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At least 55 records · Page 3

Report on FY 2023 Research and Development on Specially Designed Creep-fatigue Experiments on Alloy 617 in Support of Improving Creep-fatigue Evaluation Approaches

Experimental and numerical studies in support of developing the integrated Elastic–Perfectly Plastic (EPP) plus Simplified Model Test (SMT) design methodology, referred to as the EPP+SMT method, continued in FY 2023. This report focuses on the methods for extrapolating the EPP+SMT creep-fatigue life curves at long hold times and low strain ranges at elevated temperatures. In this work, the available uniaxial creep-fatigue failure data on Alloy 617 at temperatures of 950°C and 850°C were analyzed to provide a guidance on the development of the extrapolation method and the creep-fatigue failure criteria. A viscoplastic constitutive model for Alloy 617 was adopted to extrapolate the mechanical responses to low strain ranges and long hold times. A set of design curves of Alloy 617 at temperatures of 950°C, 850°C, and 800°C with tensile hold times of 1 hr, 100 hr, and 1,000 hr are developed. Furthermore, creep-fatigue testing on two notch specimen geometries, shallow-notch and sharp V-notch, on Alloy 617 was performed 950°C to understand the multiaxial stress relaxation behavior. The experimental and numerical results on the notch specimens were compared with those on the standard uniaxial smooth bar specimens. The effect of multi-axial stress state combined with elastic follow-up on the stress relaxation behavior was investigated in this report.

36 MATERIALS SCIENCE↗

Diffusional creep and creep degradation in the dispersion-strengthened alloy TD-NiCr

Dispersoid-free regions were observed in TD-NiCr (Ni-20Cr-2ThO2) after slow strain rate testing in air from 1145 to 1590 K. Formation of the dispersoid-free regions appears to be the result of diffusional creep. The net effect of this creep is the degradation of TD-NiCr to a duplex microstructure. Degradation is further enhanced by the formation of voids and integranular oxidation in the thoria-free regions. These regions apparently provided sites for void formation and oxide growth since the strength and oxidation resistance of Ni-20Cr is much less than Ni-20Cr-2ThO2. This localized oxidation does not appear to reduce the static load bearing capacity of TD-NiCr since long stress rupture lives were observed even with heavily oxidized microstructures. But this oxidation does significantly reduce the ductility and impact resistance of the material. Dispersoid-free bands and voids were also observed for two other dispersion strengthened alloys, TD-NiCrAl and IN-853. Thus, it appears that diffusional creep is charactertistic of dispersion-strengthened alloys and can play a major role in the creep degradation of these materials.

Whittenberger, J. D.↗

Correlation of creep rate with microstructural changes during high temperature creep

Creep tests were conducted on Haynes 188 cobalt-base alloy and alpha titanium. The tests on Haynes 188 were conducted at 1600 F and 1800 F for stresses from 3 to 20 ksi, and the as-received, mill-annealed results were compared to specimens given 5%, 10%, and 15% room temperature prestrains and then annealed one hour at 1800 F. The tests on alpha titanium were performed at 7,250 and 10,000 psi at 500 C. One creep test was done at 527 C and 10,000 psi to provide information on kinetics. Results for annealed titanium were compared to specimens given 10% and 20% room temperature prestrains followed by 100 hours recovery at 550 C. Electron microscopy was used to relate dislocation and precipitate structure to the creep behavior of the two materials. The results on Haynes 188 alloy reveal that the time to reach 0.5% creep strain at 1600 F increases with increasing prestrain for exposure times less than 1,000 hours, the increase at 15% prestrain being more than a factor of ten.

Young, C. T.↗

Stochastic modeling of crack initiation and short-crack growth under creep and creep-fatigue conditions

A simplified stochastic model is proposed for crack initiation and short-crack growth under creep and creep-fatigue conditions. Material inhomogeneity provides the random nature of crack initiation and early growth. In the model, the influence of microstructure is introduced by the variability of: (1) damage accumulation along grain boundaries, (2) critical damage required for crack initiation or growth, and (3) the grain-boundary length. The probabilities of crack initiation and growth are derived by using convolution integrals. The model is calibrated and used to predict the crack density and crack-growth rate of short cracks of 304 stainless steel under creep and creep-fatigue conditions. The mean-crack initiation lives are predicted to be within an average deviation of about 10 percent from the experimental results. The predicted cumulative distributions of crack-growth rate follow the experimental data closely. The applicability of the simplified stochastic model is discussed and the future research direction is outlined.

Kitamura, Takayuki↗

Stochastic modeling of crack initiation and short-crack growth under creep and creep-fatigue conditions

A simplified stochastic model is proposed for crack initiation and short-crack growth under creep and creep-fatigue conditions. Material inhomogeneity provides the random nature of crack initiation and early growth. In the model, the influence of microstructure is introduced by the variability of: (1) damage accumulation along grain boundaries, (2) critical damage required for crack initiation or growth, and (3) the grain-boundary length. The probabilities of crack initiation and growth are derived by using convolution integrals. The model is calibrated and used to predict the crack density and crack-growth rate of short cracks of 304 stainless steel under creep and creep-fatigue conditions. The mean-crack initiation lives are predicted to be within an average deviation of about 10 percent from the experimental results. The predicted comulative distributions of crack-growth rate follow the experimental data closely. The applicability of the simplified stochastic model is discussed and the future research direction is outlined.

Kitamura, Takayuki↗

A creep cavity growth model for creep-fatigue life prediction of a unidirectional W/Cu composite

A microstructural model was developed to predict creep-fatigue life in a (0)(sub 4), 9 volume percent tungsten fiber-reinforced copper matrix composite at the temperature of 833 K. The mechanism of failure of the composite is assumed to be governed by the growth of quasi-equilibrium cavities in the copper matrix of the composite, based on the microscopically observed failure mechanisms. The methodology uses a cavity growth model developed for prediction of creep fracture. Instantaneous values of strain rate and stress in the copper matrix during fatigue cycles were calculated and incorporated in the model to predict cyclic life. The stress in the copper matrix was determined by use of a simple two-bar model for the fiber and matrix during cyclic loading. The model successfully predicted the composite creep-fatigue life under tension-tension cyclic loading through the use of this instantaneous matrix stress level. Inclusion of additional mechanisms such as cavity nucleation, grain boundary sliding, and the effect of fibers on matrix-stress level would result in more generalized predictions of creep-fatigue life.

Kim, Young-Suk↗

Creep and Stress-strain Behavior After Creep from Sic Fiber Reinforced, Melt-infiltrated Sic Matrix Composites

Silicon carbide fiber (Hi-Nicalon Type S, Nippon Carbon) reinforced silicon carbide matrix composites containing melt-infiltrated Si were subjected to creep at 1315 C for a number of different stress conditions, This study is aimed at understanding the time-dependent creep behavior of CMCs for desired use-conditions, and also more importantly, how the stress-strain response changes as a result of the time-temperature-stress history of the crept material. For the specimens that did not rupture, fast fracture experiments were performed at 1315 C or at room temperature immediately following tensile creep. In many cases, the stress-strain response and the resulting matrix cracking stress of the composite change due to stress-redistribution between composite constituents during tensile creep. The paper will discuss these results and its implications on applications of these materials for turbine engine components.

Morscher, Gregory N.↗

Engineering-scale Modeling of High-Temperature Creep and Creep Crack Growth in Alloy 316H

This document demonstrates completion of the goals described in the technical narrative of the Department of Energy’s Industry Funding Opportunity Announcement (iFOA) project entitled “Modeling and Simulation Development Pathways to Accelerating KP-FHR Licensing,” which relates to the development and demonstration of capabilities for conducting engineering-scale simulations of Alloy 316H components under high-temperature conditions. This work encompassed two major aspects: integrating and testing constitutive models for the creep response of 316H at high temperatures, and developing tools for modeling creep crack growth (CCG) in 316H. Two classes of constitutive models were used in this effort: phenomenological models based on behavior observed at the engineering scale, and reduced-order models (ROMs) that represent the nonlinear response of mesoscale models that capture the sensitivity to material microstructure and processing. Likewise, the approaches employed for CCG modeling considered both simplified engineering approaches and detailed simulations of creep and damage ahead of the crack tip. These developments, which were performed by utilizing the Grizzly code as well as the open-source libraries it depends on, strengthen Grizzly’s ability to support licensing and safety analyses of high-temperature reactor components.

316H↗

Dislocation interactions in olivine control postseismic creep of the upper mantle

Changes in stress applied to mantle rocks, such as those imposed by earthquakes, commonly induce a period of transient creep, which is often modelled based on stress transfer among slip systems due to grain interactions. However, recent experiments have demonstrated that the accumulation of stresses among dislocations is the dominant cause of strain hardening in olivine at temperatures ≤600 °C, raising the question of whether the same process contributes to transient creep at higher temperatures. Here, we demonstrate that olivine samples deformed at 25 °C or 1150–1250 °C both preserve stress heterogeneities of ~1 GPa that are imparted by dislocations and have correlation lengths of ~1 μm. The similar stress distributions formed at these different temperatures indicate that accumulation of stresses among dislocations also provides a contribution to transient creep at high temperatures. The results motivate a new generation of models that capture these intragranular processes and may refine predictions of evolving mantle viscosity over the earthquake cycle.

58 GEOSCIENCES↗

Report on FY 2020 creep, fatigue and creep fatigue testing of Alloy 709 base metal at ORNL

The testing activities and research in support of ASME Code qualification of Alloy 709, an advanced austenitic steel, are being carried out at Oak Ridge National Laboratory (ORNL), Argonne National Laboratory, and Idaho National Laboratory. This report summarizes the status and results of FY 2020 planned testing at ORNL. Uniaxial tensile tests on the electroslag remelt (ESR) solution-annealed plate (heat number 58776-3RBC) with additional heat treatment were performed for the baseline mechanical properties evaluation for ASME code qualification of Alloy 709. The tensile properties were found to meet ASME SA-213 specifications and were comparable to the Nippon Steel NF709 data generated for an ASME Section I Code Case for seamless tubing. ORNL was tasked to carry out a subset of the Code Case testing for creep rupture. Creep rupture data from 18 tests were generated on a solution-annealed ESR plate with a solution annealing temperature of 1100°C. There are total of 19 intermediate and long-term creep rupture tests of Alloy 709 ongoing at ORNL. A preliminary fatigue design curve at 760°C was developed for Alloy 709, and the results show that the fatigue design curve of Alloy 709 is comparable to that of Alloy 800H at 760°C.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Interim Creep, Fatigue and Creep-Fatigue Data from FY 2022 INL Testing of A709 with Precipitation Treatment for ASME Code Case Data Package

This report provides the status of creep, fatigue, and creep-fatigue testing that transpired in fiscal year 2022 at Idaho National Laboratory (INL). This testing is being conducted to develop the data package to qualify A709 in Section III, Division 5 of the American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel Code (BPVC). This would permit the use of A709 for elevated temperature nuclear construction. Preliminary results continue to demonstrate the improved creep and fatigue resistance of A709 compared to 316H stainless steel.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Transient creep‐fatigue crack growth in creep‐brittle materials: Application to Alloy 718

Abstract This study presents incremental finite element computations of creep‐fatigue crack growth in Alloy 718 at in air. Alloy 718 is representative of creep‐brittle materials, in which viscoplastic deformation is restricted near the tip of a growing crack. The computations predict crack growth using a unique combination of an irreversible cohesive zone formulation and a strain gradient viscoplastic material model based on the Kocks–Mecking formulation. Cohesive zone damage parameters are estimated using sustained loading and constant‐amplitude cyclic loading experiments. Computations of crack extension under three different waveforms containing overloads all predict post‐overload retardation. The amount of retardation depends strongly on the overload ratio, consistent with experiments in the literature using similar waveforms. Analysis of the crack‐tip fields demonstrates retardation is associated with unloading in the highly deformed material near the advancing crack tip. Dynamic recovery and geometrically necessary dislocations are shown to significantly influence post‐overload crack extension.

36 MATERIALS SCIENCE↗

Single-Bar SMT Creep-Fatigue Testing on Alloy 617 with Software Controls on elastic Follow-Up Feedback in Support of New Creep-Fatigue Design Methodology

The Simplified Model Test (SMT) is one of the alternative ways to calculate the creep-fatigue damage of elevated temperature components. The SMT approach unifies the creep and fatigue damage, simplifying the damage calculation process with improved accuracy. Traditionally, SMT tests has have been conducted through the two bars: first is the driver bar and second is the test bar. The driver bar stays elastic and imposes the confinement to the second bar. This experimental procedure requires two test frames and a large test specimen, which limits the test parameter range and accessibility of this testing procedures. Hence, a single-bar SMT (SB-SMT) tests has been developed to simplify complexity in SMT experiment setup. The software-controlled SB-SMT test process has been introduced which completely replaces the driver bar. This paper discusses the single-bar SMT (SB-SMT) test procedure with software controls. The challenges and critical parameters in the software-controlled SB-SMT procedure are addresses addressed and recommendations are provided. A scoping test with a set of wider strain range, elastic follow-ups and dwell time validated the proposed test procedure.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Evaluation of Reduced Order Model for HT-9 Creep and Modifications to Current HT-9 Creep Model in BISON

In order to leverage existing reduced order models (ROM) for the modeling of LANL-developed HT-9 cladding constitutive behavior, mechanistic-based models have been implemented into BISON. It is posited that the increased fidelity of the ROM will show improvement over engineering-scale models in terms of comparison against experimental measurements. INL will assist LANL in implementing an HT9 ROM in BISON. Once the HT-9 mechanistic constitutive model can be leveraged in nuclear performance simulations, the numerical results of fast reactor models will be analyzed and compared against the Fuels Irradiation & Physics Database (FIPD) and separate effects tests to attempt a validation process. INL and LANL will work together to perform any necessary improvement that is identified during the implementation and use processes. Successful completion of the milestone will enable the general use of validated mechanistic ROMs for HT-9 cladding in BISON. This report provides a brief introduction to the Los Alamos Reduced Order Model Applied to Nonlinear Constitutive Equations (LAROMANCE) code, mechanical testing used to illustrate its creep and plastic deformation predictions for HT-9 cladding, and a comparison with existing models implemented into BISON. Current models have been modified to more appropriately account for primary thermal creep and results for corresponding testing are included in this report.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Creep and creep-recovery of a thermoplastic resin and composite

The database on advanced thermoplastic composites, which is currently available to industry, contains little data on the creep and viscoelastic behavior. This behavior is nevertheless considered important, particularly for extended-service reliability in structural applications. The creep deformation of a specific thermoplastic resin and composite is reviewed. The problem to relate the data obtained on the resin to the data obtained on the composite is discussed.

Hiel, Clem↗