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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 523 records · Page 29
All sourcesNASA NTRSDOE OSTI
DOE OSTI2014

Measuring contact angle and meniscus shape with a reflected laser beam

Side-view imaging of the contact angle between an extended planar solid surface and a liquid is problematic. Even when aligning the view perfectly parallel to the contact line, focusing one point of the contact line is not possible. We describe a new measurement technique for determining contact angles with the reflection of a widened laser sheet on a moving contact line. We verified this new technique measuring the contact angle on a cylinder, rotating partially immersed in a liquid. A laser sheet is inclined under an angle φ to the unperturbed liquid surface and is reflected off the meniscus. Collected on a screen, the reflection image contains information to determine the contact angle. When dividing the laser sheet into an array of laser rays by placing a mesh into the beam path, the shape of the meniscus can be reconstructed from the reflection image. We verified the method by measuring the receding contact angle versus speed for aqueous cetyltrimethyl ammonium bromide solutions on a smooth hydrophobized as well as on a rough polystyrene surface.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

Suppressing light reflection from polycrystalline silicon thin films through surface texturing and silver nanostructures

This work demonstrates a novel method combining ion implantation and silver nanostructures for suppressing light reflection from polycrystalline silicon thin films. Samples were implanted with 20-keV hydrogen ions to a dose of 10¹⁷/cm², and some of them received an additional argon ion implant to a dose of 5×10¹⁵ /cm² at an energy between 30 and 300 keV. Compared to the case with a single H implant, the processing involved both H and Ar implants and post-implantation annealing has created a much higher degree of surface texturing, leading to a more dramatic reduction of light reflection from polycrystalline Si films over a broadband range between 300 and 1200 nm, e.g., optical reflection from the air/Si interface in the AM1.5 sunlight condition decreasing from ~30% with an untextured surface to below 5% for a highly textured surface after post-implantation annealing at 1000°C. Formation of Ag nanostructures on these ion beam processed surfaces further reduces light reflection, and surface texturing is expected to have the benefit of diminishing light absorption losses within large-size (>100 nm) Ag nanoparticles, yielding an increased light trapping efficiency within Si as opposed to the case with Ag nanostructures on a smooth surface. A discussion of the effects of surface textures and Ag nanoparticles on light trapping within Si thin films is also presented with the aid of computer simulations.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Backward-propagating MeV electrons in ultra-intense laser interactions: Standing wave acceleration and coupling to the reflected laser pulse

Laser-accelerated electron beams have been created at a kHz repetition rate from the reflection of intense (∼10{sup 18 }W/cm{sup 2}), ∼40 fs laser pulses focused on a continuous water-jet in an experiment at the Air Force Research Laboratory. This paper investigates Particle-in-Cell simulations of the laser-target interaction to identify the physical mechanisms of electron acceleration in this experiment. We find that the standing-wave pattern created by the overlap of the incident and reflected laser is particularly important because this standing wave can “inject” electrons into the reflected laser pulse where the electrons are further accelerated. We identify two regimes of standing wave acceleration: a highly relativistic case (a{sub 0} ≥ 1), and a moderately relativistic case (a{sub 0} ∼ 0.5) which operates over a larger fraction of the laser period. In previous studies, other groups have investigated the highly relativistic case for its usefulness in launching electrons in the forward direction. We extend this by investigating electron acceleration in the specular (back reflection) direction and over a wide range of intensities (10{sup 17}–10{sup 19 }W cm{sup −2})

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2015

Reflection and transmission of light waves from the air-magnetoplasma interface: Spatial and angular Imbert-Fedorov shifts

We have investigated the reflection and transmission of an electromagnetic wave from the air-magnetoplasma interface. The reflection and transmission coefficients are obtained for an arbitrary polarized incident wave. The spatial and angular Imbert-Fedorov (IF) shifts are discussed. The numerical results are presented to study the dependence of the reflection and transmission coefficients and IF shifts on relevant parameters of the system. The plasma and wave parameters can be used to control the reflection coefficients and IF shifts.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2016

Beam profile and coherence properties of synchrotron beams after reflection on modified multilayer mirrors

Multilayer mirrors present an attractive alternative for reflective hard X-ray monochromators due to their increased bandwidth compared with crystal-based systems. An issue remains the strong modulations in the reflected beam profile, i.e. an irregular stripe pattern. This is a major problem for micro-imaging applications, where multilayer-based monochromators are frequently employed to deliver higher photon flux density. A subject of particular interest is how to overcome beam profile modifications, namely the stripe patterns, induced by the reflection on a multilayer. For multilayer coatings in general it is known that the substrate and its surface quality significantly influence the performance of such kind of mirrors as the coating reproduces to a certain degree roughness and shape of the substrate. Our studies have shown that modified coatings can significantly change the impact of the multilayer reflection on the beam profile. We will present recent results as well as a critical review.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2017

Analysis of an anti-reflecting nanowire transparent electrode for solar cells

Transparent electrodes are an important component in many optoelectronic devices, especially solar cells. In this study, we investigate a nanowire transparent electrode that also functions as an anti-reflection coating for silicon solar cells, taking into account the practical constraints that the electrode is typically encapsulated and needs to be in electric contact with the semiconductor. Numerical simulations show that the electrode can provide near-perfect broadband anti-reflection over much of the frequency range above the silicon band gap for both polarizations while keeping the sheet resistance sufficiently low. To provide insights into the physics mechanism of this broadband anti-reflection, we introduce a generalized Fabry–Perot model, which captures the effects of the higher order diffraction channels as well as the modification of the reflection coefficient of the interface introduced by the nanowires. This model is validated using frequency-domain electromagnetic simulations. Finally, our work here provides design guidelines for nanowire transparent electrode in a device configuration that is relevant for solar cell applications.

14 SOLAR ENERGY↗
DOE OSTI2021

Reflectivity and spectrum of relativistic flying plasma mirrors

Flying plasma mirrors induced by intense lasers via laser wake field acceleration scheme have been proposed as a promising way to generate few-cycle EUV or x-ray lasers. In addition, if such a relativistic plasma mirror can accelerate, then it would serve as an analog black hole to investigate the information loss paradox associated with the black hole Hawking evaporation. Among these applications, the reflectivity, which is usually frequency-dependent, would affect the outgoing photon spectrum and, therefore, impact on the analysis of the physics under investigation. In this paper, these two issues are investigated analytically and numerically with one-dimensional particle-in-cell simulations. Based on our simulation results, we propose a new model that provides a better estimate of the reflectivity than those studied previously. Moreover, we found that the peak frequency of the reflected spectrum of a Gaussian incident wave deviates from the expected value, 4γ 2 ω, due to the dependence of reflectivity on the frequency of the incident wave.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
DOE OSTI2013

Observation of two regions of selective light reflection from a thin film of a cholesteric liquid crystal

Two regions of selective light reflection (in the short- and long- wavelength parts of the visible spectrum) from a thin film of a cholesteric liquid crystal (CLC), consisting of the mixture of two CLCs with opposite chirality and a nematic liquid crystal, are experimentally found for the first time. The spectral position of the reflection regions and the separation between them varies depending on the CLC composition and the temperature. The long-wavelength region of reflection corresponds to the region of Bragg reflection from the CLC helix, while the short-wavelength region is probably due to the defects in the structure of the CLC film. (letters)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2017

Reflection of light beams from a chirped dielectric plane-layered structure

The reflection of light beams with various widths of the angular spectrum from a chirped plane-layered dielectric structure is numerically studied. For wide beams, the total lateral shift of the reflected beam depends on the position of the photonic barrier inside the structure and the value of the Goos – Hänchen shift. For narrow beams, the region of the interaction with the structure increases, the profile broadens and the reflected beam wavefront becomes phase modulated. It is shown that the light reflected from a quasi-periodic structure with negative spatial dispersion undergoes focusing. (light beams)

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2022

Phase tuning of multiple Andreev reflections of Dirac fermions and the Josephson supercurrent in Al–MoTe 2 –Al junctions

When an electron is incident on a superconductor from a metal, it is reflected as a hole in a process called Andreev reflection. If the metal N is sandwiched between two superconductors S in an SNS junction, multiple Andreev reflections (MARs) occur. We have found that, in SNS junctions with high transparency (τ → 1) based on the Dirac semimetal MoTe 2 , the MAR features are observed with exceptional resolution. By tuning the phase difference φ between the bracketing Al superconductors, we establish that the MARs coexist with a Josephson supercurrent I s =I A sin φ. As we vary the junction voltage V, the supercurrent amplitude I A varies in step with the MAR order n, revealing a direct relation between them. Two successive Andreev reflections serve to shuttle a Cooper pair across the junction. If the pair is shuttled coherently, it contributes to I s . The experiment measures the fraction of pairs shuttled coherently vs. V. Surprisingly, superconductivity in MoTe 2 does not affect the MAR features.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2012

SECONDARY WAVES AND/OR THE 'REFLECTION' FROM AND 'TRANSMISSION' THROUGH A CORONAL HOLE OF AN EXTREME ULTRAVIOLET WAVE ASSOCIATED WITH THE 2011 FEBRUARY 15 X2.2 FLARE OBSERVED WITH SDO/AIA AND STEREO/EUVI

For the first time, the kinematic evolution of a coronal wave over the entire solar surface is studied. Full Sun maps can be made by combining images from the Solar Terrestrial Relations Observatory satellites, Ahead and Behind, and the Solar Dynamics Observatory, thanks to the wide angular separation between them. We study the propagation of a coronal wave, also known as the 'Extreme Ultraviolet Imaging Telescope' wave, and its interaction with a coronal hole (CH) resulting in secondary waves and/or reflection and transmission. We explore the possibility of the wave obeying the law of reflection. In a detailed example, we find that a loop arcade at the CH boundary cascades and oscillates as a result of the extreme ultraviolet (EUV) wave passage and triggers a wave directed eastward that appears to have reflected. We find that the speed of this wave decelerates to an asymptotic value, which is less than half of the primary EUV wave speed. Thanks to the full Sun coverage we are able to determine that part of the primary wave is transmitted through the CH. This is the first observation of its kind. The kinematic measurements of the reflected and transmitted wave tracks are consistent with a fast-mode magnetohydrodynamic wave interpretation. Eventually, all wave tracks decelerate and disappear at a distance. A possible scenario of the whole process is that the wave is initially driven by the expanding coronal mass ejection and subsequently decouples from the driver and then propagates at the local fast-mode speed.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

CONTRIBUTION OF VELOCITY VORTICES AND FAST SHOCK REFLECTION AND REFRACTION TO THE FORMATION OF EUV WAVES IN SOLAR ERUPTIONS

We numerically study the detailed evolutionary features of the wave-like disturbance and its propagation in the eruption. This work is a follow-up to Wang et al., using significantly upgraded new simulations. We focus on the contribution of the velocity vortices and the fast shock reflection and refraction in the solar corona to the formation of the EUV waves. Following the loss of equilibrium in the coronal magnetic structure, the flux rope exhibits rapid motions and invokes the fast-mode shock at the front of the rope, which then produces a type II radio burst. The expansion of the fast shock, which is associated with outward motion, takes place in various directions, and the downward expansion shows the reflection and the refraction as a result of the non-uniform background plasma. The reflected component of the fast shock propagates upward and the refracted component propagates downward. As the refracted component reaches the boundary surface, a weak echo is excited. The Moreton wave is invoked as the fast shock touches the bottom boundary, so the Moreton wave lags the type II burst. A secondary echo occurs in the area where reflection of the fast shock encounters the slow-mode shock, and the nearby magnetic field lines are further distorted because of the interaction between the secondary echo and the velocity vortices. Our results indicate that the EUV wave may arise from various processes that are revealed in the new simulations.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2017

X-ray reflectivity measurement of interdiffusion in metallic multilayers during rapid heating

A technique for measuring interdiffusion in multilayer materials during rapid heating using X-ray reflectivity is described. In this technique the sample is bent to achieve a range of incident angles simultaneously, and the scattered intensity is recorded on a fast high-dynamic-range mixed-mode pixel array detector. Heating of the multilayer is achieved by electrical resistive heating of the silicon substrate, monitored by an infrared pyrometer. As an example, reflectivity data from Al/Ni heated at rates up to 200 K s -1 are presented. At short times the interdiffusion coefficient can be determined from the rate of decay of the reflectivity peaks, and it is shown that the activation energy for interdiffusion is consistent with a grain boundary diffusion mechanism. At longer times the simple analysis no longer applies because the evolution of the reflectivity pattern is complicated by other processes, such as nucleation and growth of intermetallic phases.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗
DOE OSTI2018

High Bragg reflectivity of diamond crystals exposed to multi-kW mm –2 X-ray beams

X-ray free-electron lasers in the oscillator configuration (XFELO) are future fully coherent hard X-rays sources with ultrahigh spectral purity. X-ray beams circulate in an XFELO optical cavity comprising diamond single crystals. They function as high-reflectance (close to 100%), narrowband (~10 meV) Bragg backscattering mirrors. The average power density of the X-ray beams in the XFELO cavity is predicted to be as high as ~10 kW mm –2 . Therefore, XFELO feasibility relies on the ability of diamond crystals to withstand such a high radiation load and preserve their high reflectivity. Here the endurance of diamond crystals to irradiation with multi-kW mm –2 power density X-ray beams is studied. It is shown that the high Bragg reflectivity of the diamond crystals is preserved after the irradiation, provided it is performed at ~1 × 10 –8 Torr high-vacuum conditions. In conclusion, irradiation under 4 × 10 –6 Torr results in a ~1 meV shift of the Bragg peak, which corresponds to a relative lattice distortion of 4 × 10 –8 , while the high Bragg reflectivity stays intact.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2017

Application of Sol-Gel Method as a Protective Layer on a Specular Reflective Surface for Secondary Reflector in a Solar Receiver

Highly-specular reflective surfaces that can withstand elevated-temperatures are desirable for many applications including reflective heat shielding in solar receivers and secondary reflectors, which can be used between primary concentrators and heat collectors. A high-efficiency, high-temperature solar receiver design based on arrays of cavities needs a highly-specular reflective surface on its front section to help sunlight penetrate into the absorber tubes for effective flux spreading. Since this application is for high-temperature solar receivers, this surface needs to be durable and to maintain its optical properties through the usable life. Degradation mechanisms associated with elevated temperatures and thermal cycling, which include cracking, delamination, corrosion/oxidation, and environmental effects, could cause the optical properties of surfaces to degrade rapidly in these conditions. Protected mirror surfaces for these applications have been tested by depositing a thin layer of SiO2 on top of electrodeposited silver by means of the sol-gel method. To obtain an effective thin film structure, this sol-gel procedure has been investigated extensively by varying process parameters that affect film porosity and thickness. Endurance tests have been performed in a furnace at 150 degrees C for thousands of hours. This paper presents the sol-gel process for intermediate-temperature specular reflective coatings and provides the long-term reliability test results of sol-gel protected silver-coated surfaces.

14 SOLAR ENERGY↗
DOE OSTI2020

Modeling thin layers of analytes on substrates for spectral analysis: use of solid/liquid n and k values to model reflectance spectra

Since solids are only sometimes seen en masse in a pure bulk form, and for liquids other than water almost never, a capability to model reflectance spectra from analytes deposited on various substrates would be highly advantageous. If available, the real, n ( ν ) , and imaginary, k ( ν ) , components of the complex refractive index, n n + i k , can be used to simulate infrared spectra, accounting for reflection, refraction, and absorption phenomena as a function of wavelength. We focus on using the Pacific Northwest National Laboratory (PNNL) derived n / k vectors for solid and liquid analytes deposited as thin layers on different types of substrates including conductors, such as aluminum, and inorganic dielectrics, such as glass. The model is an adaptation of the Monte Carlo ray trace modeling program, TracePro, extended through the use of its macrolanguage. The model is tested using thin films of organic liquids including silicone oil and no. 2 diesel fuel, as well as organic solids such as caffeine and acetaminophen on aluminum and glass. The predicted spectra for the solid films were compared to experimental hemispherical reflectance data measured using a Fourier transform spectrometer with an integrating sphere. The thickness of the calculated layer is a parameter for predicting the (transflectance) spectra and is obtained using the areal density measured from gravimetric methods to generate the thin-layer samples. Comparison of the calculated spectra with experimental hemispherical reflectance data shows excellent agreement, indicating promise for the use of measured n / k data to synthesize reference spectral data. In particular, accounting for the inhomogeneity of the deposits greatly improved the match with experimental data. Finally, the theoretical modeling shows that for thicker layers (ca. 20 to 100 μm) of typical organics possessing moderately strong k values, the longwave infrared features are often saturated and better spectral contrast is obtained from the overtone/combination bands in the shortwave infrared.

42 ENGINEERING↗
DOE OSTI2018

Reflection Spectra of Microarrays of Silicon Nanopillars

The optical-reflection spectra of microarrays of silicon nanopillars are studied in the visible and near-IR regions. The microarrays of silicon nanopillars are formed by electron-beam lithography and reactive ion etching. The reflection spectra of nanopillar arrays with pitches of 400, 600, 800, and 1000 nm are measured. The height of nanopillars in the array is 0.5 μm, and the diameter varies from 150 to 240 nm. It is noted that the spectral features of the reflection are caused by increased absorption of individual nanopillars and interference effects inside the array. A relation between the geometric parameters of nanopillars and the resonance reflection characteristics is determined taking into account the influence of the substrate.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2014

Direct observation of ballistic Andreev reflection

An overview is presented of experiments on ballistic electrical transport in inhomogeneous superconducting systems which are controlled by the process of Andreev reflection. The initial experiments based on the coexistence of a normal phase and a superconducting phase in the intermediate state led to the concept itself. It was followed by a focus on geometrically inhomogeneous systems like point contacts, which provided a very clear manifestation of the energy and direction dependence of the Andreev reflection process. The point contacts have recently evolved towards the atomic scale owing to the use of mechanical break-junctions, revealing a very detailed dependence of Andreev reflection on the macroscopic phase of the superconducting state. In present-day research, the superconducting in homogeneity is constructed by clean room technology and combines superconducting materials, for example, with low-dimensional materials and topological insulators. Alternatively, the superconductor is combined with nano-objects, such as graphene, carbon nanotubes, or semiconducting nanowires. Each of these “inhomogeneous systems” provides a very interesting range of properties, all rooted in some manifestation of Andreev reflection.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗