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At least 523 records · Page 29

Comparative study of microstructure and properties of low-alloy-steel/nickel-based-alloy interfaces in dissimilar metal weld joints prepared by different GTAW methods

Highlights: • Number of type I and type II boundaries: H-DMWJ > C-DMWJ > W-DMWJ. • Width carbon depleted zones and carbon enriched zones: H-DMWJ > C-DMWJ > W-DMWJ. • Type I and type II boundaries are susceptible to SCC and cracked during mechanical bending. • C-DMWJ has the best performance while H-DMWJ has the worst one. - Abstract: Low-alloy-steel/buttering (or welding) metal interfaces in safe-end dissimilar metal weld joints (DMWJs) at nuclear power plants are weak parts. To optimize the quality of the safe-end DMWJs used for the construction of domestic nuclear power plants and to improve the welding productivity, a series of DMWJs in full-size have been manufactured by using different gas tungsten arc welding (GTAW) methods. The microstructure, chemical composition distribution and local properties across the SA508/52(M) interfaces in these DMWJs are studied. The high heat input and long high temperature duration during hot-wire GTAW process promote the carbon diffusion and grain boundary migration and hence the DMWJ by hot-wire GTAW has the largest amount of type I and type II boundaries and the widest carbon depleted zones and carbon enriched zones, which resulting in the worst performance among the DMWJs in simulated primary water. Type I and type II boundaries are high angle random grain boundaries (RGBs) and Cr-depleted zones are found along type II boundaries resulting in their high susceptibility to SCC. In addition, these boundaries are prone to be cracked during mechanical bending process.

36 MATERIALS SCIENCE↗

Microstructural evolution and hardness response in the laser beam welded joints of pure titanium during recrystallization and grain growth

Highlights: • The LABs and high local misorientations indicate the existence of plastic strains in the as-welded HAZ and FZ. • During heat treatment the recrystallization occurs in the HAZs, decreasing plastic strains, but it doesn't appear in the FZs. • The coarse and unstrained grains gradually replace the fine and strained ones in the HAZs during recrystallization. • The decrease of plastic strains in the HAZs during recrystallization causes the descent of average hardness values based on the strain strengthening. - Abstract: Microstructural evolution and hardness response in the laser beam welded joints of pure titanium during recrystallization and grain growth were investigated by means of electron backscatter diffraction and hardness measurement. The low-angle boundaries (LABs) and high local misorientations, in the as-welded heat affected zone (HAZ) and fusion zone (FZ), indicate the existence of plastic strains caused by the plastic strains due to the thermal stress and the non-equilibrium phase transformations. The recrystallization occurs in the HAZs during heat treatment, but the grain growth after recrystallization does not appear under the heat treatment conditions. Moreover as a result of the slightly high impurity contents in the as-welded FZ, no distinct recrystallization is found in the FZs in this work. During recrystallization in the HAZs, the coarse and unstrained grains with equiaxed shape and smooth boundary gradually consume the fine and strained ones with irregular shape and serrate boundary. Meanwhile, the LABs disappear and the low local misorientations replace the high ones in the modified grains. The recrystallization during heat treatment causes the decrease of plastic strains in the HAZs, which reflects on the descent of average hardness values based on the strain strengthening.

36 MATERIALS SCIENCE↗

Macroscale property assessment and indentation characteristics of thick section friction stir welded AA 5083

The spatial gradients in microstructure have been proven to be effective in optimizing the performance of components, and several techniques have been developed to achieve this microstructure. Nevertheless, the local microstructural modification methods inevitably result in the formation of gradient microstructure leading to a variation in the property. Herein this work systematically investigates the effect of gradient microstructure formed during thick section friction stir weld Al5083 alloy on its mechanical properties. A novel macro-indentation technique, profilometer-based indentation plastometry (PIP), is utilized to capture the variation in the mechanical properties in the feedstock (rolled plate) and weld region. The feedstock exhibited a gradient microstructure owing to different stress states during rolling. Additionally, the stirring of the tool resulted in a complex material flow pattern producing a microstructure gradient in the weld region. The aspect ratio of the grains was identified as the primary factor causing variation in indentation response in the feedstock. In contrast, variation in the grain size in the weld region resulted in property variation. Overall, the stir zone has a lower yield strength (158±4MPa) than the base material (173±3MPa). In addition, microstructure heterogeneity in the stir zone resulted in lower elongation than the base material.

36 MATERIALS SCIENCE↗

The Role of Friction Stir Welding on the Microstructure and Mechanical Properties of AZ31B-H24 Mg alloy

In this study, an attempt was made to join AZ31B magnesium alloy by friction stir welding (FSW) process. A single tool with cylindrical screw threaded pin was used to investigate the effect of welding parameters on microstructure and mechanical properties of stir zone (SZ). Several welds were made at different rotational ({omega}) and traverse ({upsilon}) speeds, while the {omega}/{upsilon} ratios were kept constant. The optical and scanning electron microscopy were used to study the variation of microstructure across the welds. Moreover, micro-hardness and tensile tests were carried out to evaluate the mechanical properties of joints. It was found that {omega} plays more significant role on the resulted grain structure than {upsilon}, and at a constant {omega}/{upsilon} ratio, decreasing rotational speed decreased the size of grains, and hence, improved the hardness value and the tensile strength of the SZ.

36 MATERIALS SCIENCE↗

Laser-ultrasonic inspection of hybrid laser-arc welded HSLA-65 steel

The hybrid laser-arc welding (HLAW) process is a relatively low heat input joining technology that combines the synergistic qualities of both the high energy density laser beam for deep penetration and the arc for wide fit-up gap tolerance. This process is especially suitable for the shipbuilding industry where thick-gauge section, long steel plates have been widely used in a butt joint configuration. In this study, preliminary exploration was carried out to detect and visualize the welding defects using laser ultrasonics combined with the synthetic aperture focusing technique (SAFT). Results obtained on 9.3 mm thick butt-welded HSLA-65 steel plates indicated that the laser-ultrasonic SAFT inspection technique can successfully detect and visualize the presence of porosity, lack of fusion and internal crack defects. This was further confirmed by X-ray digital radiography and metallography. The results obtained clearly show the potential of using the laser-ultrasonic technology for the automated inspection of hybrid laser-arc welds.

36 MATERIALS SCIENCE↗

Wear behavior of the surface alloyed AISI 1020 steel with Fe-Nb-B by TIG welding technique

Weld overlay coatings also known as hardfacing is a method which involves melting of the alloys and solidification for applied coatings. Recently hardfacing by welding has become a commonly used technique for improvement of material performance in extreme (high temperature, impact/abrasion, erosion, etc.) conditions.In the present study, the coatings were produced from a mixture of ferrous niobium, ferrous boron and iron powders in the ranges of -45µm particle size with different ratio. Fe{sub 12}Nb{sub 5}B{sub 3} and Fe{sub 2}NbBalloys were coated on the AISI 1020 steel surface by TIG welding. The phases formed in the coated layer are Fe{sub 2}B, NbB{sub 2}, NbFeB and Fe0,2 Nb{sub 0,8} phases. The hardness of the presence phases are changing between 1689±85 HV{sub 0.01}, and 181±7 HV{sub 0.1}. Microstructural examinations were realized by optical and scanning electron microscopy. The wear and friction behaviors of Fe{sub 12}Nb{sub 5}B{sub 3} and Fe2NbB realized on the AISI 1020 steel were investigated by the technique of TIG welding by using ball-on-disk arrangement against alumina ball.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Model Predictive Control of GTAW Weld Pool Penetration

Weld pool penetration is a major implication of weld integrity but it is not directly measurable. The key to solving this issue is to find or create observable phenomena that can be used to derive the penetration. An innovative method has recently been proposed/developed to derive the penetration from the reflection of projected laser from an oscillating weld pool surface. Yet, in addition to the penetration, the oscillation, thus the reflection determined by it, also depends on the pulse amplitude of the current, which needs to be adjusted as the control variable to feedback control the penetration as the output. This dependence imposes a constraint on the control algorithm such that the adjustment of the control variable must be relatively slow to minimize additional sources that affect the oscillation/sensor. This restriction on the control variable adjustment also brings challenges to the identification of the dynamic model of the weld process to be controlled, which has to apply a varying control signal to stimulate the dynamics. To solve these issues, this letter proposes using a low order model to catch the dominant dynamics such that a high speed variation in the control signal can be avoided when choosing the model predictive control algorithm. This allows use of relatively poor models to determine the adjustment on the pulsing amplitude, and still achieves relatively accurate control. Experimental results verified the effectiveness of the resultant penetration control system despite the restrictions imposed by the penetration sensor, which affect the identification of high order dynamics and free adjustments of control variables.

42 ENGINEERING↗

Modelling of the effect of process parameters on tensile strength of friction stir welded aluminium alloy joints

Friction stir welding (FSW) process is a promising solid-state joining process with the potential to join low-melting point material, particularly, aluminium alloy. The most attractive reason for joining aluminium alloy with this process is the avoidance of the solidification defects formed by conventional fusion welding processes. In this article, an attempt has been made to develop an empirical relationship between FSW variables and tensile strength. Central composite rotatable design was used by considering four factor and five levels, which enables to quantify the direct and interactive effect of four numeric factors, that is, tool rotational speed, welding speed, axial force, and tapered pin diameter on the tensile strength. The developed relationship is useful for prediction of tensile strength in friction stir welded AA6082 aluminium alloy joints at 95% confidence level. It will also be helpful for selection of process variable to obtain desired strength of the joint. Furthermore, the optimized capabilities in design-expert software were used to numerically optimize the input parameters. At the optimal parameters, three experiments were conducted to compare the predicted value of tensile strength with the experimental value.

36 MATERIALS SCIENCE↗

Diffusion Welding of Alloys for Molten Salt Service – Status Report

The present work is concerned with heat exchanger development for molten salt service, including the proposed molten salt reactor (MSR), a homogeneous reactor in which the fuel is dissolved in a circulating fluid of molten salt. It is an outgrowth of recent work done under the Next Generation Nuclear Plant (NGNP) program; what the two reactor systems have in common is an inherently safe nuclear plant with a high outlet temperature that is useful for process heat as well as more conventional generation The NGNP program was tasked with investigating the application of a new generation of nuclear power plants to a variety of energy needs. One baseline reactor design for this program is a high temperature, gas-cooled reactor (HTGR), which provides many options for energy use. These might include the conventional Rankine cycle (steam turbine) generation of electricity, but also other methods: for example, Brayton cycle (gas turbine) electrical generation, and the direct use of the high temperatures characteristic of HTGR output for process heat in the chemical industry. Such process heat is currently generated by burning fossil fuels, and is a major contributor to the carbon footprint of the chemical and petrochemical industries. The HTGR, based on graphite fuel elements, can produce very high output temperatures; ideally, temperatures of 900°C or even greater, which has significant energy advantages. Such temperatures are, of course, at the frontiers of materials limitations, at the upper end of the performance envelope of the metallic materials for which robust construction codes exist, and within the realm of ceramic materials, the fabrication and joining of which, on the scale of large energy systems, are at an earlier stage of development. A considerable amount of work was done in the diffusion welding of materials of interest for HTGR service with alloys such as 617 and 800H. The MSR output temperature is also materials limited, and is projected at about 700°C. (RR E) A different set of alloys, such as Alloy N and 242, are needed to handle molten salts at this temperature. The diffusion welding development work described here builds on techniques developed during the NGNP work, as applied to these alloys. There is also the matter of dissimilar metal welding, since alloys suitable for salt service are generally not suited for service in gaseous oxidizing environments, and vice versa, and welding is required for the Class I boundaries in these systems, as identified in the relevant ASME codes.

02 PETROLEUM↗

Towards High-Speed friction stir welding of 25 mm Thick AA2139-T8: tool innovation and process development

Joining thick plates (≥ 12 mm) of aluminum (Al) alloys is challenging due to high tool forces, uneven material flow, and non-uniform heat distribution through the material’s thickness. Recent advancements in tool design and welding parameters for friction stir welding (FSW) in thick plates butt joining have encountered a developmental plateau, highlighting the need for innovative approaches to overcome existing limitations. Here, this study focuses on the systematic development of single-pass and double-pass FSW processes for high-strength aluminum alloy AA2139-T8, to improve joint efficiency and enable high-speed welding capabilities. Experimental evidence is presented for a novel tool design with opposing pin threads, enabling high-speed (178 mm/min) single-pass friction stir butt welding of 25 mm thick AA2139-T8. A series of FSW trials was conducted both in air and with a trailing water spray, using steel backing plates (BPs) to investigate the impact of quenching and cooling rates on process response and joint performance. A joint efficiency of 83% was attained using the novel tool features and effectively controlling process forces and thermal boundary conditions.

AA2139-T8↗

Experimental Investigation on Acoustic Control Droplet Transfer in Ultrasonic-Wave-Assisted Gas Metal Arc Welding

Ultrasonic-wave-assisted gas metal arc welding (U-GMAW) is a new, advanced arc welding method that uses an ultrasonic wave emitted from an ultrasonic radiator above the arc. However, it remains unclear how the ultrasonic wave affects the metal droplet, hindering further application of U-GMAW. In this paper, an improved U-GMAW system was used and its superiority was experimentally demonstrated. Then a series of experiments were designed and performed to study how the ultrasonic wave affects droplet transfer, including droplet size, velocity, and motion trajectory. The behavior of droplet transfer was observed in high-speed images. The droplet transfer is closely related to the distribution of the acoustic field, determined by the ultrasonic current. Moreover, by analyzing the variably accelerated motion of the droplet, the acoustic control of the droplet transfer was intuitively demonstrated. Finally, U-GMAW was successfully used in vertical-up and overhead welding experiments, showing that U-GMAW is promising for use in welding in all positions.

36 MATERIALS SCIENCE↗

Phase-Field Modeling of Nugget Zone for a AZ31-Mg-Alloy Friction Stir Weld

This work presents simulation of microstructure evolution in the nugget zone (NZ) of a AZ31-Mg-alloy friction stir weld. The process parameters (tool geometrical characteristics, rotational speed, travel speed, applied load) have been correlated with the resulting microstructural features in the NZ of the weld (grain size and population) with the aid of the MICRESS software, which provides the ability to simulate both nucleation and grain growth during dynamic recrystallization phenomena evolving in the NZ during the weld thermal cycle. The input parameters of the developed model include the tool geometry, the welding conditions as well as the recrystallization energy, the grain boundary mobility and specific material properties. NZ microstructure obtained by simulation shows good agreement with experimental measurements for both grain population and size.

36 MATERIALS SCIENCE↗

Microstructure and Mechanical Characterization of Friction-Stir-Welded 316L Austenitic Stainless Steels

Fusion welding of austenitic stainless steels (ASSs) causes undesirable metallographic changes. An attempt has been made to join 3-mm-thick 316L ASS plates using friction stir welding and correlate the microstructural evolution and the mechanical properties under various welding conditions. Tungsten alloy (W-Re) tool was employed for welding. Successful joints were obtained within a range of traverse speeds (45-85 mm/min) used in this work. Various zones were observed across the joint line. The stir zone exhibited considerable grain refinement and traces of delta ferrite phase. EBSD images showed a decreasing grain size with increased traverse speed. XRD patterns and TEM images confirmed the existence of delta ferrite. The mechanical properties of the joints including microhardness, tensile strength, impact toughness and bending were further reported.

36 MATERIALS SCIENCE↗

Evaluation of Plastic “Eta” Factor for Welds of SS316L(N) with High Strength Mismatch Ratio

Fracture testing standards of ASTM and ISO recommend expressions for plastic η factor of various fracture test specimen geometries to evaluate the fracture behavior of materials. These are intended for homogenous specimens, but according to ISO 15653, it can be extended for weldments up to a strength mismatch ratio (M) of 1.25. In practice, M > 1.25 is encountered in many applications. In the present study, η factor has been evaluated for welded compact tension specimens using a limit load-based approach. The η factors obtained using this approach for homogenous specimens with elastic–perfectly plastic material model are found to be within ± 4% of those from the ASTM E 1820-17a, thereby validating the procedure. For welds, the limit load is obtained from nonlinear (elastic–plastic) FE simulations. η factors for specimens with various crack lengths (a), weld width (h) and strength mismatch have been evaluated and found to be significantly influenced by these parameters. For M > 1.25, the estimated η values were found to be ~ 16% lower compared to that from the ASTM E 1820-17a. Thus, the use of the η values from the proposed method provides a conservative estimate of J–R curve for the welds. Further, it has been observed that depending on the slope of the blunting line, the J{sub Ic} value may vary significantly with the estimated η values.

36 MATERIALS SCIENCE↗

Electron Beam Welding of Nimonic 80A Superalloy: Microstructure Evolution and EBSD Study After Aging Heat Treatment

The purpose of this research was to evaluate integrity and microstructure changes of the electron beam-welded Nimonic 80A and the base metal after aging heat treatment process, i.e., 700 °C/72 h/air cooling. Here, microstructure, microhardness and tensile were investigated by various tools, i.e., scanning electron microscope with energy-dispersive spectroscopy and electron backscatter diffraction, x-ray diffraction analysis and Vickers hardness. Evaluation of microstructure shows that the weld zone mainly consists of columnar dendrites. The effect of aging heat treatment on the microstructure morphology and phase structure is very limited. Also, it was observed that there are obvious segregation and precipitates in intracrystalline and along the grain boundaries after aging heat treatment. Electron backscatter diffraction results show that the weld zone and base metal have a clear difference in the grain boundary characterization and kernel average misorientation at room temperature and after aging heat treatment, which leads to a difference in microhardness of the weld zone. In addition, the relationship between microhardness and tensile strength is discussed.

36 MATERIALS SCIENCE↗

Mechanical Properties and Corrosion Behavior of AA5754-AA6061 Dissimilar Aluminum Alloys Welded by Cold Metal Transfer

The trend of using lightweight materials in the automotive industry brings along the necessity of dissimilar welding of aluminum alloys such as AA5754 and AA6061. Hybrid structures in automobiles are subjected not only to mechanical forces but also corrosive effects of the environment. In this study, cold metal transfer welding, which is suitable for welding thin sheets and dissimilar materials, was applied to join AA5754 to AA6061. It was aimed to investigate the effect of weld heat input on mechanical properties and corrosion rate measured by the Tafel extrapolation method in 3.5 wt.% NaCl solution at room temperature. The tensile strength of AA5754-AA6061 joints tended to reduce with increasing heat input. Corrosion test results showed that the increased heat input decreased the corrosion resistance and caused intergranular corrosion besides pitting corrosion.

36 MATERIALS SCIENCE↗

Investigation on Microstructure and Mechanical Properties of TA10–Q245R Composite Plate Formed by Explosive Welding

The titanium alloy TA10 and the carbon steel Q245R are welded by explosive welding, and post-weld heat treatment (PWHT) is carried out for the TA10–Q245R composite plate. Microstructure and mechanical properties of the composite plate are investigated both in as-welded (AW) condition and after PWHT, respectively. Results show that, in AW condition, the bonding interface of composite plate presents wavy morphology, and at both sides of the interface plastic deformation is generated to a certain degree. Near the interface interdiffusion zone of alloying elements exists, and no Fe-Ti intermetallic compound is produced at the interface. SEM images indicate that the tensile fracture of composite plate presents the characteristic of ductile fracture, and no defects such as gas pores or impurities are found on the surface of shear fracture. After PWHT, the interfacial microstructure of the composite plate is obviously changed. Compared with the mechanical properties of the composite plate in AW condition, both tensile strength and shear strength of the composite plate are decreased to a certain extent after PWHT. With various factors into consideration, the suitable heat treatment procedure of TA10–Q245R composite plate is determined as follows: 550 °C × 1.5 h.

36 MATERIALS SCIENCE↗

Influence of FSW Repairing Process on the Microstructures and Mechanical Properties of Friction Stir-Welded 6082Al Alloy

When two 42-mm 6082Al plates were welded by friction stir welding (FSW), a discontinuously distributing groove defect is formed on the surface of the joint. Subsequently, the FSW repairing process was conducted at the defect location. The influence of the repairing process on the microstructures and mechanical properties of the joints were studied, and a description of the softening mechanism of the repaired joints is provided. The results show that TMAZ at the advance side is the weakest zone of the as-welded joints. The repairing process increases the heat input into the joints and thus promotes the coarsening and transformation of the precipitates in the joints, which further weakens the repaired joints. The average tensile strength of the joints repaired with a 24-mm pin is 205 MPa, which is 91% of that of the as-welded joint. The tensile strength generally increases when the size of the repaired pin decreases. The average tensile strength of the joints repaired with an 8-mm pin is 220 MPa, which is equivalent to the initial joints.

36 MATERIALS SCIENCE↗