollers travel along the length of a sheet while locally bending and unbending it so that the final shape and thickness of the sheet remains unchanged. Room temperature bending/unbending (B/U) produces a deformation gradient through thickness and local hardening in both T4 and T6 sheets (with 41% and 18% greater Vickers hardness, respectively). High temperature bending/unbending performed at ~ 500°C via induction heating, produces significant improvements in local formability as measured by bend testing. Formability levels equivalent to the as-received T4 temper are achieved within the processed zones of T6 sheets with bend angles of ~ 150°, without disturbing the T6 temper in the remainder of the sheet. Finite element simulations and characterization explained the mechanical property improvements and the heterogenous microstructure with weakened Cube texture. Due to its similarity with the roller hemming process, and its compact dimensions, the apparatus developed for B/U has the potential for seamless integration with roller hemming robots to selectively process high strength aluminum sheet materials within mass-production settings.

Efe, Mert [BATTELLE (PACIFIC NW LAB)]↗

DOE OSTI2023

High-entropy materials: fundamentals and applications

Metallic high-entropy materials (HEMs), also known as high-entropy alloys (HEAs), are an exotic class of materials that possess desirable properties, such as exceptional strength and ductility, high wear resistance, and corrosion resistance. Due to these positive attributes, HEAs have been proposed for use in the automotive and aerospace industries, nuclear reactor technology, and the biomedical field. In terms of composition, HEAs contain five or more elements in amounts ranging from 5 to 35 atomic percent (at.%) each, resulting in a vast compositional space that is still mainly unexplored to this day. More recently, the field of HEMs has broadened to include materials such as polymers and ceramics.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Influence of Supporting Electrolyte on Hydroxide Exchange Membrane Water Electrolysis Performance: Anolyte

Hydroxide-exchange-membrane water electrolysis (HEMWE) is an emerging hydrogen-production pathway that combines many advantages of incumbent alkaline water electrolysis (AWE) and proton-exchange-membrane water electrolysis (PEMWE). Advancement in HEMWE has been accelerated with the development of stable and conductive hydroxide exchange membranes (HEMs) and a more comprehensive understanding of alkaline gas-evolving kinetics. However, performance and durability without supporting electrolytes (SELs) remain inferior to PEMWE and AWE and little is known about the role and impact of the SELs. This study investigates the effects of SELs used as anolyte solutions in HEMWEs including cation-type, anion-type, SEL conductivity and pH, presence of carbonates and increased cation/OH- ratios on cell voltage and stability. We report our findings that (i) cell potential and high-frequency resistance did not correlate with anolyte SEL conductivity, (ii) cation-type influences cell voltage at low current densities (<50 mA cm -2 ) as predicted by half-cell measurements, (iii) increased cation/OH- ratio causes increased overpotentials, and (iv) carbonates are exchanged in the HEM but removed via self-purging at high current density. Overall, this study concludes that concentrated KOH is still the best SEL.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1979

Silicon ingot casting: Heat exchanger method. Multi-wire slicing: Fixed abrasive slicing technique, phase 3

In the area of ingot casting the proof of concept of heat exchanger method (HEM) was established. It was also established that HEM cast silicon yielded solar cell performance comparable to Czochralski grown material. Solar cells with conversion efficiencies of up to 15% were fabricated. It was shown that square cross-section ingots can be cast. In the area of crystal slicing, it was established that silicon can be sliced efficiently with the fixed abrasive slicing technique approach. This concept was carried forward to 10 cm diameter workpiece.

Schmid, F.↗

NASA NTRS1979

Low-cost, high-efficiency silicon by heat exchanger method and fixed abrasive slicing technique

The paper describes the heat exchanger method (HEM) for growing silicon crystals. The problem of ingot cracking was solved by using a graded structure silica crucible, and vacuum processing eliminated expensive high-purity argon. Solar cells fabricated from HEM silicon demonstrated conversion efficiencies up to 15% (AM1) at low cost, using square cross-section, single crystal silicon. A modified multiblade slurry machine was adapted for multiwire fixed abrasive slicing of silicon which uses a diamond attached to wires; this method provides a conversion ratio of 1.08 sq m of wafer per kg of silicon ingot, and produces wafers free of edge chipping with a surface damage of 3-5 microns.

Khattak, C. P.↗

NASA NTRS1981

Silicon solar cell process development, fabrication and analysis

The fabrication of solar cells from several unconventional silicon materials is described, and cell performance measured and analyzed. Unconventional materials evaluated are edge defined film fed grown (EFG), heat exchanger method (HEM), dendritic web grown, and continuous CZ silicons. Resistivity, current voltage, and spectral sensitivity of the cells were measured. Current voltage was measured under AM0 and AM1 conditions. Maximum conversion efficiencies of cells fabricated from these and other unconventional silicons were compared and test results analyzed. The HEM and continuous CZ silicon were found to be superior to silicon materials considered previously.

Minahan, J. A.↗

NASA NTRS1980

Silicon solar cell process development, fabrication, and analysis

Solar cells from HEM, Dendritic Webs, and EFG ribbons were fabricated and characterized. The HEM solar cells showed only slight enhancement in cell performance after gettering steps (diffusion glass) were added. Dendritic webs from various growth runs indicated that performance of solar cells made from the webs was not as good as that of the conventional CZ cells. The EFG ribbons grown in CO ambient showed significant improvement in silicon quality.

Yoo, H. I.↗

NASA NTRS1983

Silicon solar cell process development, fabrication and analysis

Measurements of minority carrier diffusion lengths were made on the small mesa diodes from HEM Si and SILSO Si. The results were consistent with previous Voc and Isc measurements. Only the medium grain SILSO had a distinct advantage for the non grain boundary diodes. Substantial variations were observed for the HEM ingot 4141C. Also a quantitatively scaled light spot scan was being developed for localized diffusion length measurements in polycrystalline silicon solar cells. A change to a more monochromatic input for the light spot scan results in greater sensitivity and in principle, quantitative measurement of local material qualities is now possible.

Leung, D. C.↗

NASA NTRS1992

Magnetic hysteresis of p(+) and He-3(2+) irradiated melt-textured YBa2Cu3O(7-delta)

We have measured the magnetic hysteresis loops and temperature dependent trapped fields in melt-textured YBa2Cu3O(7-delta) samples before and after p(+) and He-3(2+) irradiation using a Hall effect magnetometer (HEM) as well as a commercial vibrating sample magnetometer (VSM). For proper He-3(2+) fluence, the critical current density may be enhanced by a factor of 10. Calculations based on various critical state models show that before the irradiation, the hysteresis loops can be well accounted for by a critical current density of a modified power law field dependence. After the irradiation, the best fit has been achieved by using an exponential form. Jc and its field dependence deduced from HEM hysteresis loops are in good agreement with those deduced from the VSM loops, suggesting that the Hall effect magnetometer can be conveniently used to characterize bulk high Tc oxide superconductors.

Song, S. N.↗

NASA NTRS1983

Solar Cells

The Heat Exchanger Method (HEM) produces high efficiency crystal ingots in an automated well-insulated furnace offering low equipment, labor and energy costs. The "grown" silicon crystals are used to make solar cells, or photovoltaic cells which convert sunlight directly into electricity. The HEM method is used by Crystal Systems, Inc. and was developed under a NASA/Jet Propulsion Laboratory contract. The square wafers which are the result of the process are sold to companies manufacturing solar panels.

Source record↗

NASA NTRS2011

Simulation Based Training Improves Airway Management for Helicopter EMS Teams

The use of paralytic medications in the performance of RSI intubation is a high risk intervention used by many HEMS crews. There is no margin for error in RSI intubation as the results can be fatal. Operating room access for airway management training has become more difficult, and is not representative of the environment in which HEMS crews typically function. LifeEvac of Virginia designed and implemented an SST airway management program to provide a realistic, consistent training platform. The dynamic program incorporates standardized scenarios, and real life challenging cases that this and other programs have encountered. SST is done in a variety of settings including the helicopter, back of ambulances, staged car crashes and simulation centers. The result has been the indoctrination of a well defined, consistent approach to every airway management intervention. The SST program facillitates enhancement of technical skills. as well as team dynamics and communication.

Dhindsa, Harinder S.↗

NASA NTRS2016

Mars Surface System Common Capabilities and Challenges for Human Missions

NASA has begun a process to identify and evaluate candidate locations where humans could land, live and work on the martian surface. These locations are referred to as Exploration Zones (EZs). Given current mission concepts, an EZ is a collection of Regions of Interest (ROIs) that are located within approximately 100 kilometers of a centralized landing site. ROIs are areas that are relevant for scientific investigation and/or development/maturation of capabilities and resources necessary for a sustainable human presence. The EZ also contains a landing site and a habitation site that will be used by multiple human crews during missions to explore and utilize the ROIs within the EZ. In parallel with this process, NASA continues to make progress on the Evolvable Mars Campaign examining alternatives that can pioneer an extended human presence on Mars that is Earth independent. This involves ongoing assessments of surface systems and operations to enable a permanent, sustainable human presence. Because of the difficulty in getting equipment and supplies to the surface of Mars, part of these assessments involve identifying those systems and processes that can perform in multiple, sometimes completely unrelated, situations. These assessments have been performed in a very generic surface mission carried out at a very generic surface location. As specific candidate EZs are identified it becomes important to evaluate the current suite of surface systems and operations as they are likely to perform for the specific locations and for the types of operations - both scientific and development - that are proposed for these EZs. It is also important to evaluate the proposed EZs for their suitability to be explored or developed given the range of capabilities and constraints for the types of surface systems and operations being considered within the EMC. This means looking at setting up and operating a field station at a central location within the EZ as well as traversing to and exploring the scientific ROIs within the boundaries of the EZ. The proposed paper will describe the current status of common systems and operations as they can be applied to actual EZ locations on Mars. Initially these EZs will be the four locations identified MEPAG's Human Exploration of Mars Science Analysis Group (HEM‐SAG) that will be used as representative of the EZs that will emerge from the process that NASA has initiated. An example process that could be commonly applied is an approach for developing a field station site plan that would be demonstrated by applying this process to each of the four HEM‐SAG sites. Examples of common systems include (a) mobility systems that can be used to off‐load and move payloads to specific locations at the central field station location that could also be used to traverse long distances to reach some of the more remote ROIs or (b) robotic systems that can support various activities (such as system set up and maintenance) at the field station that could also be used to explore scientific ROIs and used to support site‐specific ISRU production activities.

Hoffman, Stephen J.↗

NASA NTRS2016

Mars Surface Systems Common Capabilities and Challenges for Human Missions

This paper describes the current status of common systems and operations as they are applied to actual locations on Mars that are representative of Exploration Zones (EZ) - NASA's term for candidate locations where humans could land, live and work on the Martian surface. Given NASA's current concepts for human missions to Mars, an EZ is a collection of Regions of Interest (ROIs) located within approximately 100 kilometers of a centralized landing site. ROIs are areas that are relevant for scientific investigation and/or development/maturation of capabilities and resources necessary for a sustainable human presence. An EZ also contains a habitation site that will be used by multiple human crews during missions to explore and utilize the ROIs within the EZ. The Evolvable Mars Campaign (EMC), a description of NASA's current approach to these human Mars missions, assumes that a single EZ will be identified within which NASA will establish a substantial and durable surface infrastructure that will be used by multiple human crews. The process of identifying and eventually selecting this single EZ will likely take many years to finalized. Because of this extended EZ selection process it becomes important to evaluate the current suite of surface systems and operations being evaluated for the EMC as they are likely to perform at a variety of proposed EZ locations and for the types of operations - both scientific and development - that are proposed for these candidate EZs. It is also important to evaluate proposed EZs for their suitability to be explored or developed given the range of capabilities and constraints for the types of surface systems and operations being considered within the EMC. Four locations identified in the Mars Exploration Program Analysis Group (MEPAG)'s Human Exploration of Mars Science Analysis Group (HEM-SAG) report are used in this paper as representative of candidate EZs that will emerge from the selection process that NASA has initiated. A field station site plan is developed for each of these four HEM-SAG sites. Because of the difficulty in getting equipment and supplies to the surface of Mars, specific assessments have been conducted to identify those systems and processes that can perform in multiple, sometimes completely unrelated, situations. Examples of common systems that are assessed at all of these sites include: (a) habitation and associated logistics storage systems, (b) a centralized power plant capable of supplying power to a geographically distributed (but within the central habitation zone) set of systems, (c) mobility systems that can be used to off-load and move payloads to specific locations at the central field station location that could also be used to traverse long distances to reach some of the more remote ROIs and (d) robotic systems that can support various activities (such as system set up and maintenance) at the field station that could also be used to explore scientific ROIs and used to support site-specific ISRU (In Situ Resource Utilization) production activities.

Toups, Larry↗

DOE OSTI2021

Improving the Power Outage Resilience of Buildings with Solar PV through the Use of Battery Systems and EV Energy Storage

Buildings with solar photovoltaic (PV) generation and a stationary battery energy storage system (BESS) may self-sustain an uninterrupted full-level electricity supply during power outages. The duration of off-grid operation is dependent on the time of the power fault and the capabilities of the home energy management system (HEMS). In this paper, building resilience is quantified by analyzing the self-sustainment duration for all possible power outages throughout an entire year. An evaluation method is proposed and exercised on a reference house in California climate zone 9 for which the detailed electricity usage is simulated using the EnergyPlus software. The influence of factors such as energy use behavioral patterns, energy storage capacity from the BESS, and an electric vehicle (EV) battery on the building resilience is evaluated. Varying combinations of energy storage and controllable loads are studied for optimally improved resilience based on user preferences. It is shown that for the target home and region with a solar PV system of 7.2 kW, a BESS with a capacity of 11 kWh, and an EV with a battery of 80 kWh permanently connected to the home, off-grid self-sustained full operation is guaranteed for at least 72 h.

14 SOLAR ENERGY↗

DOE OSTI2020

High-Entropy Metal Sulfide Nanoparticles Promise High-Performance Oxygen Evolution Reaction

Transition metal sulfide with a multi-elemental nature represents a class of promising catalysts for oxygen evolution reaction (OER) owing to its good catalytic activity. However, its synthesis remains a grand challenge due to the thermodynamic immiscibility of the constituent multimetallic elements in a sulfide structure. Herein, we for the first time report a high-entropy metal sulfide (HEMS, i.e., (CrMnFeCoNi)Sx) solid solution nanoparticles. Computational and X-ray photoelectron spectroscopy analysis suggest that the (CrMnFeCoNi)S x exhibits a synergistic effect among metal atoms that leads to desired electronic states to enhance OER activity. The (CrMnFeCoNi)Sx nanoparticles showed one of the best activities (low overpotential 295 mV at 100 mA cm -2 in 1 M KOH solution) and good durability (only slight polarization after 10 hours by chronopotentiometry) compared with the unary, binary, ternary, and quaternary sulfide counterparts. This work opens up a new synthesis paradigm for high-entropy compound nanoparticles for highly efficient electrocatalysis applications.

25 ENERGY STORAGE↗