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At least 523 records · Page 29
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Study on Emulsification/Demulsification Behavior and Mechanism of Produced Liquid from Polymer Flooding on Alaska North Slope

Heavy oil reservoirs on Alaska North Slope (ANS) are unconsolidated and contain abundant clay minerals, where the first-ever field pilot is currently implemented to validate the use of polymer floods for heavy oil enhanced oil recovery (EOR). The polymer molecules and/or fine clay particles carried with the produced liquid could potentially affect the oil/water separation, which is one of the major concerns for field operators. This dissertation aims to investigate the emulsification behavior of produced liquid, understand the emulsifying mechanism, and seek an adaptive and cost-effective method to treat the produced liquid from polymer flooding. Emulsions were prepared by mechanically mixing the actual heavy oil and the produced water from the pilot site, of which the stability was investigated by bottle test method or multiple light scattering method. Drop size distribution and interfacial properties were measured via microscope and pendant drop technique to probe the stability mechanism further. Results showed that oil-continuous or water-continuous emulsion could be generated depending on the water cut, clay types, clay concentration, and polymer concentration. In the crude oil/water system, the increasing water cut triggered the phase inversion of oil-continuous emulsion to water-continuous emulsion, resulting in faster separation and lower emulsion stability. Whereas, clay particles, no matter added to the oil or water phase, resulted in an unfavorable phase inversion from the loose water-continuous emulsion to the tight oil-continuous emulsion as clay concentration increased. For all four types of clay except Ca-montmorillonite, clay particles added to water led to an earlier phase inversion and higher emulsion stability than that added to the oil. The dual function of polymer on emulsion stability was observed. On the one hand, both sheared and unsheared polymer tended to convert the oil-continuous emulsion formed in either crude oil/water system or complex crude oil/water/clay particle system to the water-continuous emulsion, acting as a weak demulsifier to accelerate the oil/water separation. On the other hand, the addition of polymer to the water-continuous emulsion could result in enhanced emulsion stability, which is primarily attributed to the increased viscosity of the continuous phase and the decreased drop size of the dispersed oil phase. Particularly, the sheared polymer had a weaker ability to stabilize the o/w emulsion than the unsheared polymer due to the lower viscosity of the sheared polymer solution resulting from the breakdown of the polymer macromolecules. As for the chemical demulsification tests, the performance of demulsifiers showed a complex dependency upon the water cut, the shearing intensity, demulsifier type and dosage, and the polymer concentration. A compound emulsion breaker, E12+E18, exhibited the most satisfactory demulsification performance despite the varied test conditions. For severe water-continuous emulsions that might require a multi-fold dosage of demulsifier, a less expensive electrolyte, KCl, was proposed to be used in combination with demulsifier E12+E18 to improve the demulsification performance. In the proposed demulsifier formula, the effectiveness of the commercial demulsifier relied on its destructive effect on the interfacial film, while the efficacy of KCl was mainly dependent on its viscosity reduction effect on the continuous phase. This dissertation illustrates that intermediate layer elimination and water clarification are the major challenges for produced liquid treatment from polymer flooding. It also provides practical and theoretical guidance in advance for the demulsification strategy of the produced liquid from the ongoing first-ever polymer flooding pilot on ANS.

Chang, Hongli↗
DOE OSTI2024

Dark Energy Survey Year 3: Blue Shear

Modeling the intrinsic alignment (IA) of galaxies poses a challenge to weak lensing analyses. The Dark Energy Survey is expected to be less impacted by IA when limited to blue, star-forming galaxies. The cosmological parameter constraints from this blue cosmic shear sample are stable to IA model choice, unlike passive galaxies in the full DES Y3 sample, the goodness-of-fit is improved and the $\Omega_{m}$ and $S_8$ better agree with the cosmic microwave background. Mitigating IA with sample selection, instead of flexible model choices, can reduce uncertainty in $S_8$ by a factor of 1.5.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2023

Systematic Study of Projection Biases in Weak Lensing Analysis

The nature of Dark Energy is possibly one of the most fundamental questions in Physics today. Comprising 70% of the energy density of the Universe, and being responsible for the accelerated expansion of the Universe, this mysterious form of energy with negative pressure is challenging our current understanding of the fundamental laws of nature. Cosmological parameters like total relative matter Density Ωm, the normalization of power spectrum σ8 and their combination S8 = σ8 p Ωm/0.3 are used to quantify our understanding of the evolution of the large-scale structure in the Universe and shed light on the accelerated expansion, caused by the Dark Energy, that started about halfway through the life of the Universe. Sky surveys, like Dark Energy Survey (DES), utilize weak lensing analysis to use the observations of galaxies and their shapes and extract these cosmological parameters. By doing an exhaustive study and quantifying the projection biases in the weak lensing statistics, the research work presented in this dissertation aims to contribute to the precise measurements of the cosmological parameters Ωm, σ8, and S8. For the analysis, we used the standard cosmological model that includes dark energy as the cosmological constant. And, we used the data taken by the DES experiment, which is one of the most complete, deep, and wide field surveys of the sky today.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
NASA NTRS2002

The Strengths and Weaknesses of Logic Formalisms to Support Mishap Analysis

The increasing complexity of many safety critical systems poses new problems for mishap analysis. Techniques developed in the sixties and seventies cannot easily scale-up to analyze incidents involving tightly integrated software and hardware components. Similarly, the realization that many failures have systemic causes has widened the scope of many mishap investigations. Organizations, including NASA and the NTSB, have responded by starting research and training initiatives to ensure that their personnel are well equipped to meet these challenges. One strand of research has identified a range of mathematically based techniques that can be used to reason about the causes of complex, adverse events. The proponents of these techniques have argued that they can be used to formally prove that certain events created the necessary and sufficient causes for a mishap to occur. Mathematical proofs can reduce the bias that is often perceived to effect the interpretation of adverse events. Others have opposed the introduction of these techniques by identifying social and political aspects to incident investigation that cannot easily be reconciled with a logic-based approach. Traditional theorem proving mechanisms cannot accurately capture the wealth of inductive, deductive and statistical forms of inference that investigators routinely use in their analysis of adverse events. This paper summarizes some of the benefits that logics provide, describes their weaknesses, and proposes a number of directions for future research.

Johnson, C. W.↗
NASA NTRS1994

Landau damping of magnetospherically reflected whistlers

Unducted VLF signals produced by lightning activity can form a population of magnetospherically reflected (MR) whistlers in the inner magnetosphere. It has been suggested recently that in the absence of significant attenuation such waves could merge into a broadband continuum with sufficient intensity to account for plasmaspheric hiss. To test this conjecture we have evaluated the path-integrated attenuation of MR whistlers along representative ray paths using the HOTRAY code. Using a realistic plasma distribution modeled on in-situ data, we find that the majority of MR waves experience significant damping after a few transits across the equator. This is primarily due to Landau resonance with suprathermal (0.1-1 keV) electrons. The attenuation is most pronounced for waves that propagate through the outer plasmasphere; this can readily account for the infrequent occurrence of multiple-hop MR waves for L greater than or equal to 3.5. Selected waves that originate at intermediate latitudes (15 deg is less than or equal to lambda is less than or equal to 35 deg) and whose ray paths are confined to the inner plasma- sphere may experience up to 10 magnetospheric reflections before substantial attentuation occurs. These waves should form the population of observed MR waves. Wave attenuation becomes more pronounced at higher frequencies; this can account for the absence of multiple-hop waves above 5 kHz. Weakly attenuated MR waves tend to migrate outward to the L shell, where their frequency is comparable to the equatorial lower hybrid frequency. The enhanced concentration of waves due to a merging of ray paths would produce a spectral feature that rises in frequency at lower L. This is quite distinct from the reported properties of plasmaspheric hiss, which maintains a constant frequency band throughout the entire plasmasphere. Furthermore, in the absence of mode conversion, waves below 500 Hz, which often form an important if not dominant part of the spectral properties of hiss, are unable to escape from the topside ionosphere in the whistler mode. Consequently, we conclude that unducted lightning signals cannot account for the origin of plasmaspheric hiss.

Thorne, Richard M.↗
NASA NTRS1992

Kasei Valles, Mars - Interpretation of canyon materials and flood sources

Kasei Valles form the most immense outflow channel system on Mars. Here, the materials that make up the canyon walls and floors of Kasei Valles are investigated along with the sources of the flood waters. It is proposed that the geological sequence of plateau materials through which Kasei Valles cuts is capped by ridged plains material overlying relatively weak Noachian plateau materials that increase in resistance to erosion below 1000 m depth. Flooding began in the Late Hesperian, probably originating from the Tharsis rise, here volcanotectonic activity produced high ground-water pressures. Ground water sluiced through hydrofractures above the resistant zone at 1000 m depth and erupted in northern Kasei Valles, forming mostly northeast-trending troughs of Sacra Fossae and etching joints in the ridged plains material. Some of the flood water invaded the upper weak zone of the Noachian plateau materials, producing chaotic and knobby terrains of low relief.

Tanaka, Kenneth L.↗
DOE OSTI2023

Universal and nonuniversal features of Bardeen-Cooper-Schrieffer theory with finite-range interactions

Here, we study analytic solutions to the Bardeen-Cooper-Schrieffer (BCS) gap equation for isotropic superconductors with finite-range interaction potentials over the full range of temperatures from absolute zero to the superconducting critical temperature 0 ≤ T ≤ T c . Using these solutions Δ (ε,T), we provide a proof of the universality of the temperature dependence of the BCS gap ratio at the Fermi level Δ (ε = 0,T)/T c . Moreover, by examining the behavior of this ratio as a function of energy ε, we find that nonuniversal features emerge away from the Fermi level, and these features take the form of a temperature-independent multiplicative factor F(ε), which is equal to Δ (ε,T)/Δ(ε = 0,T) up to exponentially small corrections, i.e., the error terms vanish like e -1/λ in the weak-coupling limit λ → 0. We discuss the model-dependent features of both F(ε) and T c , and we illustrate their behavior focusing on several concrete examples of physically relevant finite-range potentials. Comparing these cases for fixed coupling constants, we highlight the importance of the functional form of the interaction potential in determining the size of the critical temperature and provide guidelines for choosing potentials which lead to higher values of T c . We also propose experimental signatures which could be used to probe the energy dependence of the gap and potentially shed light on the underlying mechanisms giving rise to superconductivity.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2025

Highly Active Hydrogen Evolution Reaction (HER) Catalysts Formed by Energetic Pt n Cluster Deposition: Deposition Dynamics and the HER Mechanism

Mass-selected Pt n + (n ≤ 7) were deposited at variable energies on highly oriented pyrolytic graphite (HOPG), creating highly active hydrogen evolution reaction (HER) electrocatalysts. HER mass activities were ~2 to >10 times higher than those for the surface atoms in bulk Pt and for Pt n deposited on several other supports. Thus, high activity reflects the Pt-C structures formed by energetic Pt n -HOPG impacts, in addition to high Pt surface availability. The Pt n /HOPG electrodes were probed by X-ray photoelectron spectroscopy, low energy ion scattering, and electron microscopy. Born-Oppenheimer molecular dynamics (BOMD) was used to simulate Pt n - HOPG impacts, revealing the types of structures formed at different energies, then DFT was used to probe their most important HER pathways. For low deposition energies, the Pt n deposit onto the HOPG surface with sub-unit sticking probability, aggregating at defects. With increasing deposition energy, the sticking probability initially decreases, then rises to unity as subplantation and defect creation allow formation of strongly bonded platinum-carbon structures. Barriers for HER on these structures were found to be low and weakly dependent on Pt n size, consistent with experiment. The activities were highest for small covalently-bonded Pt-C structures created at high deposition energies. The larger aggregated structures formed at low energies were less active, but still substantially better than the bulk Pt surface monolayer. The catalysts were stable in repeated potential cycling at reducing potentials, but electrodes containing subplanted Pt became more active when scanned to oxidizing potentials, due to emergence of subplanted Pt onto the surface.

08 HYDROGEN↗
NASA NTRS1996

Enhancing Adhesion: Relative Merits of Different Approaches

Adhesive performance is improved mainly by manipulation of the bimaterials interface zone, which is only a few molecules thick. There are three approaches to enhancement of interfacial adhesion at the molecular level. They are 1) changing the nonchemically bonded interactions across the interface from weak ones to strong ones, 2) making the true interfacial area much larger than the simple geometric area, and 3) inducing chemical bonding between the two materials forming the interface. Our goal this summer was to question some of the built-in assumptions contained within these approaches and to determine the most promising approach, both theoretically and practically, for enhancing adhesion in NASA structures. Our computations revealed that all three of these approaches have, in theory, the potential to enhance molecular adhesion approximately ten-fold. Experiments, however, revealed that this excellent level of enhancement is not likely to be reached in practice. Each approach was found to be severely limited by practical problems. In addition, some of the built-in assumptions associated with these approaches were found to be insufficient or inadequate. The first approach, changing the nonchemically bonded interactions from weak to strong, Is an example of one containing inadequate assumptions. The extensive literature on intermolecular interactions, based on solution studies, shows that certain functional group pairs interact much more strongly than others. It has always been assumed that these data can be reliably extended to systems where only one member of the pair is in solution and the other Is contained in a solid surface. Our experiments this summer demonstrated that solution data do not adequately predict the strength of functional group interaction at the solid-liquid interface. Furthermore, the strong solvents needed to dissolve the monomers or polymers to which the functional groups of interest are attached compete successfully with the solid surface for the functional group. As a result, functional groups in solution cannot pair with the complementary groups in the solid surface, and the expected enhancement of nonchemically bonded interactions is not realized. The second approach, increasing the true interfacial area, is an example of one containing inadequate assumptions and suffering from numerous practical problems. First, practitioners have assumed that material removal, such as bead blasting or etching, increases true surface area (and therefore interfacial area) in a meaningful way. Our geometric analysis demonstrated that removal methods increase area by a factor of two at most. To increase interfacial area by an order of magnitude or more. a thin layer of high porosity must be added to the substrate surface prior to application of the adhesive phase. Consistent with this finding, we attempted to create a thin layer of rigid, highly porous glass on the surface of our smooth glass substrate by means of sol-gel technology. We were unable to surmount a wide variety of practical problems and obtained only collapsed, nonporous layers. Thus this approach, appealing in principle, would require long term development and is not promising in the near term. The third approach, inducing chemical bonding at the interface, is an example of one having neither inadequate assumptions nor insurmountable practical problems. When silicate glass is the substrate, there are only a few chemical reactions that can be successfully conducted to create these chemical bonds, and these reactions usually involve silicon-containing reagents. We compared the silazane reagents to the silane reagents and found through experiment that the silazanes react with the glass surface much more readily, and under milder conditions, than the silanes. The functional groups attached to the glass surface by silazane reactions were not able to be removed by solvent extraction, elevated temperature exposure, or mechanical action. This clearly indicates that the formation of chemical bonds at the interface is the most effective approach for enhancing molecular adhesion.

Penn, L. S.↗
DOE OSTI2022

Correlation between Redox Potential and Solvation Structure in Biphasic Electrolytes for Li Metal Batteries

The activity of lithium ions in electrolytes depends on their solvation structures. However, the understanding of changes in Li + activity is still elusive in terms of interactions between lithium ions and solvent molecules. Herein, the chelating effect of lithium ion by forming [Li(15C5)] + gives rise to a decrease in Li + activity, leading to the negative potential shift of Li metal anode. Moreover, weakly solvating lithium ions in ionic liquids, such as [Li(TFSI) 2 ] - (TFSI = bis(trifluoromethanesulfonyl)imide), increase in Li + activity, resulting in the positive potential shift of LiFePO 4 cathode. This allows the development of innovative high energy density Li metal batteries, such as 3.8 V class Li | LiFePO 4 cells, along with introducing stable biphasic electrolytes. In addition, correlation between Li + activity, cell potential shift, and Li + solvation structure is investigated by comparing solvated Li + ions with carbonate solvents, chelated Li + ions with cyclic and linear ethers, and weakly solvating Li + ions in ionic liquids. These findings elucidate a broader understanding of the complex origin of Li + activity and provide an opportunity to achieve high energy density lithium metal batteries.

25 ENERGY STORAGE↗
DOE OSTI2025

A Reductively Stable Electrolyte Realizes Deep Cycling Behavior in Anode‐free Sodium Batteries

For anode‐free sodium batteries to achieve practical consideration, highly reversible chemistries require exceptional ≥99.95% coulombic efficiencies that maintain over prolonged cycling periods. To do so, consumption of this severely limited sodium inventory must be restricted while metal nucleation processes that comprise the in situ formed metal anode are improved. Herein, we describe a fluorine‐free carborane electrolyte that satisfies these criteria by emphasizing reductive stability and weakly coordinating anion behavior as design principles. We find this approach promotes the development of a thin, robust SEI chemistry rich in both organic speciation and boron. The electrolyte described herein exhibits ideal metal nucleation behavior on one‐micron thin carbonaceous current collector surfaces and achieves a metal deposition/stripping efficiency near parity for 400 cycles. This novel anode chemistry is introduced to anode‐free full cell configurations where 87% of the initial discharge capacity is retained after 1000 cycles at 2.0 C. In conclusion, post‐test characterization of deep‐cycled anode‐free cells reveals suppressed capacity fade in these systems is attributed to the chemical stability of the carborane anion.

anode-free↗
DOE OSTI2020

A composite Higgs with a heavy composite axion

We consider the strong dynamics associated with a composite Higgs model that simultaneously produces dynamical axions and solves the strong CP problem. The strong dynamics arises from a new Sp or SU(4) hypercolor gauge group containing QCD colored hyperfermions that confines at a high scale. The hypercolor global symmetry is weakly gauged by the Standard Model electroweak gauge group and an enlarged color group, SU(N + 3) × SU(N)'. When hyperfermion condensates form, they not only lead to an SU(5)/SO(5) composite Higgs model but also spontaneously break the enlarged color group to SU(3) c × SU(N) D . At lower energies, the SU(N) D group confines, producing two dynamical axions that eliminates all CP violation. Furthermore, small instantons from the SU(N)' group can enhance the axion mass, giving rise to TeV scale axion masses that can be detected at collider experiments. Our model provides a way to unify the composite Higgs with dynamical axions, without introducing new elementary scalar fields, while also extending the range of axion masses that addresses the strong CP problem.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

High compressive energy absorption and shape recovery behavior of additively manufactured textile-inspired cylindrical braided metamaterials

Mechanical metamaterials (MMs) are engineered structures with unique mechanical properties that arise from their unique spatial arrangement or lattice-like structure. The most commonly designed MMs such as honeycomb and re-entrant auxetics are prone to failure at the sharp corners and weak joints due to the increased stress concentration under deformation. To mitigate this challenge, braided MM structures involving intertwining threads of nylon—forming curved unit cells—have been studied. These textile-inspired cylindrical braided metamaterials (CBMMs) with contrasting unit cells, namely diamond and regular CBMMs, were fabricated by 3D printing. The layer-by-layer deposited structure built by fused filament fabrication delivered an assembly of overlapped threads that are fused at the contact point. To understand deformation behavior of these MMs, finite element models were developed for various load scenarios including quasi-static compression, cyclic and creep loads at room temperature. Stress distribution, deformation mechanisms, and failure modes were analyzed and validated by experiments to analyze the geometries and associated performance. The diamond CBMMs showed stress softening at 30 % compressive strain, withstanding a load of ∼440 N, whereas the regular CBMMs at 50 % strain experienced ∼250 N. The diamond CBMMs delivered higher creep resistance under sustained load and better energy absorption under cyclic loading than the regular CBMMs. The latter, however, exhibited 94 % shape recovery in contrast to 88 % recovery in former prototype during their first cyclic load. In conclusion, this study helps design mechanical lightweight devices that endure significant sustained load and exhibit enhanced energy absorption and shape recovery characteristics in cyclic loading.

Creep↗
DOE OSTI2024

Real-time observation of the exchange process between H 2 O and NO in the metal–organic framework Ni-MOF-74

Molecular exchange is a common step occurring in many technological processes such as competitive adsorption, chemical separation, capture, delivery, and release. However, the underlying principle is not fully understood, especially in nanoconfined environments where the energetics and kinetics of such processes can deviate from that on flat surfaces. In this study, we unravel the mechanism of a molecular exchange process by studying the displacement of NO by H 2 O in Ni-MOF-74 in real-time using in situ infrared spectroscopy combined with ab initio calculations. We show that weakly bound H 2 O gradually displaces strongly bound NO on the metal sites by first weakening the M–N bond through forming H-bond and then moving the NO away so that it eventually desorbs. Interestingly, we further find that additional water facilitates this exchange by significantly lowering the kinetic barrier associated with this process as well as the overall energy of the final state. Although our study focuses on Ni-MOF-74, we believe that our finding and explanation of unexpected exchange phenomena—where strongly adsorbed molecules are apparently easily displaced by much weaker bound H 2 O—is applicable to a much larger group of frameworks and will be helpful in designing and improving MOFs for real-world applications where humidity is often present.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1982

Visible signatures of the multi-step transition to a beam-plasma-dicharge

Observations are presented of the beam-plasma-discharge (BPD) at pressures below 4 x 10 to the -6th Torr, which show that there are three abrupt transitions in the beam-plasma interactions. The low-current A1 state (the basic beam with its noded configuration), is dominated by direct collisional ionization of the background gas. In the A2 state (the noded beam surounded by a weak halo), the ionization is supplemented by another mechanism which perhaps involves cyclotron interactions. The B and C states are distinctly separate forms of the BPD which involve a convective redistribution of beam energy as indicated by the changes in the beam nodes. The B and C states are also found to involve enhancements of between 20-100 in the power dissipation by ionization. Thus, in a 20 m pathlength, it is found that approximately 1-4 percent of the beam power is dissipated by the ionization associated with the BPD.

Hallinan, T. J.↗
NASA NTRS1992

Effects of long-wavelength dissipation on beam-driven Langmuir turbulence

The effects of long-wavelength dissipation on beam-driven Langmuir turbulence are investigated using numerical simulations that include both weak and strong turbulence effects. Strong-turbulence wave collapses occur concurrently with weak-turbulence energy cascades if the long-wavelength damping is sufficiently small relative to the growth rate of the beam-unstable waves. Above a threshold damping level, only the weak-turbulence backscatter cascade is observed, and it becomes increasingly truncated as the damping increases, eventually consisting of only a single backscatter. A simple Lotka-Volterra model gives an excellent description of the periodic evolution observed in the weak-turbulence regime. Suppression of the usual backscatter cascade by long-wavelength damping enables intense beam-aligned density troughs to form, which trap and duct Langmuir waves.

Robinson, P. A.↗
NASA NTRS1993

Circularly polarized radio emission from the T Tauri star Hubble 4

Multiwavelength VLA observations of the weak-lined T Tauri star (WTTS) Hubble 4, which is located in the nearby (about 140 pc) Taurus-Auriga star-forming region, are reported. The emission is characterized by a nearly flat spectral energy distribution with a spectral index of 0 (S sub nu varies as nu exp alpha). Right circular polarization was detected at both 3.6 and 6 cm at levels of 19 +/- 5 percent and 18 +/- 3 percent, respectively, with an upper limit of not more than 15 percent (3 sigma) at 20 cm. The star was in a state of low radio activity, with flux densities of 1.3-1.7 mJy and a radio luminosity of 10 exp 16.5 ergs/Hz s. The unambiguous detection of circularly polarized radio emission from Hubble 4 provides direct evidence for the existence of ordered magnetic fields in this WTTS.

Skinner, Stephen L.↗
NASA NTRS1994

The deformation of flux tubes in the solar wind with applications to the structure of magnetic clouds and CMEs

Two dimensional magnetohydrodynamic simulations of the distortion of a magnetic flux tube, accelerated through ambient solar wind plasma, are presented. Vortices form on the trailing edge of the flux tube, and couple strongly to its interior. If the flux tube azimuthal field is weak, it deforms into an elongated banana-like shape after a few Alfven transit times. A significant azimuthal field component inhibits this distortion. In the case of magnetic clouds in the solar wind, it is suggested that the shape observed at 1 AU was determined by distortion of the cloud in the inner heliosphere. Distortion of the cloud beyond 1 AU takes many days. It is estimated that effective drag coefficients slightly greater than unity are appropriate for modeling flux tube propagation. Synthetic magnetic field profiles as would be seen by a spacecraft traversing the cloud are presented.

Cargill, Peter J.↗