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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 523 records · Page 29
All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Application of IR imaging for free-surface velocity measurement in liquid-metal systems

Measuring free-surface, liquid-metal flow velocity is challenging to do in a reliable and accurate manner. This paper presents a non-invasive, easily-calibrated method of measuring the surface velocities of open-channel liquid-metal flows using an IR camera. Unlike other spatially-limited methods, this IR camera particle tracking technique provides full field-of-view data that can be used to better understand open-channel flows and determine surface boundary conditions. This method could be implemented and automated for a wide range of liquid-metal experiments, even if they operate at high-temperatures or within strong magnetic fields.

Free surface↗
DOE OSTI2024

Two-step retrace error calibration removing tilt ambiguity in coherence scanning interferometry

In interferometry measurement, the retrace error often limits its high-precision metrology applications. Retrace error calibration with tilted flats can give a relation between the retrace error and the introduced tilt angles, but there is still an ambiguity between the introduced tilt angles and the tilt terms in the created retrace error. Here, we propose a novel, to the best of our knowledge, two-step calibration method to resolve this tilt ambiguity. It involves additional measurements of spherical mirror(s) with known curvature(s). The experiment shows that the curvature deviation due to the tilt ambiguity can be significantly reduced after applying the proposed method.

36 MATERIALS SCIENCE↗
DOE OSTI2013

Acoustic Array Development for Wind Turbine Noise Characterization

This report discusses the design and use of a multi-arm, logarithmic spiral acoustic array by the National Renewable Energy Laboratory (NREL) for measurement and characterization of wind turbine-generated noise. The array was developed in collaboration with a team from the University of Colorado Boulder. This design process is a continuation of the elliptical array design work done by Simley. A description of the array system design process is presented, including array shape design, mechanical design, design of electronics and the data acquisition system, and development of post-processing software. System testing and calibration methods are detailed. Results from the initial data acquisition campaign are offered and discussed. Issues faced during this initial deployment of the array are presented and potential remedies discussed.

17 WIND ENERGY↗
DOE OSTI2016

Arctic Clouds Infrared Imaging Field Campaign Report

The Infrared Cloud Imager (ICI), a passive thermal imaging system, was deployed at the North Slope of Alaska site in Barrow, Alaska, from July 2012 to July 2014 for measuring spatial-temporal cloud statistics. Thermal imaging of the sky from the ground provides high radiometric contrast during night and polar winter when visible sensors and downward-viewing thermal sensors experience low contrast. In addition to demonstrating successful operation in the Arctic for an extended period and providing data for Arctic cloud studies, a primary objective of this deployment was to validate novel instrument calibration algorithms that will allow more compact ICI instruments to be deployed without the added expense, weight, size, and operational difficulty of a large-aperture onboard blackbody calibration source. This objective was successfully completed with a comparison of the two-year data set calibrated with and without the onboard blackbody. The two different calibration methods produced daily-average cloud amount data sets with correlation coefficient = 0.99, mean difference = 0.0029 (i.e., 0.29% cloudiness), and a difference standard deviation = 0.054. Finally, the ICI instrument generally detected more thin clouds than reported by other ARM cloud products available as of late 2015.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2018

Special Analysis: Impact of Updated GSA Flow Model on E-Area Low-Level Waste Facility Groundwater Performance

In March 2018, the Savannah River National Laboratory (SRNL) notified Solid Waste Management (SWM) of new information that could potentially impact groundwater (GW) disposal limits and possibly require temporary protective measures (Crowley 2018). GW flow directions in the E-Area Low-Level Waste Facility (LLWF) Slit Trenches (STs), Engineered Trenches (ETs), and the Low Activity Waste Vault (LAWV) have notably changed in the new 2018 General Separations Area (GSA) flow model (Flach 2018a). The 2018 GSA flow model had been updated using 20 years of new hydrologic field data and model calibration methods that employed mathematical optimization software. It was later determined that the primary reason for the change in GW flow directions was due to the influence of low permeability caps that had been placed over the Old Burial Grounds and the Low Level Radioactive Waste Disposal Facility (LLRWDF). Updated flow directions in the model produce a higher degree of plume overlap for disposal units (DU’s) in the southeastern portion of E-Area than had been predicted in the 2008 E-Area LLWF Performance Assessment (PA). SWM and SRNL outlined the scope for this Special Analysis (SA) and proposed a set of interim measures (IM’s) to protect trench operations from exceeding Performance Objectives (PO’s) during the preparation of this SA, both of which were approved by the SWM Performance Assessment Review Committee (PARC) (Mooneyhan 2018).

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2018

Grain Boundary Diffusion Characterized by KPFM

The nanometer scale characterization technique of Frequency Modulated Kelvin Probe Force Microscopy (FM-KPFM) will be used to assess a preliminary diffusion study on thin metal films that undergo accelerated aging. The KPFM technique provides a relatively easy, non-destructive methodology that does not require high-vacuum facilities to obtain nanometer spatial resolution of surface chemistry changes and will be exercised in an effort to explore its capacity to map surface potential contrast caused by Cu diffusion in a manner that allows for a qualitative assessment of diffusion rate kinetics. Supporting data will be obtained from traditional techniques: AES, XPS and UPS. An aging study was conducted on thin metal test specimens comprised of Ti or Cr/Cu/Au layer thicknesses of 50nm/500nm/500nm up to 4μm respectively. The accelerated aging process, was performed in air at aging temperatures of 60°C, 100°C, and 125°C for aging times of 8 hours, 24 hours, 96 hours (4 days), and 216 hours (9 days). A calibration method was developed using Au, Al and Ni standards to establish precision and repeatability of the KPFM technique. Average CPDs and standard deviations for each metal were found and summarized.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Total Measurement Uncertainty in Neutron Coincidence Multiplicity Analysis

Neutron multiplicity counting is the most commonly used nondestructive assay technique for determining the plutonium mass within containers of scrap PuO 2 or mixed oxide (MOX). In multiplicity analysis, the 240 Pu eff mass, leakage multiplication, and alpha ratio (the ratio of [α, n]-to-spontaneous fission neutron production) are the three primary unknown sample properties. They must be determined simultaneously. To solve for these three unknowns in a multiplicity assay, three measured values are needed: the singles, doubles, and triples neutron count rates. While the analysis is limited to solving for three unknowns, there are many additional factors that impact the observed count rates and contribute to the measurement uncertainty. In this study we investigate the various uncertainty contributors for the multiplicity analysis through a combination of traditional uncertainty propagation techniques supplemented by Monte Carlo simulations to address the dependences not explicitly expressed by the point source model. Uncertainties arising from counting statistics, calibration parameters, calibration method, nuclear data, and various material characteristics (isotopic abundances, chemical form, density, and impurities) are considered. A Total Measurement Uncertainty (TMU) estimate is then developed from these uncertainty contributors. This study is confined to multiplicity analysis of items commonly encountered in international safeguards applications. That is, the study focused on Pu oxides and MOX materials for the masses ranging up to 4000 grams total Pu. Multiplicity measurements were simulated using MCNP V6 based on the Plutonium Scrap Multiplicity Counter (PSMC), Epithermal Multiplicity Counter (ENMC), Pyrochemical Multiplicity Counter, and Large Epithermal Multiplicity Counter (LEMC) for this study; however, this report focuses on the parameterization of the uncertainties for the PSMC. The performance differences between the PSMC and the other multiplicity counting systems are relatively small, primarily manifesting in the impact on measurement precision so that the evaluation developed for the PSMC can be applied to the other multiplicity counting systems. Finally an analysis tool, the Multiplicity TMU Estimator, was developed from this study to serve as an aid for evaluation of the total measurement uncertainty of multiplicity assay results obtained from the commonly used INCC acquisition and analysis software.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗
DOE OSTI2019

Cu/Al Through Au Diffusion Characterized by KPFM

The nanometer scale characterization technique of Frequency Modulated Kelvin Probe Force Microscopy (FM-KPFM) will be used to assess a diffusion study on thin metal films that undergo accelerated aging. The KPFM technique provides a relatively easy, non-destructive methodology that does not require high-vacuum facilities to obtain nanometer-scale spatial resolution of surface chemistry changes. The KPFM technique will be exercised in an effort to explore its capacity to map surface potential contrast caused by diffusion in a manner that allows for a qualitative assessment of diffusion of Cu or Al through Au. Supporting data will be obtained from traditional techniques: AES, XPS and UPS. An aging study was conducted on thin metal test specimens comprised of 500nm Cu or Al then 500nm Au on Si. The accelerated aging process was performed under inert conditions at aging temperatures of 100°C for Cu/Au film stack and 175°C for Al/Au film stack at aging times of 8 hours, 24 hours, 96 hours (4 days), and 216 hours (9 days).A calibration method was developed using Au, Al and Cu standards to establish precision and repeatability of the KPFM technique. The average Contact Potential Difference (CPD)s and standard deviations for each metal were found and summarized. Averages from surface roughness of the AFM topography images and roughness analysis of KPFM potential images which yield an average CPD of each area of unaged vs aged coupon surfaces were compared and show trends that indicate surface chemistry.

36 MATERIALS SCIENCE↗
DOE OSTI2023

New NBL Pu Isotopic Standards C137A and C136A as Working Reference Materials for Radiochronometry in Nuclear Forensics

Lawrence Livermore National Laboratory (LLNL) and the NBL Program Office (NBL PO) are collaborating on production of purified sub-units of the former NBS 936, 937 and 938 plutonium isotopic reference materials, which will be certified for plutonium isotopic composition and sold as certified reference materials (CRMs) C136A, C137A, and C138A, respectively. These reference materials are used throughout the United States and international community as standards for isotopic measurement method calibration and quality control and were first produced over 50 years ago. To reduce quantities of in-grown daughter products and potentially enable their use as Pu radiochronometry reference materials, the materials undergo a two-stage anion exchange purification to significantly reduce the quantities of U, Am, and Np in the source material. The purified Pu is aliquoted into ~1 mg units in the nitrate form, which will facilitate easier shipping and use compared to the 0.25 g parent units. The production process has been completed for the high- and medium- burnup isotopic standards C137A and C136A and will soon be performed for the weapons-grade Pu standard C138A. This report describes the measurement of trace actinide progeny of the Pu isotopes ( 234 U, 235 U, 236U, 241 Am and 237 Np) in purified C137A and 136A isotopic standards to provide informational values and assess the possibility of their use as working reference materials for radiochronometry.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Light Yield Calibration in MicroBooNE

The MicroBooNE detector is a Liquid Argon Time Projection Chamber (LArTPC) located along the Booster Neutrino Beam (BNB) at Fermilab. Its primary physics goal is to contribute to addressing the elusive short-baseline MiniBooNE low energy excess. MicroBooNE records and utilises both the ionisation charge and scintillation light produced inside the TPC to select and reconstruct neutrino interactions. The scintillation light collected using a plane of PhotoMultiplier Tubes (PMTs) is also used for accurate event timing and cosmic muon rejection with the latter being an important background for detectors, such as MicroBooNE, located on the surface. A good understanding of light modeling and its related systematic uncertainties is crucial to evaluate their impact on physics analyses. The experience acquired from MicroBooNE regarding how the stability of the scintillation light behaves and evolves during the 5 years of the primary physics run will be discussed as well as the calibration method used. This experience will help with understanding the physics of scintillation light in LArTPCs for the future long-running Short-Baseline Neutrino (SBN) and Deep Underground Neutrino Experiment (DUNE) programs.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

Calibration and Measurement techniques in the LLRF systems of the Fermilab PIP-II Linac

he PIP-II Accelerator is an 800 MeV superconducting Linac in the injection chain of the Fermilab accelerator complex. The LLRF systems are a based on two different hardware platforms controlling a variety of cavity types and resonance control systems including temperature, pneumatic and piezzo tuners. The various calibrations required prior to beam operation include, signal power, gradient, amplifier characterization, cavity Q measurement and detune constants. Measurements such as piezzo capacitance, cavity piezo transfer function help in determining tuner health and in devising microphonics control strategies. These measurement and calibration methods of the PIP-II LLRF system are discussed here.

Varghese, P.↗
DOE OSTI2026

MIP dQ/dx Calibration in DUNE ND-LAr Prototypes with Pixelated Charge Readout

The Deep Underground Neutrino Experiment (DUNE) will be a next-generation long baseline neutrino oscillation experiment that will employ LArTPC technology in a near detector placed at Fermilab and a far detector at the Sanford Underground Research Facility, at a baseline of 1300 km. The DUNE Liquid Argon Near Detector (ND-LAr) design takes into account the high neutrino intensity expected from the beam at the Long-Baseline Neutrino Facility (LBNF): 35 modules, each containing two optically separated time projection chambers, are instrumented with a pixel-based, true 3D charge readout alongside scintillation light traps to disentangle the O(100) interactions expected per 10us beam spill. A robust prototyping program supports ND-LAr’s design: the 2x2 Demonstrator consists of four scaled-down ND-LAr modules exposed to the NuMI beam at Fermilab, and the Full Scale Demonstrator (FSD) is a single ND-LAr module tested with cosmic rays at the University of Bern. We present here an analysis of minimum ionizing particle (MIP) tracks selected from 2x2 beam data and FSD cosmic ray data used to benchmark the pixel-based charge readout simulation and calibration in both detectors, with the ultimate goal of validating the design of DUNE ND-LAr as well as informing future calibration methods. This poster will showcase the dependence of the charge response on track inclination as well as a per-pixel dQ/dX extraction.

Mandujano, Roberto [UC, Irvine]↗
DOE OSTI2019

The Terra Vega Active Light Source: A First Step in a New Approach to Perform Nighttime Absolute Radiometric Calibrations and Early Results Calibrating the VIIRS DNB

A fully automated, National Institute of Standards and Technology (NIST)-traceable artificial light source called Terra Vega has been developed to radiometrically calibrate the Visible Infrared Imaging Radiometer (VIIRS) Day Night Band (DNB) working in high gain stage (HGS) mode. The Terra Vega active point source is a calibrated integrating sphere that is only a fraction in size of a VIIRS DNB pixel. As such, it can be considered analogous to a ground-based photometric reference star. Vicarious calibrations that employ active point sources are different than those that make use of traditional extended sources and can be applyed to quantify the brightness of artificial light sources. The active source is successfully fielded, and early results indicate that it can be used to augment and validate the radiometric calibration of the VIIRS DNB HGS sensor on both the Suomi National Polar-orbiting Partnership (NPP) and NOAA-20 satellites. The VIIRS DNB HGS sensor can benefit from this technology as on-board calibration is challenging and hinges on transferring low gain stage (LGS) calibration using a solar diffuser to the medium gain stage (MGS) and HGS via regions of overlap. Current vicarious calibration methods that use a lunar-illuminated extended source estimate the HGS radiometric accuracy to within 8-15%. By comparison, early results and analysis showed that Terra Vega is stable to about 1%. Under clear dark night conditions, predicted top-of-atmosphere radiance from Terra Vega ranged between 1–11% of VIIRS measured values. Terra Vega’s excellent stability opens up new opportunities to validate and develop nighttime imaging applications based on point sources.

Ryan, Robert↗
DOE OSTI2023

High-Resolution Image Products Acquired from Mid-Sized Uncrewed Aerial Systems for Land–Atmosphere Studies

We assess the viability of deploying commercially available multispectral and thermal imagers designed for integration on small uncrewed aerial systems (sUASs, <25 kg) on a mid-size Group-3-classification UAS (weight: 25–600 kg, maximum altitude: 5486 m MSL, maximum speed: 128 m/s) for the purpose of collecting a higher spatial resolution dataset that can be used for evaluating the surface energy budget and effects of surface heterogeneity on atmospheric processes than those datasets traditionally collected by instrumentation deployed on satellites and eddy covariance towers. A MicaSense Altum multispectral imager was deployed on two very similar mid-sized UASs operated by the Atmospheric Radiation Measurement (ARM) Aviation Facility. This paper evaluates the effects of flight on imaging systems mounted on UASs flying at higher altitudes and faster speeds for extended durations. We assess optimal calibration methods, acquisition rates, and flight plans for maximizing land surface area measurements. We developed, in-house, an automated workflow to correct the raw image frames and produce final data products, which we assess against known spectral ground targets and independent sources. We intend this manuscript to be used as a reference for collecting similar datasets in the future and for the datasets described within this manuscript to be used as launching points for future research.

47 OTHER INSTRUMENTATION↗
DOE OSTI2025

Wireless Patch Antenna Characterization for Live Health Monitoring Using Machine Learning

Temperature monitoring in extreme environments, such as coal-fired power plants, was addressed by designing and testing wireless patch antennas for use in machine learning-aided temperature estimation. The sensors were designed to monitor the temperature and health of boiler systems. Wireless interrogation of the sensor was performed using a Vector Network Analyzer (VNA) and a pair of interrogation antennas to capture resonance behavior under varying thermal and spatial conditions with sensitivities ranging from 0.052 to 0.20 $\frac{𝑀𝐻𝑧}{°C}$. Sensor calibration was conducted using a Long Short-Term Memory (LSTM) model, which leveraged temporal patterns to account for hysteresis effects. The calibration method demonstrated improved performance when combined with an LSTM model, achieving up to a 76% improvement in temperature estimation error when compared with Linear Regression (LR). The experiments highlighted an innovative solution for patch antenna-based non-contact temperature measurement, which addresses limitations with conventional methods such as RFID-based systems, infrared, and thermocouples.

20 FOSSIL-FUELED POWER PLANTS↗
DOE OSTI2023

Bump Morphology of the CMAGIC Diagram

Abstract We apply the color–magnitude intercept calibration method (CMAGIC) to the Nearby Supernova Factory SNe Ia spectrophotometric data set. The currently existing CMAGIC parameters are the slope and intercept of a straight line fit to the linear region in the color–magnitude diagram, which occurs over a span of approximately 30 days after maximum brightness. We define a new parameter, ω XY , the size of the “bump” feature near maximum brightness for arbitrary filters X and Y . We find a significant correlation between the slope of the linear region, β XY , in the CMAGIC diagram and ω XY . These results may be used to our advantage, as they are less affected by extinction than parameters defined as a function of time. Additionally, ω XY is computed independently of templates. We find that current empirical templates are successful at reproducing the features described in this work, particularly SALT3, which correctly exhibits the negative correlation between slope and “bump” size seen in our data. In 1D simulations, we show that the correlation between the size of the “bump” feature and β XY can be understood as a result of chemical mixing due to large-scale Rayleigh–Taylor instabilities.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2014

Ground-based All-sky Mid-infrared and Visible Imagery for Purposes of Characterizing Cloud Properties

This paper describes the All Sky Infrared Visible Analyzer (ASIVA), a multi-purpose visible and infrared sky imaging and analysis instrument whose primary functionality is to provide radiometrically calibrated imagery in the mid-infrared (mid-IR) atmospheric window. This functionality enables the determination of diurnal hemispherical cloud fraction (HCF) and estimates of sky/cloud temperature from which one can derive estimates of cloud emissivity and cloud height. This paper describes the calibration methods and performance of the ASIVA instrument with particular emphasis on data products being developed for the meteorological community. Data presented here were collected during a field campaign conducted at the Atmospheric Radiation Measurement (ARM) Southern Great Plains (SGP) Climate Research Facility from May 21 to July 27, 2009. The purpose of this campaign was to determine the efficacy of IR technology in providing reliable nighttime HCF data. Significant progress has been made in the analysis of the campaign data over the past several years and the ASIVA has proven to be an excellent instrument for determining HCF as well as several other important cloud properties.

analyzer↗