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NASA NTRS1998

Plasma Processing of Metallic and Semiconductor Thin Films in the Fisk Plasma Source

The use of plasmas to process materials has become widespread throughout the semiconductor industry. Plasmas are used to modify the morphology and chemistry of surfaces. We report on initial plasma processing experiments using the Fisk Plasma Source. Metallic and semiconductor thin films deposited on a silicon substrate have been exposed to argon plasmas. Results of microscopy and chemical analyses of processed materials are presented.

Lampkin, Gregory↗

NASA NTRS1998

Fabrication and Atomic Force Microscopy Characterization of Molecular Composites of Fullerenes in Aerogel Matrix for Optical Limiting

An optical limiter is a device which exhibits a decrease in the transmittance in a material with an increase in intensity of light. Sol-gel techniques offer many advantages in the fabrication of materials. These materials possess many desirable properties for nonlinear optical (NLO) device applications which include transparency, high thermal and chemical stabilities, very low refractive index and dielectric constants. C60 shows a higher excited state absorption cross section than the ground state absorption cross section over the complete visible spectrum, and the spectrum of the excited state absorption of C60 has the same general shape as the ground state absorption. This fact suggests that fullerenes are ideal optical limiting materials. Aerogels are fabricated by sol-gel processing. One of the key issues is the dispersion of fullerenes into small and uniform pores of silica aerogel host matrices. The aerogel network was characterized by Raman spectroscopy. Atomic force microscopy is a technique with many advantages to characterize the aerogel materials. The morphology of the cleaved surface for a C60/aerogel sample shows that there are long paralleled shaped stripes with 20-30 nm in width and about 500 nm in length on the cleaved surface. The cleaved surface also was etched by 5% HF solution for one minutes, and it became smoother after HF etching. The main feature in on the surface is the spherical particles with the size of few nanometers, and no aggregated fullerenes appear. The fullerenes are well dispersed in the aerogel matrices.

Lu, W. J .↗

NASA NTRS2001

The Porosity of Eros and Implications for Its Internal Structure

We estimate the porosity of Eros to be between 21-33%. Based on this porosity range and morphologic observations of the surface, we suggest that the asteroid is heavily fractured (but not a rubble pile). Additional information is contained in the original extended abstract.

Wilkison, S. L.↗

NASA NTRS2002

En Echelon Ridge and Trough Structures on Europa

Europa#s surface is tectonically and morphologically complex. Europan ridges, bands, ridged bands, double ridges, complex ridges, and troughs are collectively referred to as lineaments. Some lineaments are fault zones and exhibit sets of en echelon ridge and trough structures (EERTS). EERTS can be used to interpret the stress field in which the lineaments formed. These observations suggest that some lineaments at low latitudes initially formed as shear zones. rather than as purely tensional fractures as is commonly assumed. From stepping directions of EERTS and the offset directions of the lineaments in which they occur, we infer that some EERTS form as a result of compressional stress and others form as a result of tensional stress. EERTS that are inferred to form in compression are morphologically indistinguishable from EERTS that form in tension. The presence of tensional EERTS may support a diapiric origin for some ridges.

Michalski, Joseph R.↗

NASA NTRS2003

Pristine Presolar Silicon Carbide

In this talk we discuss a simple physical disaggregation technique coupled with an X-ray mapping procedure used to locate 81 micrometer-sized presolar SiC grains from the Murchison carbonaceous chondrite, that preserves them in their pristine state. We then describe pristine SiC surface characteristics and overall morphologies determined by high resolution field emission scanning electron microscopy (FESEM), and compare these features to those of presolar SiC grains that have been prepared using chemical dissolution techniques.

Bernatowicz, T. J.↗

NASA NTRS2002

2001 Mars Odyssey Project report

The Mars Odyssey orbiter was launched on April 7, 2001, and arrived at Mars on October 24, 2001. The orbiter carries scientific instruments that will determine surface elemental composition, mineralogy and morphology, and measure the Mars radiation environment from orbit. In addition, the orbiter will serve as a data relay for future surface missions. This paper will present an overview of the Odyssey project, including the key elements of the spacecraft design, mission design and navigation, mission operations, and the science approach. The project's risk management process will be described. Initial findings of the science team will be summarized.

Mars Odyssey↗

NASA NTRS1990

Modeling of interactions between biosphere and atmosphere on the global scale

Simulations of weather and climate with general circulation models show that the circulation and rainfall are sensitive to the transfers of radiation, sensible heat, water vapor, and momentum across the atmosphere land surface interface. Because, in nature, these transfers depend in large measure on the morphological and physiological characteristics of the surface vegetation, an interactive biosphere is needed for GCM's. The simple model of the biosphere (SiB) that the authors have constructed is based on the recognized difference between ground cover vegetation (grasses and other herbaceous plants) and canopy vegetation (trees and shrubs), where the latter act like elevated blocks of porous material which efficiently extract momentum from the air that flows through them; by a large number of multiple reflections enhance the absorption of the incident solar radiation; when the canopy is wet, act like well ventilated psychrometers which extract sensible heat from the air and produce a negative Bowen ratio; and, in all of these ways, behave differently from ground cover vegetation. The complete set of governing equations of SiB, whereby the various allowable combinations of trees, ground covers, and bare ground, in interaction with the atmosphere, determine all of the vegetation dependent transfers at the land surface, have been presented and described.

Baer, Ferdinand↗

NASA NTRS2012

The Origin of Ina: Evidence for Inflated Lava Flows on the Moon

Ina is an enigmatic volcanic feature on the Moon known for its irregularly shaped mounds, the origin of which has been debated since the Apollo Missions. Three main units are observed on the floor of the depression (2.9 km across, < or =64 m deep) located at the summit of a low-shield volcano: irregularly shaped mounds up to 20 m tall, a lower unit 1 to 5 m in relief that surrounds the mounds, and blocky material. Analyses of Lunar Reconnaissance Orbiter Camera images and topography show that features in Ina are morphologically similar to terrestrial inflated lava flows. Comparison of these unusual lunar mounds and possible terrestrial analogs leads us to hypothesize that features in Ina were formed through lava flow inflation processes. While the source of the lava remains unclear, this new model suggests that as the mounds inflated, breakouts along their margins served as sources for surface flows that created the lower morphologic unit. Over time, mass wasting of both morphologic units has exposed fresh surfaces observed in the blocky unit. Ina is different than the terrestrial analogs presented in this study in that the lunar features formed within a depression, no vent sources are observed, and no cracks are observed on the mounds. However, lava flow inflation processes explain many of the morphologic relationships observed in Ina and are proposed to be analogous with inflated lava flows on Earth.

Garry, W. B.↗

NASA NTRS1985

Fracture surface analysis in composite and titanium bonding

To understand the mechanical properties of fiber-reinforced composite materials, it is necessary to understand the mechanical properties of the matrix materials and of the reinforcing fibers. Another factor that can affect the mechanical properties of a composite material is the interaction between the fiber and the matrix. In general, composites with strong fiber matrix bonding will give higher modulus, lower toughness composites. Composites with weak bonding will have a lower modulus and more ductility. The situation becomes a bit more complex when all possibilities are examined. To be considered are the following: the properties of the surface layer on the fiber, the interactive forces between polymer and matrix, the surface roughness and porosity of the fiber, and the morphology of the matrix polymer at the fiber surface. In practice, the surface of the fibers is treated to enhance the mechanical properties of a composite. These treatments include anodization, acid etching, high temperature oxidation, and plasma oxidation, to name a few. The goal is to be able to predict the surface properties of carbon fibers treated in various ways, and then to relate surface properties to fiber matrix bonding.

Devilbiss, T. A.↗

NASA NTRS1988

Arc-textured metal surfaces for high thermal emittance space radiators

Carbon arc electrical discharges struck across the surfaces of metals such as Nb-1 percent Zr, alter the morphology to produce a high thermal emittance surface. Metal from the surface and carbon from the arc electrode vaporize during arcing, and then condense on the metal surface to produce a microscopically rough surface having a high thermal emittance. Quantitative spectral reflectance measurements from 0.33 to 15 microns were made on metal surfaces which were carbon arc treated in an inert gas environment. The resulting spectral reflectance data were then used to calculate thermal emittance as a function of temperature for various methods of arc treatment. The results of arc treatment on various metals are presented for both ac and dc arcs. Surface characterization data, including thermal emittance as a function of temperature, scanning electron microscopy, and atomic oxygen durability, are also presented. The ac arc texturing was found to increase the thermal emittance at 800 K from 0.05 to 0.70.

Banks, Bruce A.↗

NASA NTRS2004

Comparing morphologies of drainage basins on Mars and Earth using integral-geometry and neural maps

We compare morphologies of drainage basins on Mars and Earth in order to confine the formation process of Martian valley networks. Basins on both planets are computationally extracted from digital topography. Integral-geometry methods are used to represent each basin by a circularity function that encapsulates its internal structure. The shape of such a function is an indicator of the style of fluvial erosion. We use the self-organizing map technique to construct a similarity graph for all basins. The graph reveals systematic differences between morphologies of basins on the two planets. This dichotomy indicates that terrestrial and Martian surfaces were eroded differently. We argue that morphologies of Martian basins are incompatible with runoff from sustained, homogeneous rainfall. Fluvial environments compatible with observed morphologies are discussed. We also construct a similarity graph based on the comparison of basins hypsometric curves to demonstrate that hypsometry is incapable of discriminating between terrestrial and Martian basins. INDEX TERMS: 1824 Hydrology: Geomorphology (1625); 1886 Hydrology: Weathering (1625); 5415 Planetology: Solid Surface Planets: Erosion and weathering; 6225 Planetology: Solar System Objects Mars. Citation: Stepinski, T. F., and S. Coradetti (2004), Comparing morphologies of drainage basins on Mars and Earth using integral-ge

Stepinski, T. F.↗

NASA NTRS1987

Geomorphic evidence for ancient seas in west Deuteronilus Mensae, Mars-2: From very high resolution Viking Orbiter images

Very high resolution Viking Orbiter images of the Martian surface, though rare, make it possible to examine specific areas at image scales approaching those of high altitude terrestrial aerial photographs. Twenty three clear images lie within west Deuteronilus Mensae. The northernmost images which constitute an almost unbroken mosaic of the west wall of a long fingerlike canyon are examined. Morphological details on the plateau surface within zone B, not detectable at low resolution, make it possible to divide the zone into two distinct subzones separated by an east-west escarpment. The morphology of the canyon floor is described in detail.

Parker, Timothy J.↗

NASA NTRS1984

The crustal tectonics and history of Europa: A structural, morphological, and comparative analysis

An evaluation of surface features and structures on the Galilean moon Europa is made using the available high resolution Voyager imagery, low resolution support imaging, and what understanding of ice structure and mechanical behavior science has that is applicable to the problem. A general discussion of the history of Europa studies and the fundamental global morphology is undertaken. The visible lineament and terrain patterns are described, and possible origins discussed. Observations of faulting and block rotation previously described are amplified. A comparison of Europa's structures to terrestrial sea ice and lava lake crust features is also included. Finally, an attempt is made at synthesizing a unified model for the evolution of Europa's crust is presented which is compared with models developed by others.

Schenk, P. M.↗

NASA NTRS2002

Properties of M40J Carbon/PMR-II-50 Composites Fabricated with Desized and Surface Treated Fibers. Characterization of M40J Desized and Finished Fibers

To increase performance and durability of high temperature composites for potential rocket engine components, it is necessary to optimize wetting and interfacial bonding between high modulus carbon fibers and high temperature polyimide resins. It has been previously demonstrated that the electro-oxidative shear treatments used by fiber manufacturers are not effective on higher modulus fibers that have fewer edge and defect sites in the surface crystallites. In addition, sizings commercially supplied on most carbon fibers are not compatible with polyimides. This study was an extension of prior work characterizing the surface chemistry and energy of high modulus carbon fibers (M40J and M60J, Torray) with typical fluorinated polyimide resins, such as PMR-II-50. A continuous desizing system which utilizes environmentally friendly chemical- mechanical processes was developed for tow level fiber and the processes were optimized based on weight loss behavior, surface elemental composition (XPS) and morphology (FE-SEM) analyses, and residual tow strength of the fiber, and the similar approaches have been applied on carbon fabrics. Both desized and further treated with a reactive finish were investigated for the composite reinforcement. The effects of desizing and/or subsequent surface retreatment on carbon fiber on composite properties and performance including fiber-matrix interfacial mechanical properties, thermal properties and blistering onset behavior will be discussed in this presentation.

Allred, Ronald E.↗

NASA NTRS1998

Surface Chemistry, Microstructure, and Tribological Properties of Cubic Boron Nitride Films

This report deals with the surface chemistry, microstructure, bonding state, morphology, and friction and wear properties of cubic boron nitride (c-BN) films that were synthesized by magnetically enhanced plasma ion plating. Several analytical techniques - x-ray photoelectron spectroscopy, transmission electron microscopy and electron diffraction, Fourier transform infrared spectroscopy, atomic force microscopy, and surface profilometry - were used to characterize the films. Sliding friction experiments using a ball-on-disk configuration were conducted for the c-BN films in sliding contact with 440C stainless-steel balls at room temperature in ultrahigh vacuum (pressure, 10(exp -6), in ambient air, and under water lubrication. Results indicate that the boron-to-nitrogen ratio on the surface of the as-deposited c-BN film is greater than 1 and that not all the boron is present as boron nitride but a small percentage is present as an oxide. Both in air and under water lubrication, the c-BN film in sliding contact with steel showed a low wear rate, whereas a high wear rate was observed in vacuum. In air and under water lubrication, c-BN exhibited wear resistance superior to that of amorphous boron nitride, titanium nitride, and titanium carbide.

Watanabe, Shuichi↗

NASA NTRS1991

Ellipsometric study of metal samples

Exposed and unexposed (shielded) portions of the surfaces of six different metal samples (Al, Cu, Ni, Ta, W, and Zr) that had been mounted on LDEF were studied by variable angle spectroscopic ellipsometry. The change in the optical constants of the metals caused by exposure to the space environment was measured. The measured optical constants reflect changes in the morphology and stoichiometry of a surface layer to a depth of this order of magnitude. For all the samples examined in this manner the exposed and unexposed portions exhibited dramatically different optical properties. In order to determine whether the observed changes were caused by the impact of oxygen atoms encountered in flight an experiment was set up in which samples identical to the original metal samples are exposed to a low-energy oxygen plasma in a microwave discharge chamber. Results of this experiment are reported, as well as an analysis of the observed data in terms of surface layers of different composition.

Franzen, W.↗

NASA NTRS1984

A new concept for a Titan atmospheric probe

Since the Voyager 1 close-pass observations of Titan, scientific interest in the nature and composition of the atmosphere and surface of Titan has increased greatly. This enhanced interest has led to the study of mission options to the Saturnian system with a principal goal of depositing a probe into the atmosphere of Titan. Such a probe could carry instrumentation to perform in situ measurements of the structure and composition of the atmosphere and clouds and of the morphology and composition of the surface. Previous studies have examined the possibility of modifying, in a minimal way, the Galileo probe currently being prepared for an atmospheric sampling mission to Jupiter. The purpose of this paper is to report the results of a study of probe-system concepts optimized for the Titan mission. The scientific rationale for such a mission to Titan is discussed and instruments to accomplish the scientific goals are indicated. Probe systems compatible with those goals and instruments are described, and the associated development costs for each are discussed.

Swenson, B. L.↗

NASA NTRS1998

Stratospheric Sulfuric Acid and Black Carbon Aerosol Measured During POLARIS and its Role in Ozone Chemistry

Stratospheric aerosol can affect the environment in three ways. Sulfuric acid aerosol have been shown to act as sites for the reduction of reactive nitrogen and chlorine and as condensation sites to form Polar Stratospheric Clouds, under very cold conditions, which facilitate ozone depletion. Recently, modeling studies have suggested a link between BCA (Black Carbon Aerosol) and ozone chemistry. These studies suggest that HNO3, NO2, and O3 may be reduced heterogeneously on BCA particles. The ozone reaction converts ozone to oxygen molecules, while HNO3 and NO2 react to form NOx. Finally, a buildup of BCA could reduce the single-scatter albedo of aerosol below a value of 0.98, a critical value that has been postulated to change the effect of stratospheric aerosol from cooling to warming. Correlations between measured BCA amounts and aircraft usage have been reported. Attempts to link BCA to ozone chemistry and other stratospheric processes have been hindered by questions concerning the amount of BCA that exists in the stratosphere, the magnitude of reaction probabilities, and the scarcity of BCA measurements. The Ames Wire Impactors (AWI) participated in POLARIS as part of the complement of experiments on the NASA ER-2. One of our main objectives was to determine the amount of aerosol surface area, particularly BCA, available for reaction with stratospheric constituents and assess if possible, the importance of these reactions. The AWI collects aerosol and BCA particles on thin Palladium wires that are exposed to the ambient air in a controlled manner. The samples are returned to the laboratory for subsequent analysis. The product of the AWI analysis is the size, surface area, and volume distributions, morphology and elemental composition of aerosol and BCA. This paper presents results from our experiments during POLARIS and puts these measurements in the context of POLARIS and other missions in which we have participated. It describes modifications to the AWI data analysis procedures in which the collection of BCA is modeled as a fractal aggregate. The new analysis results in an increase in BCA surface area of approximately 24 and an increase in mass of 7-10 from the previous method. For the current study, BCA surface area is used in computer models that attempt to predict measured NOx/NOy ratios and O3 depletion rates. Inclusion of the HNO3 reaction with BCA in one model tends to improve the agreement of calculated to measured NOx/NOy ratio. However, it was found that these trends are viable only if the reactions are catalytic.

Strawa, Anthony W.↗