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At least 523 records · Page 29

Nanoscale serration characteristics of additively manufactured superalloys

Structural elements made of nickel-based superalloys usually operate at high temperatures. Many surface failure mechanisms such as creep, fatigue, fretting fatigue, corrosion, and stress corrosion cracking start from the surface. Thus, studying the surface mechanical properties and deformation behavior of materials is vital in order to draw a correlation between the surface properties and failures. Herein, a nanoindentation technique was implemented to characterize surface properties of a widely used additively manufactured (AM) superalloy, i.e., Inconel 625. The specimens were tested in a range of temperatures in a vacuum chamber. Serrated plastic flow characterized by pop-in events during nanoindentation, known as Portevin-Le Chatelier (PLC) effect, was observed in all three tested elevated temperatures. This phenomenon depicts itself as bursts of plasticity in the loading section of the load-displacement curves. These bursts were studied comprehensively to explore incipient plasticity. Hertzian contact mechanics were implemented to extract the maximum shear stress beneath the indenter from the pop-in loads. The results show that the initial pop-in load increases as the temperature increases. The average initial pop-in load increases by almost four times from 300 °C to 650 °C. This was attributed to the formation of strengthening precipitates. The average size of the serrations and the magnitude of dislocation nucleation increase from 300 °C to 500 °C and decrease from 500 °C to 650 °C. Finally, the serrations are attributed to the dislocation generation and movement as well as their interaction with the solute atoms and precipitates.

36 MATERIALS SCIENCE↗

Fatigue crack growth in 7475-T651 aluminum alloy plate in hard vacuum and water vapor

Compact specimens of 25 mm thick aluminum alloy plate were subjected to constant amplitude fatigue testing at a load ratio of 0.2. Crack growth rates were determined at frequencies of 1 Hz and 10 Hz in hard vacuum and laboratory air, and in mixtures of water vapor and nitrogen at water vapor partial pressures ranging from 94 Pa to 3.8 kPa. A significant effect of water vapor on fatigue crack growth rates was observed at the lowest water vapor pressure tested. Crack rates changed little for pressures up to 1.03 kPa, but abruptly accelerated at higher pressures. At low stress intensity factor ranges, cracking rates at the lowest and highest water vapor pressure tested were, respectively, two and five times higher than rates in vacuum. Although a frequency was observed in laboratory air, cracking rates in water vapor and vacuum are insensitive to a ten-fold change in frequency. Surfaces of specimens tested in water vapor and vacuum exhibited different amounts of residual deformation. Reduced deformation on the fracture surfaces of the specimens tested in water vapor suggests embrittlement of the plastic zone ahead of the crack tip as a result of environmental interaction.

Dicus, D. L.↗

Gas Shielding Technology for Welding and Brazing

Welding is a common method that allows two metallic materials to be joined together with high structural integrity. When joints need to be leak-tight, light-weight, or free of contaminant-trapping seams or surface asperities, welding tends to be specified. There are many welding techniques, each with its own advantages and disadvantages. Some of these techniques include Forge Welding, Gas Tungsten Arc Welding, Friction Stir Welding, and Laser Beam Welding to name a few. Whichever technique is used, the objective is a structural joint that meets the requirements of a particular component or assembly. A key practice in producing quality welds is the use of shielding gas. This article discusses various weld techniques, quality of the welds, and importance of shielding gas in each of those techniques. Metallic bonds, or joints, are produced when metals are put into intimate contact. In the solid-state "blacksmith welding" process, now called Forge Welding (FOW), the site to be joined is pounded into intimate contact. The surfaces to be joined usually need to be heated to make it easier to deform the metal. The surfaces are sprinkled with a flux to melt surface oxides and given a concave shape so that surface contamination can be squeezed out of the joint as the surfaces are pounded together; otherwise the surface contamination would be trapped in the joint and would weaken the weld. In solid-state welding processes surface oxides or other contamination are typically squeezed out of the joint in "flash."

Nunes, Arthur J.↗

Assessing mechanical response of CO 2 storage into a depleted carbonate reef using a site-scale geomechanical model calibrated with field tests and InSAR monitoring data

Geomechanical risks of injection have raised concerns regarding secure CO 2 storage. In this work, a combined monitoring and modeling approach is used to assess the stress changes and surface uplift associated with CO 2 injection into a depleted carbonate reef of the Michigan basin. A site-scale geomechanical model is built by assigning mechanical properties of formations using well-log and experimental data. Gravity load is applied to the model to estimate the vertical component of stress as well as different lateral boundary displacement scenarios to estimate horizontal stresses. We used a poroelastic pressure-dependent model (instead of a linear elastic mechanical earth model) to calibrate initial stresses using hydraulic fracture test data measured at depleted reservoir status. Multi-phase fluid flow-geomechanical simulations are performed to estimate the poroelastic response during (1) primary depletion (2) field-scale CO 2 injection phase (3) a hypothetical forecast scenario in which well bottom hole pressure (BHP) reach 45000 KPa. The predicted surface uplift is less than 1 mm at the end of the field-scale CO 2 injection phase which is in good agreement with Interferometric Synthetic Aperture Radar (InSAR) uplift measurement. Although the InSAR data shows an insignificant uplift, hydromechanical modeling of injection shows that CO 2 injection still causes reservoir deformation emphasizing the role of carbonate overburden and reservoir formation mechanical properties and limited size of reef on diminishing the surface deformation. Modeling indicates poroelastic response of caprock matters to estimate uplift. The lower permeability of the top two layers provides additional barrier to large uplift. Also, history of subsidence due to production should be accounted to predict uplift due to a follow up injection correctly. This report shows the significance of combining a calibrated geomechanical model with field measured stresses and monitoring data to be used as a tool to ensure the safety of CO 2 storage.

42 ENGINEERING↗

The Geothermal Artificial Intelligence for geothermal exploration

Exploration of geothermal resources involves analysis and management of a large number of uncertainties, which makes investment and operations decisions challenging. Remote Sensing (RS), Machine Learning (ML) and Artificial Intelligence (AI) have potential in managing the challenges of geothermal exploration. In this paper, we present a methodology that integrates RS, ML and AI to create an initial assessment of geothermal potential, by resorting to known indicators of geothermal areas namely mineral markers, surface temperature, faults and deformation. We demonstrated the implementation of the method in two sites (Brady and Desert Peak geothermal sites) that are close to each other but have different characteristics (Brady having clear surface manifestations and Desert Peak being a blind site). Here, we processed various satellite images and geospatial data for mineral markers, temperature, faults and deformation and then implemented ML methods to obtain pattern of surface manifestation of geothermal sites. We developed an AI that uses patterns from surface manifestations to predict geothermal potential of each pixel. We tested the Geothermal AI using independent data sets obtaining accuracy of 92-95%; also tested the Geothermal AI trained on one site by executing it for the other site to predict the geothermal / non-geothermal delineation, the Geothermal AI performed quite well in prediction with 72-76% accuracy.

15 GEOTHERMAL ENERGY↗

Modeling Deformable Linear Objects for Autonomous Robotic Outfitting of Lunar Surface Systems

The construction of in-space facilities is a significant capability for the establishment of a long-term human presence in space. Autonomous robotic technologies are a critical tool to enabling the construction and maintenance of such permanent facilities. This paper evaluates the outfitting portion of the construction process, focusing on modeling required for robotic manipulation of cable-like objects, referred to as Deformable Linear Objects (DLOs). DLOs contain a high degree of variability, which makes accurate real-time autonomous operations a difficult task. Different modeling methods for DLOs such as discrete mass-spring systems and Cosserat elastic rod models range in problem complexity and accuracy, a trade-off that must be understood to fully realize autonomous cable routing technologies. This paper validates different DLO models through simulation and a hardware experiment, highlighting the size of the state space and accuracy of different approaches. The development of DLO manipulation models for outfitting enables an autonomous architecture for the construction of lunar surface systems.

Deformable Modeling↗

Laser speckle strain and deformation sensor using linear array image cross-correlation method for specifically arranged triple-beam triple-camera configuration

The invention provides a method of triple-beam and triple-sensor in a laser speckle strain/deformation measurement system. The triple-beam/triple-camera configuration combined with sequential timing of laser beam shutters is capable of providing indications of surface strain and structure deformations. The strain and deformation quantities, the four variables of surface strain, in-plane displacement, out-of-plane displacement and tilt, are determined in closed form solutions.

Sarrafzadeh-Khoee, Adel K.↗

Histological preparation of developing vestibular otoconia for scanning electron microscopy

The unique nature of vestibular otoconia as calcium carbonate biominerals makes them particularly susceptible to chemical deformation during histological processing. We fixed and stored otoconia from all three otolith endorgans of embryonic, hatchling and adult Japanese quail in glutaraldehyde containing either phosphate or non-phosphate buffers for varying lengths of time and processed them for scanning electron microscopy. Otoconia from all age groups and otolith endorgans processed in 0.1 M phosphate buffer (pH 7.4) showed abnormal surface morphology when compared to acetone fixed controls. Otoconia processed in 0.1 M sodium cacodylate or HEPES buffered artificial endolymph (pH 7.4) showed normal morphology that was similar to controls. The degree of otoconial deformation was directly related to the time exposed to phosphate buffer. Short duration exposure produced particulate deformations while longer exposures resulted in fused otoconia that formed solid sheets. Otoconial surface deformation and fusing was independent of the glutaraldehyde component of the histological processing. These findings should help vestibular researchers to develop appropriate histological processing protocols in future studies of otoconia.

Non-NASA Center↗

Venus Interior Structure Mission (VISM): Establishing a Seismic Network on Venus

Magellan radar data show the surface of Venus to contain a wide range of geologic features (large volcanoes, extensive rift valleys, etc.). Although networks of interconnecting zones of deformation are identified, a system of spreading ridges and subduction zones like those that dominate the tectonic style of the Earth do not appear to be present. In addition, the absence of a mantle low-viscosity zone suggests a strong link between mantle dynamics and the surface. As a natural follow-on to the Magellan mission, establishing a network of seismometers on Venus will provide detailed quantitative information on the large scale interior structure of the planet. When analyzed in conjunction with image, gravity, and topography information, these data will aid in constraining mechanisms that drive surface deformation.

Stofan, E. R.↗

Discrete control of linear distributed systems with application to the deformable primary mirror of a large orbiting telescope

One of the more significant technological problems associated with the orbital operation of large astronomical telescope's is the fabrication and maintenance of the primary mirror surface to the tolerance required for diffraction-limited performance. An interesting approach to the solution of this problem involves continuously measuring and automatically correcting the optical surface of a thin deformable mirror by means of discrete actuators located on its rear surface: The realization of diffraction-limited performance from a telescope in space by this method rests on the ability of the designer to achieve extremely accurate control of a highly complex, interacting, multivariable system. This paper presents the results of a detailed study of the discrete control of linear distributed systems with specific application to the design of a practical controller for a plant representative of a telescope primary mirror for an orbiting astronomical observatory. The problem of controlling the distributed plant is treated by employing modal techniques to represent variations in the optical figure. Distortion of the mirror surface, which arises primarily from thermal gradients, is countered by actuators working against a backing structure to apply a corrective force distribution to the controlled surface. Each displacement actuator is in series with a spring attached to the mirror by means of a pad intentionally introduced to restrict the excitation of high-order modes. Control is then exerted over a finite number (equal.to the number of actuators) of the most significant modes. Through the application of the modal expansion technique the mirror equation of motion is transformed tb a set of uncoupled, linear, time-invariant, ordinary differential equations. The desired dynamic response and static accuracy may then be achieved by the application of classical single-variable design techniques. The formulation of a quadratic performance index which incorporates a measure of image quality permits determination of the trade-off between the-number of actuators and optical purity. A criterion for defining actuator placement and pad size is presented which minimizes the tendency of the controller to excite the unmonitored modes.

Jeremiah F Creedon↗

On the internal structure of the major satellites of the outer planets

The structures and thermal evolutions of the large icy-satellites of the outer solar system are considered. It is shown (for bodies comparable in size and mass to the Galilean satellites, having sizeable mass fraction of H2O, and with meteoritic abundances of radioactive materials contained within their silicate fractions) that the crust of solid ice over a liquid mantle predicted by conductive heat-transfer calculations is unstable to large-scale solid-state convection. For appropriate material parameters, convective heat-transfer rates are sufficient to freeze a large liquid mantle on a time scale that is short compared to the lifetime of the body. It is also concluded that the ice layer is convecting at the present time. A reevaluation of previous work, using improved values for material parameters and boundary conditions, reverses earlier conclusions and implies a rigid outer crust with resulting long-term stability of surface features to creep deformation. The combination of a rigid crust with active internal convection presents the additional possibility of surface features that are produced and maintained by dynamic internal processes.

Reynolds, R. T.↗

Erosion of iron-chromium alloys by glass particles

The material loss upon erosion was measured for several iron-chromium alloys. Two types of erodent material were used: spherical glass beads and sharp particles of crushed glass. For erosion with glass beads the erosion resistance (defined as the reciprocal of material loss rate) was linearly dependent on hardness. This is in accordance with the erosion behavior of pure metals, but contrary to the erosion behavior of alloys of constant composition that were subjected to different heat treatments. For erosion with crushed glass, however, no correlation existed between hardness and erosion resistance. Instead, the erosion resistance depended on alloy composition rather than on hardness and increased with the chromium content of the alloy. The difference in erosion behavior for the two types of erodent particles suggested that two different material removal mechanisms were involved. This was confirmed by SEM micrographs of the eroded surfaces, which showed that for erosion with glass beads the mechanism of material removal was deformation-induced flaking of surface layers, or peening, whereas for erosion with crushed glass it was cutting or chopping.

Salik, J.↗

Flow Trajectories in Friction Stir Welding

In the Friction Stir Welding (FSW) process, a rotating, shouldered tool with a threaded pin is inserted under pressure along the seam of two pieces of metal which are tightly clamped together, and secured against a rigid anvil underneath. The rotating pin travels along the seam and through a combination of pressure and friction heating produces a zone of plastic deformation around the pin within the workpiece on either side of the seam. As the pin is moved in the direction of welding, the plasticised material moves around the tool and bonds together behind it. The elements of the material flow behavior are a combination of three elements. There is a rotational transport of material being carried around the tool, extrusion of material being forced around the pin on both sides into the cavity created behind it, and a lifting and dropping of material as it is stirred and mixed by the rotating action of the pin. It was assumed that rotational motion of the plastic zone is the primary mechanism for transport of material around the welding tool. A kinematic mathematical model was used to compute trajectories of material movement for various distributions of rotational slip within the plastic zone. These trajectories were then compared with the results of an experiment that produced radiographs of markers embedded in a workpiece that was welded with the FSW process. It was assumed that the copper wire markers retained their original length as the aluminum material flowed around them. The kinematic model included a constraint so that the displacements were such that the total length of the wire markers did not increase after deformation. There was good agreement between the calculated trajectories for the case of localized slip at the outer surface of the plastic deformation zone and the radiographs of the copper wire markers. The trajectories differed markedly from the radiograph traces when a distributed slip zone was assumed. It was concluded that the flow field could be described generally by a rotating plug model with slip occurring on the surface at the outer boundary of the plastic zone.

Bernstein, Edward L.↗

Numerical benchmark of transient pressure-driven metallic melt flows

Fluid dynamics simulations of melting and crater formation at the surface of a copper cathode exposed to high plasma heat fluxes and pressure gradients are presented. The predicted deformations of the free surface and the temperature evolution inside the metal are benchmarked against previously published simulations. Despite the physical model being entirely hydrodynamic and ignoring a variety of plasma–surface interaction processes, the results are also shown to be remarkably consistent with the predictions of more advanced models, as well as experimental data. This provides a sound basis for future applications of similar models to studies of transient surface melting and droplet ejection from metallic plasma-facing components after disruptions.

36 MATERIALS SCIENCE↗

Characterization of mechanical deformation in aluminum by optical second harmonic generation

Second harmonic generation (SHG), a laser-based surface technique, was used to characterize near-surface defect evolution associated with mechanical deformation in 2024-T3 aluminum due to tensile loads. Electron backscatter diffraction (EBSD) measurements were also performed to determine the geometrically necessary dislocation density before and after tensile deformation. Comparison of the EBSD and SHG results found that dislocation density and SHG signal are inversely proportional; tensile deformation in the plastic regime led to an increase in dislocation density and a decrease in SHG response. A similar trend was seen in the SHG results on as-received (unpolished) Al samples; SHG response decreases with extent of plastic deformation. Furthermore, this study suggests that SHG has potential as a nondestructive evaluation technique.

36 MATERIALS SCIENCE↗

Plastic set of smooth large radii of curvature thermal conductance specimens at light loads

Thermal contact conductance test data at high vacuum were obtained from two Armco iron specimens having smooth, large radii of curvature, convex, one-half wave length surfaces. The data are compared with calculations based on two macroscopic elastic deformation theories and an empirical expression. Major disagreement with the theories and fair agreement with the empirical expression resulted. Plastic deformation of all the contacting surfaces was verified from surface analyzer statistics. These results indicate that the theoretical assumption of macroscopic elastic deformation is inadequate for accurate prediction of heat transfer with light loads for Armco iron specimens similar to those used in this investigation.

Mckinzie, D. J., Jr.↗

Plastic set of smooth large radii of curvature thermal conductance specimens at light loads.

Thermal contact conductance test data at high vacuum were obtained from two Armco iron specimens having smooth, large radii of curvature, convex, one-half wave length surfaces. The data are compared with calculations based on two macroscopic elastic deformation theories and an empirical expression. Major disagreement with the theories and fair agreement with the empirical expression resulted. Plastic deformation of all the contacting surfaces was verified from surface analyzer statistics. These results indicate that the theoretical assumption of macroscopic elastic deformation is inadequate for accurate prediction of heat transfer with light loads for Armco iron specimens similar to those used in this investigation.

Mckinzie, D. J., Jr.↗