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All sources NASA NTRS DOE OSTI

DOE OSTI2022

Context and mitigation of lost circulation during geothermal drilling in diverse geologic settings

Lost circulation is one of the most common and expensive problems facing geothermal energy development, representing up to 30% of drilling costs. We examined drilling records from four geothermal fields—McGinness Hills in central Nevada, Don A. Campbell and Steamboat Hills in western Nevada, and Puna Geothermal Venture on the Big Island of Hawai'i— to identify geologies most prone to lost circulation, as well as common mitigation strategies. Depths of lost circulation events varied, but their frequency often increased in the production interval. Lost circulation commonly occurred near fault intersections, and heavily faulted fields like McGinness Hills and Don A. Campbell showed secondary mineralization within approximately 100 m (328 ft) or less of where circulation was lost. Lost circulation mitigation strategies included using locally available materials (e.g., cotton seed hulls) as well as more expensive proprietary lost circulation materials, cement plugs above the reservoir, and drilling blind with aerated, polymer-based mud in the production zone. Addressing lost circulation using a well thought out decision-making approach and materials above the reservoir will save time and cost, and provide needed well integrity. Mitigation often requires a series of steps, typically applied from perceived least expensive to most, and are dependent on the severity and location in the well where circulation was lost and availability of materials. Placing cement plugs can cure lost circulation events, however these plugs are often expensive, time-consuming, and may not be successful.

15 GEOTHERMAL ENERGY↗

DOE OSTI2014

A complex systems analysis of stick-slip dynamics of a laboratory fault

We study the stick-slip behavior of a granular bed of photoelastic disks sheared by a rough slider pulled along the surface. Time series of a proxy for granular friction are examined using complex systems methods to characterize the observed stick-slip dynamics of this laboratory fault. Nonlinear surrogate time series methods show that the stick-slip behavior appears more complex than a periodic dynamics description. Phase space embedding methods show that the dynamics can be locally captured within a four to six dimensional subspace. These slider time series also provide an experimental test for recent complex network methods. Phase space networks, constructed by connecting nearby phase space points, proved useful in capturing the key features of the dynamics. In particular, network communities could be associated to slip events and the ranking of small network subgraphs exhibited a heretofore unreported ordering.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1997

Lunar and Planetary Science XXVIII

The present conference discusses such topics as density crossovers in lunar picrites, the geology of the Cassini impact basin, Mars, nanobacteria in carbonates, the properties of shocked aerogels, a chemical model of Comet Halley, lunar mascons, the impact evolution of icy regoliths, the geology of the Venera 8 landing site, the photogeologic mapping of northern Venus, HST observations of Mars, observational constraints on the rotational dynamics of Mars, and primordial magnetic field measurements from the moon. Also discussed are models of the S2 fluorescence spectra of comets, Martian crater ejecta, the heights of Venusian steep-sided domes, cloud-climate interactions on Venus, the Humorum basin geology from Clementine data, an early Amazonian lake in the Gale crater of Mars, nebular fractionations and Mn-Cr systematics, the Rock Chipper planetary surface sample collection, Mariner 10 stereo images of Mercury, remote and local stresses and Calderas on Mars, the electrostatic charging of saltating particles, SO2 detected on Callisto, the Mars Explorer Planetary Data System, an assessment of explosive venting on Europa, the sequential faulting history of the Mars Valles Marineris, a search for Martian sediments, the composition and internal structure of Europa, long-term and 'diurnal' tidal stresses on Europa, and episodic greenhouse climates on Mars.

Source record↗

NASA NTRS2011

Improving Distributed Diagnosis Through Structural Model Decomposition

Complex engineering systems require efficient fault diagnosis methodologies, but centralized approaches do not scale well, and this motivates the development of distributed solutions. This work presents an event-based approach for distributed diagnosis of abrupt parametric faults in continuous systems, by using the structural model decomposition capabilities provided by Possible Conflicts. We develop a distributed diagnosis algorithm that uses residuals computed by extending Possible Conflicts to build local event-based diagnosers based on global diagnosability analysis. The proposed approach is applied to a multitank system, and results demonstrate an improvement in the design of local diagnosers. Since local diagnosers use only a subset of the residuals, and use subsystem models to compute residuals (instead of the global system model), the local diagnosers are more efficient than previously developed distributed approaches.

Bregon, Anibal↗

DOE OSTI2023

Hydrologic Impacts of a Strike-Slip Fault Zone: Insights from Joint 3D Body-Wave Tomography of Rock Valley

The Rock Valley fault zone (RVFZ), an intraplate strike-slip fault zone in the southern Nevada National Security Site (NNSS), hosted a series of very shallow (<3 km) earthquakes in 1993. The RVFZ may also have hydrological significance within the NNSS, potentially playing a role in regional groundwater flow, but there is a lack of local hydrological data. In the Spring of 2021, we collected active-source accelerated weight drop seismic data over part of the RVFZ to better characterize the shallow subsurface. Here, we manually picked ~17,000 P-wave travel times and over 14,000 S-wave travel times, which were inverted for P-wave velocity (V P ), S-wave velocity (V S ), and V P /V S ratio in a 3D joint tomographic inversion scheme. Seismic velocities are imaged as deep as ~700 m in areas and generally align with geologic and structural expectations. V P and V S are relatively reduced near mapped and inferred faults, with the most prominent lower V P and V S zone around the densest collection of faults. We image V P /V S ratios ranging from ~1.5 to ~2.4, the extremes of which occur at a depth of ~100 m and are juxtaposed across a fault. One possible interpretation of the imaged seismic velocities is enhanced fault damage near the densest collection of faults with relatively higher porosity and/or crack density at ~100 m depth, with patches of semiperched groundwater present in the sedimentary rock in higher V P /V S areas and drier rock in lower V P /V S areas. A relatively higher V P /V S area beneath the densest faults persists at depth, which suggests percolation of groundwater via the fault damage zone to the regionally connected lower carbonate aquifer. Potentially, the presence and movement of groundwater may have played a role in the 1993 earthquake aftershocks.

58 GEOSCIENCES↗

DOE OSTI2024

Regional-scale fault-to-structure earthquake simulations with the EQSIM framework: Workflow maturation and computational performance on GPU-accelerated exascale platforms

Continuous advancements in scientific and engineering understanding of earthquake phenomena, combined with the associated development of representative physics-based models, is providing a foundation for high-performance, fault-to-structure earthquake simulations. However, regional-scale applications of high-performance models have been challenged by the computational requirements at the resolutions required for engineering risk assessments. The EarthQuake SIMulation (EQSIM) framework, a software application development under the US Department of Energy (DOE) Exascale Computing Project, is focused on overcoming the existing computational barriers and enabling routine regional-scale simulations at resolutions relevant to a breadth of engineered systems. This multidisciplinary software development—drawing upon expertise in geophysics, engineering, applied math and computer science—is preparing the advanced computational workflow necessary to fully exploit the DOE’s exaflop computer platforms coming online in the 2023 to 2024 timeframe. Achievement of the computational performance required for high-resolution regional models containing upward of hundreds of billions to trillions of model grid points requires numerical efficiency in every phase of a regional simulation. This includes run time start-up and regional model generation, effective distribution of the computational workload across thousands of computer nodes, efficient coupling of regional geophysics and local engineering models, and application-tailored highly efficient transfer, storage, and interrogation of very large volumes of simulation data. This article summarizes the most recent advancements and refinements incorporated in the workflow design for the EQSIM integrated fault-to-structure framework, which are based on extensive numerical testing across multiple graphics processing unit (GPU)-accelerated platforms, and demonstrates the computational performance achieved on the world’s first exaflop computer platform through representative regional-scale earthquake simulations for the San Francisco Bay Area in California, USA.

58 GEOSCIENCES↗

DOE OSTI2026

Study of the Protection Improvements for a Weak Grid Area With High Inverter-Based Resources (IBRs)

This project designs enhanced protection scheme for the real-world weak grid area with a high penetration of IBRs. As the existing protection schemes are originally designed for traditional synchronous machines, we first evaluate if the protection scheme will continue to operate reliably in systems with high levels of IBRs. Hardware relays are tested using a controller-hardware-in-the-loop setup. PSCAD electromagnetic transient simulation with IBR original equipment manufacturer black-box models is used to perform fault studies and generate COMTRADE data, which are replayed by a real-time digital simulator (RTDS) to feed input to the hardware relays. Three scenarios are analyzed: normal operation, an N-1 contingency, and an IBR-only scenario. The evaluation results reveal the following: 1) the protection scheme remains reliable under normal conditions and N-1 contingencies and 2) in IBR-only scenarios, differential protection (87L) continues to operate reliably, whereas local protection elements, such as distance and directional elements, fail because of the lack of regulated negative sequence current contributed by IBRs. Enhanced protection is designed to address the challenge of lack of negative sequence current from IBRs, including increased restraining factors a2 and k2 to block 32Q or using V instead QV ORDER for ground faults, enhanced mho distance element with voltage and phase angle supervision for L-L faults. The efficacy of enhanced protection logic is validated and proven to work reliably. Additionally, IEEE Std. 2800-2022 negative sequence current compliant GFL and GFM IBRs from another vendor are tested and proven to work reliably without need for enhanced logic. Therefore, this work provides valuable decision-making for utilities facing protection system challenges due to IBRs, either designing enhanced protection scheme or requesting their IBRs being IEEE Std. 2800-2022 compliant to produce regulated negative sequence current for protection relay to make correct decision.

24 POWER TRANSMISSION AND DISTRIBUTION↗

DOE OSTI2018

Cyclic plastic deformation behaviour of a directionally solidified nickel base superalloy at 850 °C: Damage micromechanisms

Highlights: • Isothermal LCF life of CM 247 DS is reduced using R = 0 instead of R = −1. • Reduction in LCF life is significant at lower values of Δε/2. • Reduction in fatigue life is attributed to the development of sustained mean stress. • Sustained mean stress prevents the slip transfer from γ-channels to γ′-precipitates. • Sustained mean stress promotes dislocation network formation and looping. - Abstract: Dislocation based deformation micromechanisms during low cycle fatigue deformation of nickel base superalloy CM 247 DS LC at 850 °C was investigated by conducting fatigue tests employing constant strain amplitudes for strain ratio (R) values of 0, −1 and carrying out extensive SEM and TEM examinations. Cyclic life of the alloy reduces for all fatigue tests conducted employing R = 0 in comparison with R = −1 owing to sustained mean stress developed during fatigue at R = 0. TEM examinations confirmed that sustained mean stress developed during low strain amplitude fatigue test (Δε/2 = 0.5%) using R = 0 condition prevented slip transfer from γ-channels to γ′-precipitates and resulted in the formation of dislocation substructures such as networks, nodes etc. and also promoted dislocation looping around γ′-precipitates. Lower fatigue life at R = 0 is mainly attributed to the development of these types of substructures, which promotes strain localization in both intra as well intergranular regions. Whereas, in specimen fatigue tested (Δε/2 = 0.5%) using R = −1 condition, shearing of γ′-precipitates by APB coupled dislocation and formation of stacking faults were observed. The formation and nature of stacking faults were analysed using weak beam imaging technique. Stacking fault formed during fatigue tests using R = −1 condition matured to micro-twins when Δε/2 value was increased to 0.8%. The mechanism of formation of these microtwins is discussed in detail. SEM based microstructural and fractographic examinations revealed that mean stress induced creep effect resulted in intergranular crack initiation and grain boundary cavitation during fatigue tests under R = 0 condition and therefore verified the facts revealed in TEM studies.

36 MATERIALS SCIENCE↗

NASA NTRS1977

Geologic investigation of Mercury data and the subsequent mapping and explanation of the quadrangle area H-12

The origin of scraps and ridges mapped in the H-12 region of Mercury are discussed. These features apparently are of non-impact origin and show distinctly non-random patterns of distribution and orientation. These patterns cannot be simply related to selective enhancement of visibility by lighting conditions, global stresses of spin down or interior cooling, or local uplifts or subsidences. Suggestions are made that the origin of these structures may lie outside the region of Mercury photographed or the scarps and ridges may have formed by reactivation of faults or joints bounding pre-existing crystal blocks.

Blasius, K. R.↗

NASA NTRS1993

Mode of emplacement of lunar mare volcanic deposits: Graben formation due to near surface deformation accompanying dike emplacement at Rima Parry 5

Theoretical analyses, together with the observed style of emplacement of lunar mare volcanic deposits, strongly suggest that mare volcanic eruptions are fed by dikes from source regions at the base of the crust or deeper in the lunar mantle. Some dikes intrude into the lower crust, while others penetrate to the surface and are the sources for voluminous outpourings of lava. Still others stall near the surface generating a near-surface extensional stress field. We have investigated the hypothesis that some lunar linear rilles (graben) are the near-surface manifestations of dikes intruded to shallow depths. For a specific example (Rima Parry 5), we show that the geometry of the faults implies a mean dike width of about 150 m and depth to the dike top of about 500 m, values consistent with other theoretical and observational data on lunar dike geometry. Localized pyroclastic deposits along Rima Parry 5 are evidence for the presence of near-surface magma, and are interpreted to be the result of degassing and pyroclastic eruption subsequent to the emplacement of the dike.

Head, J. W.↗

NASA NTRS2006

Aeroelastic Flight Data Analysis with the Hilbert-Huang Algorithm

This report investigates the utility of the Hilbert Huang transform for the analysis of aeroelastic flight data. It is well known that the classical Hilbert transform can be used for time-frequency analysis of functions or signals. Unfortunately, the Hilbert transform can only be effectively applied to an extremely small class of signals, namely those that are characterized by a single frequency component at any instant in time. The recently-developed Hilbert Huang algorithm addresses the limitations of the classical Hilbert transform through a process known as empirical mode decomposition. Using this approach, the data is filtered into a series of intrinsic mode functions, each of which admits a well-behaved Hilbert transform. In this manner, the Hilbert Huang algorithm affords time-frequency analysis of a large class of signals. This powerful tool has been applied in the analysis of scientific data, structural system identification, mechanical system fault detection, and even image processing. The purpose of this report is to demonstrate the potential applications of the Hilbert Huang algorithm for the analysis of aeroelastic systems, with improvements such as localized online processing. Applications for correlations between system input and output, and amongst output sensors, are discussed to characterize the time-varying amplitude and frequency correlations present in the various components of multiple data channels. Online stability analyses and modal identification are also presented. Examples are given using aeroelastic test data from the F-18 Active Aeroelastic Wing airplane, an Aerostructures Test Wing, and pitch plunge simulation.

Brenner, Martin J.↗

DOE OSTI2020

Resilient Autonomous Wind Farms: Preprint

With the advent of an increasing number of control strategies that seek to optimize wind turbine performance on a farm-level, taking account of individual wind turbine information to achieve wind farm-level objectives has become an increasingly important goal. Methods for controlling wind turbines on an individual and farm level have seen significant development, and an abundance of new implementations for gathering and using data from turbines have created potential for novel control mechanisms which can further optimize the performance and delivery characteristics of a wind farm. A key element of making these wind farms more efficient is to develop reliable algorithms that use local sensor information that is already being collected, such as supervisory control and data acquisition (SCADA) data, local meteorological stations, and nearby radars/sodars/lidars. Making use of information from all wind turbines in a wind farm can enable such approaches as determining the atmospheric conditions across the farm, improving fault-finding, and enabling more efficient overall control of farm-wide optimizations through mechanisms such as wake-steering. However, these approaches typically involve a centralized communications and control center. In order to ensure the resilient operation of the farm, it is necessary to develop an approach which distributes the calculation and communication amongst multiple nodes throughout the farm. In this fashion, a redundant, robust, and secure network can be created, which can tolerate faults in calculation, communication, and even external attacks which seek to disrupt the operation of the wind farm. This paper introduces the use of the Raft Byzantine Fault Tolerance algorithm in the implementation of autonomous control of a wind farm. This implementation will allow for fault tolerance for malfunctioning nodes, sensors, transmitters, and connectors. This approach is equally extensible to account for malicious actors. It will be shown to achieve overall consensus, provided the number of faults/malicious nodes is less than 3$n$+1, where $n$ is the number of turbine cluster faults which may occur, and to be robust in the face of multiple arbitrary faults.

autonomous↗

DOE OSTI2018

Local Radiation Shielding Design Methodology

The NSLS-II accelerators are housed within a radiation enclosure of normal concrete (and in some places high density concrete) that has been designed to reduce the radiation generated from an assumed operational beam loss or bulk shielding current (BCS) from each accelerator. The beam loss model used to estimate the thickness of this bulk shielding, assumed a beam energy at the expected operating energy and a current loss based on reasonable assumptions for the fraction of the expected operating current. The thickness of the shield was determined to be the amount required to reduce the radiation outside the shield to a maximum dose rate of <0.5mrem/hr. for occupied areas for these normal operational losses. These assumed beam losses and the bulk shielding thicknesses required are given in reference [1]. Abnormal operating conditions generating higher than normal beam losses must also be considered, and additional engineering controls will be required depending on the magnitude of the radiation levels generated during the abnormal condition. Additional local shielding subject to configuration control may be utilized to reduce radiation levels associated with these abnormal loss conditions. Interlocked area radiation monitors are another means to prevent continued operation with higher than an acceptable level. The NSLS-II Shielding Policy requires that an engineered system be utilized to mitigate an abnormal condition producing radiation levels greater than 100 mR/h, and that two systems are required if the projected radiation levels during a fault condition are > 2000 mR/h. It is intended that shielding limits the dose rate to < 0.5 mR/h in occupied areas for normal operational losses, and the combination of administrative and engineered controls for abnormal losses will maintain radiation exposure to trained personnel working at the NSLS-II facility to as low as reasonably achievable. It is anticipated that all individual exposures will be well within the planned administrative control level of 100mrem/year. This technical note presents the method used to identify these potential high beam loss locations, evaluate the potential radiation risk these losses create outside the enclosure shield and the design process that specifies the required local radiation shielding needed to reduce this risk below the maximum dose rate of the bulk shield design, listed above. If shielding can’t be adequately provided or if other fault initiated losses could occur, then the necessary engineering controls will be indicated that will limit the energy, current or duration of the beam transport that constitute this high beam loss risk.

36 MATERIALS SCIENCE↗

NASA NTRS2018

Self-Stabilizing Distributed Symmetric-Fault Tolerant Synchronization Protocol

A network system includes at least one node configured to exchange messages through a set of communication links. Each node includes a synchronizer, a set of monitors in communication with the synchronizer, a physical oscillator and a state timer clock and a local timer clock, each clock being driven by the physical oscillator and having a variable clock value that locally tracks passage of clock time for the node. The network system is configured to execute a synchronization process when a specified condition occurs. Upon receiving a Sync message, each of the nodes is configured to store an incoming Sync message, increment a local timer clock value, or ignore the Sync message based on a local timer clock value associated with an incoming Sync message.

Malekpour, Mahyar R.↗

DOE OSTI2016

Arc-Fault Primer: Numerical, Analytical, and Experimental Characteristics of Initiation and Sustainment of Arc Plasmas (DRAFT)

While arc-faults are rare in electrical installations, many documented events have led to fires that resulted in significant damage to energy-generation, commercial and residential systems, as well as surrounding structures, in both the United States and abroad. Arc-plasma discharges arise over time due to a variety of reliability issues related to cable material degradation, electrical and mechanical stresses or acute conductive wiring dislocations. These may lead to discontinuity between energized conductors, facilitating arcing events and fires. Arc-flash events rapidly release significant energy in a localized volume, where the electric arc experiences a reduction in resistance. This facilitates a reduction in electrical resistance as the arc temperature and pressure can increase rapidly. Strong pressure waves, electromagnetic interference (EMI), and intense light from an arc pose a threat to electrical worker safety and system equipment. This arc-fault primer provides basic fundamental insight into arc-fault plasma discharges, and an overview of direct current (DC) and alternating current (AC) arc-fault phenomena. This primer also covers pressure waves and EMI arc-fault hazard analyses related to incident energy prediction and potential damage analysis. Mitigation strategies are also discussed related to engineering design and employment of protective devices including arc-fault circuit interrupters (AFCIs). Best practices related to worker safety are also covered, especially as they pertain to electrical codes and standards, particularly Institute of Electrical and Electronics Engineers (IEEE) 1584 and National Fire Protection Agency (NFPA) 70E. Throughout the primer various modelling and test capabilities at Sandia National Laboratories are also covered, especially as they relate to novel methods of arc-fault/arc-flash characterization and mitigation approaches. Herein, this work describes methods for producing and characterizing controlled, sustained arcs at atmospheric pressures as well as methods for mitigation with novel materials.

42 ENGINEERING↗

DOE OSTI2017

Landslides caused by the Mw7.8 Kaikōura earthquake and the immediate response

Tens of thousands of landslides were generated over 10,000 km 2 of North Canterbury and Marlborough as a consequence of the 14 November 2016, M w 7.8 Kaikōura Earthquake. The most intense landslide damage was concentrated in 3500 km 2 around the areas of fault rupture. Given the sparsely populated area affected by landslides, only a few homes were impacted and there were no recorded deaths due to landslides. Landslides caused major disruption with all road and rail links with Kaikōura being severed. The landslides affecting State Highway 1 (the main road link in the South Island of New Zealand) and the South Island main trunk railway extended from Ward in Marlborough all the way to the south of Oaro in North Canterbury. The majority of landslides occurred in two geological and geotechnically distinct materials reflective of the dominant rock types in the affected area. In the Neogene sedimentary rocks (sandstones, limestones and siltstones) of the Hurunui District, North Canterbury and around Cape Campbell in Marlborough, first-time and reactivated rock-slides and rock-block slides were the dominant landslide type. These rocks also tend to have rock material strength values in the range of 5-20 MPa. In the Torlesse ‘basement’ rocks (greywacke sandstones and argillite) of the Kaikōura Ranges, first-time rock and debris avalanches were the dominant landslide type. These rocks tend to have material strength values in the range of 20-50 MPa. A feature of this earthquake is the large number (more than 200) of valley blocking landslides it generated. This was partly due to the steep and confined slopes in the area and the widely distributed strong ground shaking. The largest landslide dam has an approximate volume of 12(±2) M m 3 and the debris from this travelled about 2.7 km 2 downslope where it formed a dam blocking the Hapuku River. The long-term stability of cracked slopes and landslide dams from future strong earthquakes and large rainstorms are an ongoing concern to central and local government agencies responsible for rebuilding homes and infrastructure. A particular concern is the potential for debris floods to affect downstream assets and infrastructure should some of the landslide dams breach catastrophically. At least twenty-one faults ruptured to the ground surface or sea floor, with these surface ruptures extending from the Emu Plain in North Canterbury to offshore of Cape Campbell in Marlborough. The mapped landslide distribution reflects the complexity of the earthquake rupture. Landslides are distributed across a broad area of intense ground shaking reflective of the elongate area affected by fault rupture, and are not clustered around the earthquake epicentre. The largest landslides triggered by the earthquake are located either on or adjacent to faults that ruptured to the ground surface. Surface faults may provide a plane of weakness or hydrological discontinuity and adversely oriented surface faults may be indicative of the location of future large landslides. Their location appears to have a strong structural geological control. Initial results from our landslide investigations suggest predictive models relying only on ground-shaking estimates underestimate the number and size of the largest landslides that occurred.

58 GEOSCIENCES↗

NASA NTRS1990

The origin of fluvial valleys and early geologic history, Aeolis Quadrangle, Mars

A valley genesis model of the southern Aeolis Quadrangle, eastern Mars, is proposed. In response to widespread effusive volcanism in interstratified, ice-reach terrains, local subsidence occurred along fractures/faults, and produced scarps that intersected local aquifers. Heated spring discharges issuing from these scarps may have carved the valleys through a combination of downvalley water, ice, and debris flows, and headward erosion along stratal discontinuities and individual conduit faults and fractures. Fifty-six asymmetric scarps or ridges that are probable thrust faults are mapped. The faults exhibit an orientation vector mean of N 63 deg W +/- 11 deg and they transect the lava plains and the older plateau sequence units. The vector mean for the 264 valleys mapped is N 48 deg W +/- 12 deg, with a larger dispersion about the mean. The similar orientations displayed by thrust faults and valley axes suggest that valley locations are partly controlled by preexisting thrust faults and fracture systems.

Brakenridge, G. Robert↗

DOE OSTI2024

Compositional effect on pressure-induced polymorphism in high-entropy alloys

Recently, pressure-induced polymorphic phase transitions were discovered in several fragmented high-entropy alloys (HEAs), offering a valuable opportunity to deepen our understanding of these materials. However, the chemical and physical factors that govern these transitions are still unclear. Here, in this work, we combined in situ high-pressure synchrotron X-ray diffraction, X-ray emission spectroscopy (XES), and high-resolution transmission electron microscopy (HRTEM) to systematically study the evolution of the atomic and electronic structures in the Cantor alloy and its face-centered-cubic ( fcc ) subset alloys (CoCrFeMnNi, CoCrFeNi, CoCrMnNi, CoFeMnNi, CoCrNi, CoFeNi, CoMnNi, CrFeNi, and FeMnNi). Surprisingly, diverse behavior was observed among these closely related alloys during compression and decompression, which includes irreversible, reversible fcc to hexagonal close-packed (hcp) phase transitions, or even no detectable phase transitions up to ∼40 GPa. HRTEM measurements confirmed that the fcc and hcp phases abided by the classic Shoji-Nishiyama orientation relationship during the transitions. XES data indicated that high-pressure suppresses the local magnetic moments in all the studied alloys, suggesting that magnetic states do not significantly influence the polymorphic transitions. By comparing the effects of the atomic size difference, entropy, valence electron concentration, and stacking fault energy across all the compositions studied, only the stacking fault energy shows a strong correlation with the phase transitions, indicating it plays a key role in inducing polymorphism in HEAs.

36 MATERIALS SCIENCE↗