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At least 505 records · Page 28

Synthesis and characterization of electron beam irradiation-induced damage in polycrystalline metal thin films

High-energy physics research, industrial sterilizing, and material processing depend extensively on electron beam accelerators. Exit windows are crucial components of such electron accelerator systems, maintaining vacuum integrity inside the machine while providing mechanical strength, thermal stability, and radiation resistance at the beam-target interface. In this study, thin metallic films of Ni, Ti, Cr, and V were explored for use in electron beam exit windows, and their properties were compared with the properties of their bulk counterparts. Simulation results of metal foils predicted Ti to exhibit less beam power dissipation compared to Ni. However, Ni possesses superior mechanical and structural properties compared to Ti. The performance of these films under electron beam irradiation was examined by depositing thin layers of these films on silicon and metallic substrates using magnetron sputtering and exposing them to e-beam irradiation in a controlled setup. The deposited films were subjected to a dose of approximately 66 kGy at a beam energy of 10 MeV and characterized prior to and postexposure to the beam using field emission scanning electron microscopy, atomic force microscopy, x-ray diffraction (XRD), and nanoindentation. Particular emphasis was given to characteristics like the grain structure, surface morphology, dislocation density, and hardness. XRD patterns revealed irradiation-induced changes in peak intensities, while the crystallinity remained largely unchanged. Nanoindentation results showed that the pristine and irradiated Ti and Ni films were twice as hard when compared to bulk Ti and Ni samples, regardless of the substrate type used (Si or bulk Ti, or Ni). These results emphasize the superior mechanical properties of thin metal films compared to their bulk counterparts. In conclusion, this study advances the optimization of thin film materials for robust and efficient e-beam applications, ensuring improved durability and operational reliability.

AFM↗

Controlled semiconductor quantum dot fabrication utilizing focus ion beam

In this project, we experimented the focused ion beam (FIB) based fabrications of semiconductor quantum dots (QDs) by using metal nano particles (NPs) (e.g., Al) on semiconductor as a template and by means of the FIB induced direct metal-to-QD conversion. We have examined effect of the experimental conditions, including Ga + ion energy and dose as well as substrate temperature. The results of experiments have shown AlGaSb QD formation on GaSb substrate can be achieved under certain conditions but there are many challenges about the techniques, including compositional nonuniformity of the QDs formed, partial conversion of the metal NP to QD, and high defect concentration in the QDs.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Dynamics and control of orbiting grid and the synchronously deployable beam

The dynamic analysis of a grid structure hung from the ceiling by two steel wires is described. The method of approach uses the discrete mass model system. The concept of the bifilar pendulum is used in writing the equation of motion. Assumptions are made with regard to the bar stiffnesses in the vertical and horizontal planes. The discrete mases are assumed to be connected by inextensible massless strings that do not provide any torsion or bending. The modal frequencies obtained by this method are compared with those obtained from the finite element model.

Abu-Saba, E. G.↗

The Potential of Phased Arrays for Planetary Exploration

Phased array antennas provide a set of operational capabilities which are very attractive for certain mission applications and not very attractive for others. Such antennas are by no means a panacea for telecommunications. In this paper the features of phased arrays are reviewed and their implications for space missions are considered in terms of benefits and costs. The primary capability provided by a phased array is electronic beam agility. The beam direction may be controlled at electronic speeds (vs. mechanical actuation) permitting time division multiplexing of multiple "users." Moreover, the beam direction can be varied over a full hemisphere (for a planar array). On the other hand, such antennas are typically much more complicated than the more commonly used reflectors and horns and this implies higher cost. In some applications, this increased cost must be accepted if the mission is to be carried out at all. The SIR-C radar is an example of such a case albeit not for deep space. Assuming for the sake of argument that the complexity and cost of a phased array can be significantly reduced, where can such antennas be of value in the future of planetary exploration? Potential applications to be discussed are planetary rovers, landers, and orbiters including both the areosynchronous and low orbit varieties. In addition, consideration is given to links from deep space to earth. As may be fairly obvious, the deep space link to earth would not benefit from the wide angle steering capability provided by a phase array whereas a rover could gain advantage from the capability to steer a beam anywhere in the sky. In the rover case, however, physical size of the aperture becomes a significant factor which, of course, has implications regarding the choice of frequency band. Recent research work concerning phased arrays has suggested that future phased arrays might be made less complex and, therefore, less costly. Successful realization of such phased arrays would enable many of the planetary missions discussed in this paper and significantly broaden the telecommunications capabilities available to the mission designers of the future.

Pogorzelski, Ronald J.↗

Ionization-Based Optical Structures for the Control of Short-Pulse Lasers (Full LDRD Report)

High-power lasers require enormous beam sizes to avoid optics damage; without plasma control of light, future higher-power systems will have prohibitive costs. The laser-induced formation of ionization patterns in gases provides an opportunity to manipulate the spatial and temporal properties of femtosecond to picosecond beams with precise control at high intensity, providing a path towards compact multi-petawatt lasers. In this project, we proposed new concepts of diffractive optics elements relying on ionization-based structures, including a holographic lens and a compression grating. The theoretical characterization of these optical elements was supported by particle-in-cell simulations. Experiments have been carried out to achieve reflective elements (i.e., plasma-based gratings) that demonstrated high robustness and efficiencies on the order of 50%, which validates the feasibility of our new concepts and paves the way for future plasma-based high-power laser systems.

47 OTHER INSTRUMENTATION↗

Load balancing for multi-beam additive manufacturing systems

As powder bed fusion (PBF) additive manufacturing (AM) becomes a more mature field, system configurations are gradually moving away from the classic single heat source, layer-by-layer system configurations towards unconventional system configurations that offer higher throughput. Higher throughput systems allow PBF systems to be considered for a larger variety of industrial applications. However, the inclusion of multiple heat sources, or beams, also increases the complexity of the control schemes needed. For multi-beam systems with overlapping fields of view, the distribution of workload, or load balancing, across these beams directly affects the total print time for a build. Additionally, the probability of any beam failing in a multi-beam system increases with the number of beams. While manual methods of load balancing and dealing with beam failures are reasonable for current generation multi-beam systems, as system configurations become more complex, manual methods will become prohibitively inefficient. Here, this paper introduces two different ways to load balance multi-beam systems of various configuration types, regardless of their complexity, which are highly performant. A consequence of this performance is the enablement of on-the-fly load balancing in the event a beam fails, thus improving system robustness.

36 MATERIALS SCIENCE↗

Selecting 1D projections for 2D tomography reconstruction

Previous works on reconstructing the 4D phase space using tomography require optimal selection of projection views to achieve accurate reconstruction. In 2D reconstruction, the process is straightforward, as an object can be evenly sampled by dividing the angles evenly. However, extending this concept from 2D to 4D is not intuitive. This work demonstrates that quaternions can be used to more effectively describe views in 4D and introduces the Fibonacci Flower algorithm and repulsive force algorithm to evenly space views in 4D space in order to achieve higher reconstruction accuracy.

Accelerator Physics↗

Covert laser remote sensing and vibrometry

Designs of single-beam laser vibrometry systems and methods. For example, a method for detecting vibrations of a target based on optical sensing is provided to include operating a laser to produce a laser probe beam at a laser frequency and modulated at a modulation frequency onto a target; collecting light at or near the laser to collect light from the target while the target is being illuminated by the laser probe beam through an optical receiver aperture; using a narrow-band optical filter centered at the laser frequency to filter light collected from the optical receiver aperture to transmit light at the laser frequency while blocking light at other frequencies; using an optical detector to convert filtered light from the narrow-band optical filter to produce a receiver electrical signal; using a lock-in amplifier to detect and amplify the receiver electrical signal at the modulation frequency while rejecting signal components at other frequencies to produce an amplified receiver electrical signal; processing the amplified receiver electrical signal to extract information on vibrations of the target carried by reflected laser probe beam in the collected light; and controlling optical power of the laser probe beam at the target to follow optical power of background illumination at the target.

Maleki, Lutfollah↗

SPS phase control system performance via analytical simulation

A solar power satellite transmission system which incorporates automatic beam forming, steering, and phase control is discussed. The phase control concept centers around the notation of an active retrodirective phased array as a means of pointing the beam to the appropriate spot on Earth. The transmitting antenna (spacetenna) directs the high power beam so that it focuses on the ground-based receiving antenna (rectenna). A combination of analysis and computerized simulation was conducted to determine the far field performance of the reference distribution system, and the beam forming and microwave power generating systems.

Lindsey, W. C.↗

Electron-Beam-Related Studies of Halide Perovskites: Challenges and Opportunities

Electron beam microscopy and related characterization techniques play an important role in revealing the microstructural, morphological, physical, and chemical information of halide perovskites and their impact on associated optoelectronic devices. However, electron beam irradiation usually causes damage to these beam-sensitive materials, negatively impacting their device performance, and complicating this interpretation. Here, the electron microscopy and spectroscopy techniques are reviewed that are crucial for the understanding of the crystallization and microstructure of halide perovskites. In addition, special attention is paid to assessing and mitigating the electron beam-induced damage caused by these techniques. Since the halide perovskites are fragile, a protocol involving delicate control of both electron beam dose and dose rate, coupled with careful data analysis, is key to enable the acquisition of reliable structural and compositional information such as atomic-resolution images, chemical elemental mapping and electron diffraction patterns. Limiting the electron beam dose is critical parameter enabling the characterization of various halide perovskites. Novel methods to unveil the mechanisms of device operation, including charge carrier generation, diffusion, and extraction are presented in scanning electron microscopy studies combined with electron-beam-induced current and cathodoluminescence mapping. Future opportunities for electron-beam-related characterizations of halide perovskites are also discussed.

36 MATERIALS SCIENCE↗

A critical look at the prediction of the temperature field around a laser-induced melt pool on metallic substrates

The study of microstructure evolution in additive manufacturing of metals would be aided by knowing the thermal history. Since temperature measurements beneath the surface are difficult, estimates are obtained from computational thermo-mechanical models calibrated against traces left in the sample revealed after etching, such as the trace of the melt pool boundary. Here we examine the question of how reliable thermal histories computed from a model that reproduces the melt pool trace are. To this end, we perform experiments in which one of two different laser beams moves with constant velocity and power over a substrate of 17-4PH SS or Ti-6Al-4V, with low enough power to avoid generating a keyhole. We find that thermal histories appear to be reliably computed provided that (a) the power density distribution of the laser beam over the substrate is well characterized, and (b) convective heat transport effects are accounted for. Poor control of the laser beam leads to potentially multiple three-dimensional melt pool shapes compatible with the melt pool trace, and therefore to multiple potential thermal histories. Ignoring convective effects leads to results that are inconsistent with experiments, even for the mild melt pools here.

42 ENGINEERING↗

Numerical and experimental evaluation for single-axis control of an LSS laboratory model

One of the major problems of LSS attitude control design stems from the modeling uncertainties due to modal truncation errors and modal parameter estimation errors. This modeling problem is investigated by evaluating poles and zeros of the frequency response functions, described in terms of constrained or unconstrained modes. The frequency domain approach is utilized to evaluated the results of modal analyses and direct output feedback controller experiments using a simple flexible spacecraft model consisting of a rigid primary body and flexible aluminum beam(s) with a control moment gyro as an actuator. The modal data are compared under the conditions that the model is constrained as the canti-lever and it is rotationally free on a single-axis air bearing table. In addition, the open-loop responses are experimentally examined under the impulsive disturbance to the appendage. The results of the control experiments show that the first vibration mode of the appendage and the interacted rotational motion of the primary body are damped in a short time as predicted by the numerical analysis, to produce damping ratio of 10-20%.

Ohkami, Y.↗

Generation of structured coherent extreme ultraviolet beams from an MgO crystal

Short wavelength high-harmonic sources are undergoing intense development for applications in spectroscopy and microscopy. Despite recent progress in peak and average power, spatial control over coherent extreme ultraviolet (XUV) beams remains a formidable challenge due to the lack of suitable optical elements for beam shaping and control. In this work, we demonstrate a robust and precise approach that structures XUV high-order harmonics in space as they are emitted from a nanostructured MgO crystal. Our demonstration paves the way for bridging the numerous applications of shaped light beams from the visible to the short wavelengths, with potential uses for applications in microscopy and nanoscale machining.

36 MATERIALS SCIENCE↗

Acoustic processing method for MS/MS experiments

Acoustical methods in which intense sound beams can be used to control the position of objects are considered. The position control arises from the radiation force experienced when a body is placed in a sound field. A description of the special properties of intense sound fields useful for position control is followed by a discussion of the more obvious methods of position, namely the use of multiple sound beams. A new type of acoustic position control device is reported that has advantages of simplicity and reliability and utilizes only a single sound beam. Finally a description is given of an experimental single beam levitator, and the results obtained in a number of key levitation experiments.

Whymark, R. R.↗

Physical conditions for conducting radiobiological experiments in beams of accelerated particles with high linear energy transfer

The design and construction of an accelerator to conduct radiobiological experiments is reported that uses aluminum filters to control the accelerated ion beam while preserving its stability, and a vacuum chamber to conduct the ion beam with the help of a collector through a lavsan exit port to the target. Depth distribution of the absorbed dose from a monodirectional ion beam is practically completely represented by the change in the energy spectrum of the biological object.

Kudryashov, Y. I.↗

Portable Electron-Beam Free-Form Fabrication System

A portable electron-beam free-form fabrication (EB F3) system, now undergoing development, is intended to afford a capability for manufacturing metal parts in nearly net sizes and shapes. Although the development effort is oriented toward the eventual use of systems like this one to supply spare metal parts aboard spacecraft in flight, the basic system design could also be adapted to terrestrial applications in which there are requirements to supply spare parts on demand at locations remote from warehouses and conventional manufacturing facilities. Prior systems that have been considered for satisfying the same requirements (including prior free-form fabrication systems) are not easily portable because of their bulk and massive size. The mechanical properties of the components that such systems produce are often inferior to the mechanical properties of the corresponding original, conventionally fabricated components. In addition, the prior systems are not efficient in the utilization of energy and of feedstock. In contrast, the present developmental system is designed to be sufficiently compact and lightweight to be easily portable, to utilize both energy and material more efficiently, and to produce components that have mechanical properties approximating those of the corresponding original components. The developmental EB F3 system will include a vacuum chamber and associated vacuum pumps, an electron-beam gun and an associated power supply, a multiaxis positioning subsystem, a precise wire feeder, and an instrumentation system for monitoring and control. The electron-beam gun, positioning subsystem, and wire feeder will be located inside the vacuum chamber (see figure). The electron beam gun and the wire feeder will be mounted in fixed positions inside the domed upper portion of the vacuum chamber. The positioning subsystem and ports for the vacuum pumps will be located on a base that could be dropped down to provide full access to the interior of the chamber when not under vacuum. During operation, wire will be fed to a fixed location, entering the melted pool created by the electron beam. Heated by the electron beam, the wire will melt and fuse to either the substrate or with the previously deposited metal wire fused on top of the positioning table. Based on a computer aided design (CAD) model and controlled by a computer, the positioning subsystem

Watson, J. Kevin↗

Structural control research and experiments at NASA/LaRC

The advances made in the area of structural dynamics and control using the flexible beam facility at the NASA Langley Research Center are surveyed. Spectral attention is given to the progress in adaptive control and reliability improvements using advanced control concepts. Both theoretical and experimental results are given to delineate the nature of the work being undertaken. With regard to adaptive control, emphasis is placed on parameter and system identification and on comparisons between competing on-line algorithms. In addition, results are presented for on-line modal control laws that are interfaced to a parameter identification scheme. This gives an on-line distributed adaptive control system. With regard to reliability, a design process is outlined that incorporates reliability over the design mission life.

Montgomery, R. C.↗