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At least 523 records · Page 29

BMDO materials testing in the EOIM-3 experiment

The NASA Evaluation of Oxygen Interactions with Materials-3 (EOIM-3) experiment served as a testbed for a variety of materials that are candidates for Ballistic Missile Defense Organization (BMDO) space assets. The materials evaluated on this flight experiment were provided by BMDO contractors and technology laboratories. A parallel ground-based exposure evaluation was conducted using the Fast Atom Sample Tester (FAST) atomic-oxygen simulation facility at Physical Sciences, Inc. The EOIM-3 flight materials were exposed to an atomic oxygen fluence of approximately 2.3 x 10(exp 20) atoms/sq cm. The ground-based exposure fluence of 2.0 - 2.5 x 10(exp 20) atoms/sq cm permits direct comparison with that of the flight-exposed specimens. The results from the flight test conducted aboard STS-46 and the correlative ground-based exposure are summarized here. A more detailed correlation study is presented in the JPL Publication 93-31 entitled 'Flight-and Ground-Test Correlation Study of BMDO SDS Materials: Phase 1 Report'. In general, the majority of the materials survived the AO environment with their performance tolerances maintained for the duration of the exposure. Optical materials, baffles, and coatings performed extremely well as did most of the thermal coatings and tribological materials. A few of the candidate radiator, threat shielding, and structural materials showed significant degradation. Many of the coatings designed to protect against AO erosion of sensitive materials performed this function well.

Chung, Shirley Y.↗

Ordered mixed-layer structures in the Mighei carbonaceous chondrite matrix

High resolution transmission electron microscopy of the Mighei carbonaceous chondrite matrix has revealed the presence of a new mixed layer structure material. This mixed-layer material consists of an ordered arrangement of serpentine-type (S) and brucite-type (B) layers in the sequence SBBSBB. Electron diffraction and imaging techniques show that the basal periodicity is approximately 17 A. Discrete crystals of SBB-type material are typically curved, of small size (less than 1 micron) and show structural variations similar to the serpentine group minerals. Mixed-layer material also occurs in association with planar serpentine. Characteristics of SBB-type material are not consistent with known terrestrial mixed-layer clay minerals. Evidence for formation by a condensation event or by subsequent alteration of pre-existing material is not yet apparent.

Mackinnon, I. D. R.↗

Variable Stiffness Panel Structural Analyses With Material Nonlinearity and Correlation With Tests

Results from structural analyses of three tow-placed AS4/977-3 composite panels with both geometric and material nonlinearities are presented. Two of the panels have variable stiffness layups where the fiber orientation angle varies as a continuous function of location on the panel planform. One variable stiffness panel has overlapping tow bands of varying thickness, while the other has a theoretically uniform thickness. The third panel has a conventional uniform-thickness [plus or minus 45](sub 5s) layup with straight fibers, providing a baseline for comparing the performance of the variable stiffness panels. Parametric finite element analyses including nonlinear material shear are first compared with material characterization test results for two orthotropic layups. This nonlinear material model is incorporated into structural analysis models of the variable stiffness and baseline panels with applied end shortenings. Measured geometric imperfections and mechanical prestresses, generated by forcing the variable stiffness panels from their cured anticlastic shapes into their flatter test configurations, are also modeled. Results of these structural analyses are then compared to the measured panel structural response. Good correlation is observed between the analysis results and displacement test data throughout deep postbuckling up to global failure, suggesting that nonlinear material behavior is an important component of the actual panel structural response.

Wu, K. Chauncey↗

Ammonia formation caused by the presence of water in the wet grinding of silicon nitride powder

Si3 N4 powder (amorphous, alpha-, and beta-Si3 N4) was mixed with MeOH containing 8.87 mol. % H2O and ground. The NH3 generation rapidly increased after a grinding time of 100 hours. Silicon nitride sintered material was chosen as one of the high temperature, high strength structural materials and studies of the control of the raw material powder, preparation of the sintered body (finding the right assistant, hot press, high pressure sintering, fracture toughness and oxidation at high temperature were performed.

Kanno, Y.↗

Experimental characterization of fatigue crack tip processes

Many analytical models have been proposed to describe the physical processes attendant to a fatigue crack tip, as well as the rate at which fatigue cracks grow. By applying advanced experimental methods (such as electron channeling, stereoimaging, and in-situ cyclic loading in an SEM) to a broad range of structural materials, it has been shown that it is possible to critically assess the physical assumptions incorporated into the models. Refinements in existing models and the development of new ones have resulted. New insights into materials' behavior are providing guidelines for improving the fatigue resistance of structural alloys. In the near future, even more advanced experimental methods, such as high temperature SEM stages and small angle neutron scattering, will be available to study creep/fatigue interactions in metals and ceramics.

Lankford, J.↗

Conceptual design of a self-deployable, high performance parabolic concentrator for advanced solar-dynamic power systems

A summary is presented of the concentrator conceptual design work performed under a NASA-funded project. The design study centers around two basic efforts: conceptual design of a self-deploying, high-performance parabolic concentrator; and materials selection for a lightweight, shape-stable concentrator. The primary structural material selected for the concentrator is PEEK/carbon fiber composite. The deployment concept utilizes rigid gore-shaped reflective panels. The assembled concentrator takes a circular shape with a void in the center. The deployable solar concentrator concept is applicable to a range of solar dynamic power systems of 25 kWe to more than 75 kWe.

Dehne, Hans Joachim↗

Lunar exploration for resource utilization

The strategy for developing resources on the Moon depends on the stage of space industrialization. A case is made for first developing the resources needed to provide simple materials required in large quantities for space operations. Propellants, shielding, and structural materials fall into this category. As the enterprise grows, it will be feasible to develop additional sources - those more difficult to obtain or required in smaller quantities. Thus, the first materials processing on the Moon will probably take the abundant lunar regolith, extract from it major mineral or glass species, and do relatively simple chemical processing. We need to conduct a lunar remote sensing mission to determine the global distribution of features, geophysical properties, and composition of the Moon, information which will serve as the basis for detailed models of and engineering decisions about a lunar mine.

Duke, Michael B.↗

Evaluation of a Gamma Titanium Aluminide for Hypersonic Structural Applications

Titanium matrix composites (TMCs) have been extensively evaluated for their potential to replace conventional superalloys in high temperature structural applications, with significant weight-savings while maintaining comparable mechanical properties. New gamma titanium aluminide alloys and an appropriate fiber could offer an improved TMC for use in intermediate temperature applications (400-800 C). The purpose of this investigation is the evaluation of a gamma titanium aluminide alloy with nominal composition Ti-46.5Al-4(Cr,Nb,Ta,B)at.% as a structural material in future aerospace transportation systems, where very light-weight structures are necessary to meet the goals of advanced aerospace programs.

Johnson, W. Steven↗

Exploring the Effect of EBC Composition on CMAS Wetting Behavior

Rare-earth disilicate (REDS) materials are existing materials used in environmental barrier coating (EBC) for the protection of structural materials in the hot-section of turbine engines. REDS interactions with molten calcium-magnesium-aluminosilicate (CMAS) debris are of interest to understand molten CMAS attack and improve CMAS mitigation strategies. This work assesses the effect of REDS composition on CMAS wetting by investigating wetting angle, spreading, and reactivity. Freestanding atmospheric plasma spray (APS) REDS coatings (for RE = Y, La, Nd, Gd, Yb, Lu) were exposed to 10 mg of CMAS (Ca33-Mg9-Al13-Si45 in single cation mol%) in stagnant lab air at 1250C. APS YbDS was compared to a dense spark plasma sintered (SPS) phase-pure Yb2Si2O7 and a nominal 20 vol% phase-mixture of Yb 2 SiO 5 in Yb 2 Si 2 O 7 (20YbMS/YbDS). CMAS mass was held constant but specimen surface areas varied, yielding a range of loading between ~6 and 10 mg/cm2. CMAS was loaded as a cylindrical rod atop the specimen surface, polished to 4000 grit, and heated to temperature in a Linseis L74/HS/1700 heating microscope. The heating microscope measured the evolution of molten CMAS diameter, height, and contact angle. Molten CMAS diameter at 1150C and contact angle measurements after two hours of exposure at 1250C yielded a positive trend with rare-earth cation size. There was no statistically significant difference in CMAS wetting behavior between SPS YbDS and 20YbMS/YbDS. Post-exposure specimens were examined in plan view and cross-section with XRD, SEM, and EDS. CMAS spreading was cross-examined using plan view SEM, while reactivity utilized plan view XRD and cross-sectional SEM/EDS.

Clark Luckhardt↗

Structural concept trends for commercial supersonic cruise aircraft design

Structural concept trends for future commercial supersonic transport aircraft are considered. Highlights, including the more important design conditions and requirements, of two studies are discussed. Knowledge of these design parameters, as determined through studies involving the application of flexible mathematical models, enabled inclusion of aeroelastic considerations in the structural-material concepts evaluation. The design trends and weight data of the previous contractual study of Mach 2.7 cruise aircraft were used as the basis for incorporating advanced materials and manufacturing approaches to the airframe for reduced weight and cost. Structural studies of design concepts employing advanced aluminum alloys, advanced composites, and advanced titanium alloy and manufacturing techniques are compared for a Mach 2.0 arrow-wing configuration concept. Appraisals of the impact of these new materials and manufacturing concepts to the airframe design are shown and compared. The research and development to validate the potential sources of weight and cost reduction identified as necessary to attain a viable advanced commercial supersonic transport are discussed.

Sakat, I. F.↗

Fatigue of supersonic transport materials using simulated flight-by-flight loading

Methods to reduce the fatigue test time for structural materials which are candidates for supersonic transport airplanes were investigated by conducting real-time and accelerated fatigue tests. The tests employed sequences of stresses and temperatures to simulate the flights of a Mach 3 transport airplane. Some of the simulated flights were altered to determine the effect of the design mean stress and the number of stress cycles per flight on fatigue life. Salt solution was also applied in other tests. Notched Ti-8Al-1Mo-1V and Ti-6Al-4V were used in the investigation.

Imig, L. A.↗

Multidisciplinary Design Of Hot Composite Structures

Unified computer code developed to implement multidisciplinary approach to design and analysis of composite-material structures that must withstand high temperatures. Code modular: includes executive module communicating with and coordinating other modules performing calculations pertaining to traditionally separate disciplines like those of acoustics, structural vibrations, structural loads, and thermal effects. Essential feature, finite-element numerical simulation of relevant physical phenomena according to applicable disciplines. Same finite-element mesh used in thermal, vibrational, and structural analyses; minimizing data-preparation time and eliminating errors incurred in transforming temperatures from one finite-element mesh to another.

Chamis, Christos C.↗

Space fabrication - The key to future large space systems

Construction techniques for large space structures are discussed. It is pointed out that in contrast to assembly in orbit and the deployment technique space fabrication offers favorable densities (transporting structural materials on reels) and can be adapted to automated construction. A space fabrication machine containing reels of flat sheet material and sets of rollers or dies is described, as is a machine for fabricating composite material (which must be heated for forming and then cooled to achieve structural strength). The use of fabrication machines to build such structures as space platforms, microwave radiometers, and satellite power systems is discussed. The versatility of the machine when operated in conjunction with the Space Shuttle and a set of jigs is illustrated by showing how large square solar panels and large hexagonal structures could be constructed. The need for a flight demonstration of the fabrication machine is stressed.

Savage, M.↗

LWIR HgCdTe: Innovative detectors in an incumbent technology

HgCdTe is the current material of choice for high performance imagers operating at relatively high temperatures. Its lack of technological maturity compared with silicon and wide-band gap III-V compounds is more than offset by its outstanding IR sensitivity and by the relatively benign effect of its materials defects. This latter property has allowed non-equilibrium growth techniques, metal oxide chemical vapor deposition (MOCVD) and molecular beam epitaxy (MBE), to produce device quality long wavelength infrared (LWIR) HgCdTe even on common substrates like GaAs and GaAs/Si. Detector performance in these exotic materials structures is comparable in many ways with devices in equilibrium-grown material. Lifetimes are similar. RoA values at 77K as high as several hundred have been seen in HgCdTe/GaAs/Si with 9.5 micron cut-off wavelength. HgCdTe/GaAs layers with approx. 15 micron cut-off wavelengths have given average 77K RoAs of greater than 2. Hybrid focal plane arrays have been evaluated with excellent operability.

Tennant, William E.↗

High performance structural laminate composite material for use to 1000.degree. F. and above, apparatus for and method of manufacturing same, and articles made with same

A novel materials technology has been developed and demonstrated for providing a high modulus composite material for use to 1000.degree. F. and above. This material can be produced at 5-20% of the cost of refractory materials, and has higher structural properties. This technology successfully resolves the problem of thermal shock or ply lift, which limits traditional high temperature laminates (such as graphite/polyimide and graphite/phenolic) to temperatures of 550-650.degree. F. in thicker (0.25 and above) laminates. The technology disclosed herein is an enabling technology for the nose for the External Tank (ET) of the Space Shuttle, and has been shown to be capable of withstanding the severe environments encountered by the nose cone through wind tunnel testing, high temperature subcomponent testing, and full scale structural, dynamic, acoustic, and damage tolerance testing.

Seal, Ellis C.↗

Silicon Research and Technology Workshop report

The materials, structures, processing, modeling and measurements of high efficiency silicon solar cells were surveyed. In the materials area, highlights included: (1) the possibility of improving cell voltages by reducing minority carrier mobilities in critical regions of the solar cells; (2) the need for and possibility of lowering the surface recombination velocity for improvement of open circuit voltage in shallow junction cells; (3) the present need for improved lifetime in high resistivity cells; and (4) the potential for new materials such as polycrystalline or dendritic web material to perform well at end of life in a radiation environment. In the area of structures, distinction was made between those for terrestrial use and those that would survive radiation environments. Areas such as epitaxial growth and laser or elctron beam annealing (and diffusion) were proposed as having certain advantages over more conventional techniques.

Meulenberg, A., Jr.↗