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Presentation to be given at the FY 2020 SDRD Annual Meeting, to be held Sept. 23-24, on WebEx. Millimeter Wave Imaging Diagnostic for High-Explosive Fireball Characterization, STL-011-19, Year 2
A high-resolution magnetic resonance imaging (MRI) protocol, together with specialized image processing techniques, was applied to the quantitative measurement of age-related changes in calcaneal trabecular structure. The reproducibility of the technique was assessed and the annual rates of change for several trabecular structure parameters were measured. The MR-derived trabecular parameters were compared with calcaneal bone mineral density (BMD), measured by dual X-ray absorptiometry (DXA) in the same subjects. Sagittal MR images were acquired at 1.5 T in 23 healthy women (mean age: 49.3 +/- 16.6 [SD]), using a three-dimensional gradient echo sequence. Image analysis procedures included internal gray-scale calibration, bone and marrow segmentation, and run-length methods. Three trabecular structure parameters, apparent bone volume (ABV/TV), intercept thickness (I.Th), and intercept separation (I.Sp) were calculated from the MR images. The short- and long-term precision errors (mean %CV) of these measured parameters were in the ranges 1-2% and 3-6%, respectively. Linear regression of the trabecular structure parameters vs. age showed significant correlation: ABV/TV (r2 = 33.7%, P < 0.0037), I.Th (r2 = 26.6%, P < 0.0118), I.Sp (r2 = 28.9%, P < 0.0081). These trends with age were also expressed as annual rates of change: ABV/TV (-0.52%/year), I.Th (-0.33%/year), and I.Sp (0.59%/year). Linear regression analysis also showed significant correlation between the MR-derived trabecular structure parameters and calcaneal BMD values. Although a larger group of subjects is needed to better define the age-related changes in trabecular structure parameters and their relation to BMD, these preliminary results demonstrate that high-resolution MRI may potentially be useful for the quantitative assessment of trabecular structure.
An extreme ultraviolet (EUV) imaging spectrograph for the wavelength range from 235 to 450 A has been developed and used for resolution observations of the sun. The instrument incorporates a glancing incidence Wolter Type II Telescope and a near-normal incidence toroidal grating spectrograph to achieve near-stigmatic performance over this spectral range. The design of the spectrograph entrance aperture enables both stigmatic spectra with spectral resolution adequate to observe emission line profiles and spectroheliograms of restricted portions of the sun to be obtained concurrently. The design and performance of the instrument are described, and an overview of results obtained during a sounding rocket flight on May 5, 1989 is provided.
Liquid sample imaging devices and processes are disclosed for high resolution TEM imaging and multimodal analyses of liquid sample materials in situ under high vacuum that are compatible with standard type TEM chip membranes and TEM sample holders allowing TEM liquid sample imaging to be performed wherever a TEM instrument is accessible and at a substantially reduced cost compared to prior art systems and approaches.
Fully two-dimensional gamma-ray imaging with simultaneous high-resolution spectroscopy has been demonstrated using an externally segmented germanium sensor. The system employs a single high-purity coaxial detector with its outer electrode segmented into 5 distinct charge collection regions and a lead coded aperture with a uniformly redundant array (URA) pattern. A series of one-dimensional responses was collected around 511 keV while the system was rotated in steps through 180 degrees. A non-negative, linear least-squares algorithm was then employed to reconstruct a 2-dimensional image. Corrections for multiple scattering in the detector, and the finite distance of source and detector are made in the reconstruction process.
Composite materials have the potential to reduce the weight of rotating drive system components. However, these components are more complex to design and evaluate than static structural components in part because of limited ability to acquire deformation and failure initiation data during dynamic tests. Digital image correlation (DIC) methods have been developed to provide precise measurements of deformation and failure initiation for material test coupons and for structures under quasi-static loading. Attempts to use the same methods for rotating components (presented at the AHS International 68th Annual Forum in 2012) are limited by high speed camera resolution, image blur, and heating of the structure by high intensity lighting. Several improvements have been made to the system resulting in higher spatial resolution, decreased image noise, and elimination of heating effects. These improvements include the use of a high intensity synchronous microsecond pulsed LED lighting system, different lenses, and changes in camera configuration. With these improvements, deformation measurements can be made during rotating component tests with resolution comparable to that which can be achieved in static tests.
Abstract An experimental apparatus for measuring the dynamic behavior of materials subjected to strain rates on the order of 10 $$^3$$ 3 s $$^{-1}$$ - 1 and temperatures up to 800°C with a unique triple actuation system is developed in this work. This system is based on the traditional Kolsky (or split-Hopkinson pressure) bar design, with the addition of an external furnace used to heat the specimen to the desired temperature. A synchronized triple pneumatic actuation system is used to control the motion and timing of the the sample, incident, and transmitted bars. The cold contact time (CCT), or the time during which the heated sample is in contact with the room temperature bars before compression, is measured experimentally and carefully controlled to minimize the development of a temperature gradient across the sample and avoid heating of the bars. Experiments are performed in conjunction with ultra high speed imaging and 2D digital image correlation (DIC), as well as high speed thermal imaging. To verify the viability of the proposed system, experiments were conducted on Ti-6Al-4V (wt.%) at temperatures from 25°C up to and 800°C at an average strain rate of approximately 1200 s $$^{-1}$$ - 1 .
The first X-ray images of Kepler's supernova remnant (SN Ophiuchi 1604) are presented, and consequences for SNR models are discussed. Observations made with the Einstein Observatory Imaging Proportional Counter and High Resolution Imager show the remnant to be circular, with a strong shell brighter in the north than in the south. A flux of 1.2 x 10 to the -10th ergs/sq cm per sec was measured in the 0.15-4.5 keV region, which corresponds to an X-ray luminosity of 1.0 x 10 to the 36th ergs/sec at a distance of 5 kpc and an interstellar medium density of 2.8 x 10 to the 21st/sq cm. The X-ray observations do not allow the determination of whether the SNR is in the adiabatic or free expansion phase, but in either case it is shown that the mean ISM density must be greater than about 0.1/cu cm. In addition, the density of the X-ray emitting gas must be high, and its electron temperature must be fairly low. The high ISM densities derived for Kepler's SNR and other SNRs thus suggest an atypical ISM, possibly influenced by mass lost from the pre-supernova star.
Here we present a comprehensive study of cycled high-Ni (LiNi 1–x M x O 2 , M = metals), Li-rich (Li 1+x Mn y M 1–x–y O 2 ), and high-voltage spinel (LiMn 1.5 Ni 0.5 O 4 ) electrodes with time-of-flight secondary ion mass spectrometry (TOF-SIMS) and X-ray photoelectron spectroscopy in conjunction with electrochemical techniques to better understand their evolving cathode–electrolyte interphase structure during cycling. TOF-SIMS provides fragment-specific information regarding the surface film content for each of the electrodes. High-Ni cathodes show thick surface films initially containing Li 2 CO 3 , later developing oxidized organic carbonates throughout cycling. Li-rich electrode surface films develop strong characteristics during their first activation cycles, where released O 2 oxidizes organic carbonates to form polymeric carbons and decomposes LiPF 6 . High-voltage spinel electrodes operate outside the standard electrolyte stability window, generating reactive oxidized electrolyte species that further decompose LiPF 6 . The distribution and concentration of these different chemical fragments measured by TOF-SIMS are finally summarized by color-coded high-resolution images of cycled high-Ni, Li-rich, and high-voltage spinel electrodes.
Many important chemically reacting systems are inherently multi-dimensional with spatial and temporal variations in the thermochemical state, which can be strongly coupled to interactions with transport processes. Fundamental insights into these systems require multi-dimensional measurements of the thermochemical state as well as fluid dynamics quantities. Laser-based imaging diagnostics provide spatially and temporally resolved measurements that help address this need. The state of the art in imaging diagnostics is continually progressing with the goal of attaining simultaneous multi-parameter measurements that capture transient processes, particularly those that lead to stochastic events, such as localized extinction in turbulent combustion. Development efforts in imaging diagnostics benefit from advances in laser and detector technology. This article provides a perspective on the progression of increasing dimensionality of laser-based imaging diagnostics and highlights the evolution from single-point measurements to 1D and 2D multi-parameter imaging and 3D high-speed imaging. This evolution is demonstrated using highlights of laser-based imaging techniques in combustion science research as an exemplar of a complex multi-dimensional chemically reacting system with chemistry–transport coupling. Imaging diagnostics impact basic research in other chemically reacting systems as well, such as measurements of near-surface gases in heterogeneous catalysis. The expanding dimensionality of imaging diagnostics leads to larger and more complex datasets that require increasingly demanding approaches to data analysis and provide opportunities for increased collaboration between experimental and computational researchers in tackling these challenges.
The author has identified the following significant results. An approach to obtain spatial precision utilizes large scale black and white ratio images with high geometric precision. These images have a precision of .005 inch across the diagonals. Evaluation of a color ratio composite image of south central Nevada using ratio images recorded at this scale shows that the respective pixels are registered throughout the scene. Thus reconnaissance mapping can be carried out for the entire scene at 1:300,000 scale and then at larger scales by analyzing photographic enlargements of the original color ratio composite image. The advantages to this approach are elimination of repetitive computer processing and considerable flexibility as to specific scales.
X rays in the energy band 0.2-3.0 keV have been detected coming from both polar regions of Jupiter. The observations were made in 1979 and 1981 by using the imaging proportional counter and high resolution imaging detectors on the Einstein X-ray astronomy satellite. The measured flux density of approximately 0.0006/sq cm-sec at earth corresponds to an X ray luminosity of approximately 4 x 10 to the 9th W in the 0.2- to 3.0-keV energy band. The energy spectrum of the X rays is extremely soft and can be characterized by a power law with an exponent of approximately 2.3. Detector energy resolution is insufficient to distinguish a soft line spectrum from a continuum. However, the shape of the response and the observed X ray power indicate that the source of this auroral emission is not electron bremsstrahlung as on the earth, but is most probably line emission from O and S ions with energies between 0.03 and 4.0 MeV/nucleon precipitating from the outer boundary of the Io plasma torus at L approximately 8.
Attention is given to the design configuration and performance requirements of the Advanced X-ray Astrophysics Facility, as established by Phase A study results, noting the conceptual apprach to instrument accommodation by means of a focal plane assembly. Conceptually, the various instruments incorporated are modular in design, so that they may be replaced in orbit using standard interfaces. The instruments in question are high and moderate resolution imagers, a high resolution dispersive spectrometer, a moderate resolution spectrometer, and a focal plane polarimeter.
Two airborne flight systems were developed for geological studies: the airborne imaging spectrometer (AIS) and the advanced visible and infrared imaging spectrometer. A satellite imaging spectrometer system, the high resolution imaging spectrometer, is currently being developed and is planned for flight on the proposed NASA Earth Orbiting System. Examples of the application of these instruments in mineral and vegetation studies are described. Experiments conducted with AIS over the Cuprite Mining District (Nevada) and the Owens Valley (California) demonstrate the power of this new approach to remote sensing.
NASA's Earth Observing System (EOS) is a prospective program for earth observation from space using various unmanned, sun-synchronous polar orbit sensor platforms in conjunction with the Space Station to conduct measurements over a period of 15 years. The most important instruments will be the Moderate-Resolution Imaging Spectrometer, the High-Resolution Imaging Spectrometer, a large-area coverage SAR, the Laser Atmospheric Wind Sounder, the Atmospheric IR Sounder, and a Geodynamics and Laser-Ranging System.
HgCdTe is the current material of choice for high performance imagers operating at relatively high temperatures. Its lack of technological maturity compared with silicon and wide-band gap III-V compounds is more than offset by its outstanding IR sensitivity and by the relatively benign effect of its materials defects. This latter property has allowed non-equilibrium growth techniques, metal oxide chemical vapor deposition (MOCVD) and molecular beam epitaxy (MBE), to produce device quality long wavelength infrared (LWIR) HgCdTe even on common substrates like GaAs and GaAs/Si. Detector performance in these exotic materials structures is comparable in many ways with devices in equilibrium-grown material. Lifetimes are similar. RoA values at 77K as high as several hundred have been seen in HgCdTe/GaAs/Si with 9.5 micron cut-off wavelength. HgCdTe/GaAs layers with approx. 15 micron cut-off wavelengths have given average 77K RoAs of greater than 2. Hybrid focal plane arrays have been evaluated with excellent operability.
Diversity imaging techniques have been successfully employed in conventional microwave range-Doppler imaging radars to obtain high resolution images of both natural and man-made targets. These techniques allow microwave radars to achieve image resolution which would otherwise require excessively large antennas. Recent advances in coherent laser radar techniques and signal processing have led to the development of range-Doppler imaging laser radars. While much of the theory and signal processing techniques used in microwave radars can be brought to bear on laser radars, the significant difference in wavelength results in issues peculiar to laser radar systems. Both the fundamental concepts and specific applications of diversity imaging techniques applied to laser radar imaging systems will be discussed. Angle, frequency, and bistatic angle degrees of freedom can be employed in a coherent laser radar imaging system to achieve image resolution which exceeds the traditional Rayleigh criterion associated with the receive aperture. In diversity imaging, angle and frequency degrees of freedom can be used to synthesize an effective aperture providing range and Doppler target information. The ability to vary the bistatic angle provides an additional means of synthesizing an effective aperture. Both simulated and experimentally obtained laser radar images of spinning and/or tumbling objects utilizing both angular and frequency diversity will be presented. In coherent laser radar systems, image quality can be dominated by laser speckle effects. In particular, the signal-to-noise ratio (SNR) of a coherent laser radar image is at most unity in the presence of fully developed speckle. Diversity techniques can be utilized to improve the image SNR; simple incoherent averaging of images utilizing temporal and polarization degrees of freedom can significantly improve image SNR. Both the SNR and image resolution (as defined by the synthetic aperture) contribute to image quality. The relationship between the available degrees of freedom and image quality are discussed.
The 2.5-m du Pont telescope at Las Campanas, the IUE, and archival high-resolution imager X-ray data from the Einstein Observatory are used to present a detailed imaging and spectroscopic study of the SNR N49 in the LMC. The asymmetry of the optical image and the relatively high X-ray and optical luminosity of this remnant both arise from its interaction with an extended dense cloud to the southeast seen in CO emission. The optical spectra reveal clear evidence of reddening variations on spatial scales as small as about 2 arcsec over the face of the SNR. UV line emission is associated primarily with the bright optical filaments, and the total luminosity of N49 is measured in several optical and UV lines. A combined analysis of IUE and optical spectra indicates a range of radiative shock velocities. Implications for the interstellar medium surrounding N49 are discussed.