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DOE OSTI2026

Alkali-Metal Interlocking of 2D V 4 O 10 Sheets Defines Discretized Interlayer Shear Relationships

Low-dimensional materials manifest structural anisotropy, quantum confinement, and tightly bound excitonic states, which make them attractive building blocks that can be assembled within three-dimensional laterally stitched heterostructures, stacked van der Waals solids, and complex moiré superlattices. Ion intercalation in the galleries between layered materials provides a means of modifying interlayer separation and coupling, but it is also known to drive the shearing of the layers. In this article, we explore the distinct ligand coordination environments afforded by vanadyl oxygens of singular [V 4 O 10 ] sheets and examine how the size, polarizability, and stoichiometry of Group I cations sandwiched between such layers determine the interlocking of the sheets in stacked structures. Based on the topochemical insertion of alkali-metal ions into the layered λ-V 2 O 5 , we identify seven types of guest ion coordination sites discretized into four distinct regimes of interlayer shear in units of half octahedral widths. The coordination preferences of intercalated cations govern how they interlock 2D [V 4 O 10 ] sheets and engender specific shear conformations. We present evidence that static and dynamic disorder in guest ion arrangement modulate the magnetic structure of the intercalated compounds based on electrostatic polarization, localization of charge and spin density, and lattice distortion. The results illustrate the use of topochemical ion insertion to modulate stacking relationships and magnetic transition characteristics.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Europa modifies Jupiter’s 1 plasma sheet

Jupiter's plasma sheet has been understood to be primarily composed of Io-genic sulfur and oxygen, along with protons at lower mass density. These ions move radially away from Jupiter, filling its magnetosphere. The material in the plasma sheet interacts with Europa, which is also a source of magnetospheric pickup ions, primarily hydrogen and oxygen. Juno's thermal plasma instrument JADE, the Jovian Auroral Distributions Experiment, has provided comprehensive in situ observations of the composition of Jupiter's plasma sheet ions with its Time-of-Flight mass-spectrometry capabilities. Here, we present observations of the magnetospheric composition in the Europa-Ganymede region of Jupiter's magnetosphere. We find material from Europa is intermittently present at comparable densities to Io-genic plasma. The intermittency of Europa-genic signatures suggests Europa's neutral oxygen toroidal cloud is more localized to Europa's vicinity than its hydrogen cloud. These observations reveal a more complex and compositionally diverse magnetosphere than previously thought.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2025

Emulation With Uncertainty Quantification of Regional Sea‐Level Change Caused by the Antarctic Ice Sheet

Abstract Projecting regional sea‐level change under various climate‐change scenarios typically involves running forward simulations of the Earth's gravitational, rotational and deformational (GRD) response to ice‐mass change, which requires substantial computational cost if applied to probabilistic frameworks requiring thousands to millions of samples. Here we build emulators of regional sea‐level change at 27 coastal locations, due to the GRD effects associated with future Antarctic Ice Sheet mass change over the 21st century. The emulators are evaluated against a numerical sea‐level model applied to an ensemble of ice‐sheet model simulations of the Antarctic Ice Sheet through 2100. We build a physics‐based emulator using a recent sensitivity kernel approach and compare it to machine learning based emulators (neural network and conditional variational autoencoder methods). In order to quantify uncertainty, we derive well‐calibrated prediction intervals for regional sea‐level change via split‐conformal inference and linear regression, and show that Monte Carlo dropout does not yield well‐calibrated uncertainties in this instance. We also demonstrate substantial gains in computational efficiency using both the physics‐based emulator and neural networks in comparison to the numerical model for the complete regional sea‐level solution. Overall, we find the physics‐based emulator modestly outperforms the machine learning emulators for this problem.

58 GEOSCIENCES↗

DOE OSTI2025

Ultrathin liquid sheets: water gets in shape for VUV absorption

We present absorption spectra of thin, free-flowing liquid sheets in the vacuum ultraviolet energy range using a gas-squeezed liquid jet. Compared to liquid flow cells, operation without transmission windows eliminates restrictions on the energy range. The temperature of the water sheet is estimated at 0 ± 3 °C, at the verge of the supercooled regime. By adjusting flow conditions in situ, we recorded absorption spectra at water sheet thicknesses ranging from 20 to 50 nm. We show that the absorption spectra of thin jets contain significant contributions from interference effects that need to be deconvoluted from spectral contributions due to the electronic structure. We employ a Fresnel propagation model to model the spectral changes and understand the impact of thickness variations and thin film interference. This opens the door for the investigation of solvation, interface, and similar effects by recording valence band spectra.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Vortex-sheet modeling of hydrodynamic instabilities produced by an oblique shock interacting with a perturbed interface in the HED regime

In this work, we consider hydrodynamic instabilities produced by the interaction of an oblique shock with a perturbed material interface under high-energy-density (HED) conditions. During this interaction, a baroclinic torque is generated along the interface due to the misalignment between the density and pressure gradients, thus leading to perturbation growth. Our objective is to understand the competition between the impulsive acceleration due to the normal component of the shock velocity, which drives the Richtmyer–Meshkov instability, and the shear flow across the interface due to the tangential component of the shock velocity, which drives the Kelvin–Helmholtz instability, as well as its relation to perturbation growth. Since the vorticity resulting from the shock-interface interaction is confined to the interface, we describe the perturbation growth using a two-dimensional vortex-sheet model. We demonstrate the ability of the vortex-sheet model to reproduce roll-up dynamics for non-zero Atwood numbers by comparing to past laser-driven HED experiments. We determine the dependence of the interface dynamics on the tilt angle and propose a time scaling for the perturbation growth at early time. Eventually, this scaling will serve as a platform for the design of future experiments. This study is the first attempt to incorporate into a vortex-sheet model the time-dependent interface decompression and the deceleration (as well as the corresponding Rayleigh–Taylor instability) arising from laser turn-off.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2025

Replenishing liquid sheet targets to enable high-intensity high-repetition-rate laser–plasma interactions for ion-beam technology

We report on the development of a robust microfluidic nozzle capable of generating replenishing liquid sheet targets with sub-micron thickness at up to kHz repetition rates, a λ/20 surface flatness over areas of at least 100 μm 2 , and in-vacuum dimensions of 6 × 1.5 mm 2 . The platform was evaluated for stability under hundreds of 4.3 J laser shots at 0.5 Hz and 6 × 10 20 W/cm 2 peak intensity, delivered in burst mode, totaling 2.9 kJ on the target. The key metrics of the platform, including sheet characteristics, nozzle aperture morphology, and proton spectra, showed no measurable degradation in the performance of the liquid sheet platform following this experiment. Beyond its application to ion beam technology, we outline a pathway to further develop the capabilities of the platform into a high-repetition-rate plasma mirror.

depth profiling techniques↗

DOE OSTI2020

Elimination of MHD current sheets by modifications to the plasma wall in a fixed boundary model

Models of magnetohydrodynamic (MHD) equilibia that for computational convenience assume the existence of a system of nested magnetic flux surfaces tend to exhibit singular current sheets. These sheets are located on resonant flux surfaces that are associated with rational values of the rotational transform. We study the possibility of eliminating these singularities by suitable modifications of the plasma boundary, which we prescribe in a fixed boundary setting. We find that relatively straightforward iterative procedures can be used to eliminate weak current sheets that are generated at resonant flux surfaces by the nonlinear interactions of resonating wall harmonics. These types of procedures may prove useful in the design of fusion devices with configurations that enjoy improved stability and transport properties.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

The maximum extent of the filaments and sheets in the cosmic web: an analysis of the SDSS DR17

Filaments and sheets are striking visual patterns in cosmic web. The maximum extent of these large-scale structures are difficult to determine due to their structural variety and complexity. We construct a volume-limited sample of galaxies in a cubic region from the SDSS, divide it into smaller subcubes and shuffle them around. We quantify the average filamentarity and planarity in the 3D galaxy distribution as a function of the density threshold and compare them with those from the shuffled realizations of the original data. The analysis is repeated for different shuffling lengths by varying the size of the subcubes. The average filamentarity and planarity in the shuffled data show a significant reduction when the shuffling scales are smaller than the maximum size of the genuine filaments and sheets. We observe a statistically significant reduction in these statistical measures even at a shuffling scale of $\sim 130 \, {{\, \rm Mpc}}$, indicating that the filaments and sheets in three dimensions can extend up to this length scale. They may extend to somewhat larger length scales that are missed by our analysis due to the limited size of the SDSS data cube. We expect to determine these length scales by applying this method to deeper and larger surveys in future.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2023

3D-printed sheet jet for stable megahertz liquid sample delivery at X-ray free-electron lasers

X-ray free-electron lasers (XFELs) can probe chemical and biological reactions as they unfold with unprecedented spatial and temporal resolution. A principal challenge in this pursuit involves the delivery of samples to the X-ray interaction point in such a way that produces data of the highest possible quality and with maximal efficiency. This is hampered by intrinsic constraints posed by the light source and operation within a beamline environment. For liquid samples, the solution typically involves some form of high-speed liquid jet, capable of keeping up with the rate of X-ray pulses. However, conventional jets are not ideal because of radiation-induced explosions of the jet, as well as their cylindrical geometry combined with the X-ray pointing instability of many beamlines which causes the interaction volume to differ for every pulse. This complicates data analysis and contributes to measurement errors. An alternative geometry is a liquid sheet jet which, with its constant thickness over large areas, eliminates the problems related to X-ray pointing. Since liquid sheets can be made very thin, the radiation-induced explosion is reduced, boosting their stability. These are especially attractive for experiments which benefit from small interaction volumes such as fluctuation X-ray scattering and several types of spectroscopy. Although their use has increased for soft X-ray applications in recent years, there has not yet been wide-scale adoption at XFELs. Here, gas-accelerated liquid sheet jet sample injection is demonstrated at the European XFEL SPB/SFX nano focus beamline. Its performance relative to a conventional liquid jet is evaluated and superior performance across several key factors has been found. This includes a thickness profile ranging from hundreds of nanometres to 60 nm, a fourfold increase in background stability and favorable radiation-induced explosion dynamics at high repetition rates up to 1.13 MHz. Its minute thickness also suggests that ultrafast single-particle solution scattering is a possibility.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2023

Statistical Generation of Ocean Forcing With Spatiotemporal Variability for Ice Sheet Models

Melting of ice at the base of floating ice shelves that fringe the Antarctic ice sheet has been identified as a significant source of uncertainty in sea level rise projections. Part of this uncertainty derives from chaotic internal variability of the coupled ocean-atmosphere system. For numerical ice sheet model projections, this uncertainty has not previously been quantified because of the prohibitive computational expense of running large climate model ensembles. Here, we develop and demonstrate a technique that generates independent realizations of internal climate variability from a single climate model simulation. Building on previous developments in model emulation, this technique uses empirical orthogonal function decomposition and Fourier-phase randomization to generate statistically consistent realizations of spatiotemporal variability fields for the target climate variable. The method facilitates efficient sampling of a wide range of climate trajectories, which can also be incorporated within ice sheet or other physical models to represent feedback processes.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2022

A detection of the sea level fingerprint of Greenland Ice Sheet melt

Rapid melting of ice sheets and glaciers drives a unique geometry, or fingerprint, of sea level change. However, the detection of individual fingerprints has been challenging because of sparse observations at high latitudes and the difficulty of disentangling ocean dynamic variability from the signal. Here we predict the fingerprint of Greenland Ice Sheet (GrIS) melt using recent ice mass loss estimates from radar altimetry data and model reconstructions of nearby glaciers and compare this prediction to an independent, altimetry-derived sea surface height trend corrected for ocean dynamic variability in the region adjacent to the ice sheet. A statistically significant correlation between the two fields (P < 0.001) provides an unambiguous observational detection of the near-field sea level fingerprint of recent GrIS melting in our warming world.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2020

Towards the Commercialization of the All-Solid-State Li-ion Battery: Local Bonding Structure and the Reversibility of Sheet-Style Si-PAN Anodes

A slurry-coated sheet-style Si-based anode is developed for use in all-solid-state Li-ion batteries. Inexpensive, mixed-conducting polyacrylonitrile (PAN) is utilized as both binder and conductive additive, enabling Si-rich electrodes (70 wt%) to attain large reversible capacities ~1,500 mAh g-1 (Si) at 1 C rates (>3 mA cm -2 ). Cross sectional analysis of a discharged all-solid-state half-cell indicates that the Si-PAN anode achieves the largest volumetric specific capacity ever reported for a Li-ion electrode (>1500 mAh cm -3 ). Ex situ Raman spectroscopic studies reveal that the anodes' reversibility is attributed to the preservation of small tetrahedrally coordinated clusters within their Si nanoparticles upon discharge. We therefore argue that careful lithiation limitations should be implemented in all Si-based Li-ion anodes to preserve this local tetrahedral atomic structure. Furthermore, the slurry-coated sheet-style Si-PAN anodes have been successfully cycled in all-solid-state full-cells against high-voltage nickel-rich NMC 811 composite cathodes to encourage future commercialization of similar sheet-style all-solid-state designs.

25 ENERGY STORAGE↗

DOE OSTI2021

AA 7075 Sheet with 700 MPa Strength for Automotive Structural Components: CRADA 520 [Abstract only]

Fairmount Technologies is developing a new metal forming machine intended to produce ultra-high strength Aluminum Alloy AA 7075 sheets and is seeking to collaborate with PNNL to optimize the production process, as well as the strength and formability of the sheet produced. Results will be used to infer (and optionally demonstrate) whether aluminum components such as side-impact beams can be successfully formed from this sheet.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Europa Modifies Jupiter's Plasma Sheet

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Cross-flow separation characteristics and piloting of graphene oxide nanofiltration membrane sheets and tubes for kraft black liquor concentration

Dewatering of weak black liquor (WBL) in the kraft cycle by evaporation is highly energy intensive. Membranes are an attractive alternative for energy-efficient dewatering, but existing commercial polymeric or ceramic membranes are either degraded in BL or have high capital costs. Our recent works have demonstrated the engineering of graphene oxide (GO) nanofiltration membranes, their stability and promising performance in BL conditions, and preliminary scale-up into sheets and tubes. Here, we describe in detail the separation characteristics of GO membrane sheets and tubes under real BL conditions and crossflow operation. Recycle-mode piloting of a GO tubular membrane showed average “production flux” of 16 L/m2/h (LMH) and high rejections of lignin (98.3%), total solids (66%), and total organic carbon (83%), with no signs of irreversible fouling identified. A corresponding GO sheet membrane produced an average flux of ~25 LMH and maintained high lignin rejection of ~97% during a slipstream pilot at a kraft mill site using WBL with ~16 wt% total solids (TS). Finally, we piloted a Dow/DuPont XUS1808 polyamide composite reverse osmosis (RO) membrane for last-mile processing of the GO nanofiltration membrane permeate. The RO membrane showed a steady state flux of 19 LMH at 65 bar and produced ~0.02 wt% TS water product, which is highly suitable for reuse in pulp washing operations in the kraft process. The results have strong positive implications for the industrial application of GO membranes in BL concentration and other related applications.

Materials Science↗

DOE OSTI2024

Current Sheet Alignment in Oblique Black Hole Magnetospheres: A Black Hole Pulsar?

Abstract We study the magnetospheric evolution of a nonaccreting spinning black hole (BH) with an initially inclined split monopole magnetic field by means of 3D general relativistic magnetohydrodynamic simulations. This serves as a model for a neutron star (NS) collapse or a BH–NS merger remnant after the inherited magnetosphere has settled into a split monopole field creating a striped wind. We show that the initially inclined split monopolar current sheet aligns over time with the BH equatorial plane. The inclination angle evolves exponentially toward alignment, with an alignment timescale that is inversely proportional to the square of the BH angular velocity, where higher spin results in faster alignment. Furthermore, magnetic reconnection in the current sheet leads to exponential decay of event-horizon-penetrating magnetic flux with nearly the same timescale for all considered BH spins. In addition, we present relations for the BH mass and spin in terms of the period and alignment timescale of the striped wind. The explored scenario of a rotating, aligning, and reconnecting current sheet can potentially lead to multimessenger electromagnetic counterparts to a gravitational-wave event due to the acceleration of particles powering high-energy radiation, plasmoid mergers resulting in coherent radio signals, and pulsating emission due to the initial misalignment of the BH magnetosphere.

Astronomy & Astrophysics↗

NASA NTRS1972

Hot press and roll welding of titanium-6-percent-aluminum-4-percent-vanadium bar and sheet with auto-vacuum cleaning

Hot press butt welds were made in 0.5 in. diameter bar, and roll lap welds were made in 0.060 in. thick sheet of Ti-6A1-4V. For hot press welds made after auto-vacuum cleaning at 1800 F for 2 hours, weld strength and ductility equaled the parent metal properties. Only 5 minutes of pressing time were needed at 1800 F and 200 psi to make the hot press welds. Roll welds were made in sheet at 1750 F with only 10 percent deformation. The welds in the bar and sheet were metallurgically indistinguishable from the parent material.

Holko, K. H.↗

NASA NTRS1972

Internal structure of the geomagnetic neutral sheet.

A study of the internal structure of the neutral sheet in the geomagnetic tail has been made from data obtained by the NASA-GSFC magnetic-field experiment on the Explorer 34 spacecraft during its tail passage in the first half of 1968. The data used in the analysis are individual measurements of the vector magnetic field at 2.56-sec intervals. The experimental results consist of statistical studies of relevant properties of the magnetic field as a function of field magnitude. The results do not support nearly one-dimensional field models with characteristic lengths for field variation parallel to the neutral sheet much larger than the neutral-sheet width. The principal conclusion from the data points toward consistency with a quasi-periodic (possibly turbulent) structure with a tendency to formation of magnetic loops as one might expect from stability studies.

Schindler, K.↗