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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 505 records · Page 28
All sourcesNASA NTRSDOE OSTI
DOE OSTI2026

Fast and bright scintillators for ultrafast materials dynamics using 4th generation synchrotron

We present recent advances in fast and bright scintillators for ultrafast X-ray phase contrast imaging of dynamic materials experiments at the upgraded Advanced Photon Source (APS-U), a fourth generation synchrotron. APS-U enables hard X-ray imaging at frame rates of at least 13 MHz (corresponding to 77 ns or shorter interframe intervals), creating a new need for scintillators with faster response and higher light output than lutetium yttrium oxyorthosilicate (LYSO). For indirect imaging and diffraction with ultrafast cameras, commercial lanthanum bromide (LaBr3) and cerium bromide (CeBr3) are promising candidates. These materials exhibit decay times approximately a factor of two shorter than LYSO (around 40 ns) and lutetium oxyorthosilicate (LSO), while maintaining comparable light yield per incident X-ray photon. However, their implementation at APS-U requires addressing several challenges, including material limitations due to hygroscopicity, efficient optical coupling to imaging systems, and high quantum efficiency for conversion of scintillation light, predominantly at wavelengths below 400 nm, into detectable electronic signals. We report results from material characterization, detector integration and packaging, and beamline experiments of materials with impact. In addition, emerging scintillator classes, including perovskites and high-entropy materials, are discussed as potential alternatives for next-generation ultrafast X-ray diagnostics.

Wang, Zhehui [Los Alamos] (ORCID:0000000178264063)↗
DOE OSTI2022

Moderate spectral resolution solar irradiance measurements, aerosol optical depth, and solar transmission, from 360 to 1070 nm, using the refurbished rotating shadow band spectroradiometer (RSS)

Abstract. This paper reports on a third-generation rotating shadow band spectroradiometer (RSS) used to measure global and diffuse horizontal plus direct normal irradiances and transmissions at 1002 wavelengths between 360 and 1070 nm. The prism-dispersed spectral data are from the Atmospheric Radiation Measurement (ARM) Southern Great Plains site in north-central Oklahoma (36.605∘ N, 97.486∘ W) and cover dates between August 2009 and February 2014. The refurbished RSS isolates the detector in a vacuum chamber with pressures near 10−7 torr. This prevents the deposition of outgassed vapors from the interior of the spectrometer shell on the cooled detector that affected the operation of the first commercial RSS. Methods for (1) ensuring the correct wavelength registration of the data and (2) deriving extraterrestrial responses over the entire spectrum, including throughout strong water vapor and oxygen bands, are described. The resulting data produced are archived as ARM data records and include cloud-screened aerosol optical depths, spectral irradiances and direct normal solar transmission, as well as normalized diffuse and global irradiances.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2023

Freeform three-mirror anastigmatic large-aperture telescope and receiver optics for CMB-S4

CMB-S4, the next-generation ground-based cosmic microwave background (CMB) observatory, will provide detailed maps of the CMB at millimeter wavelengths to dramatically advance our understanding of the origin and evolution of the universe. CMB-S4 will deploy large and small aperture telescopes with hundreds of thousands of detectors to observe the CMB at arcminute and degree resolutions at millimeter wavelengths. Inflationary science benefits from a deep delensing survey at arcminute resolutions capable of observing a large field of view at millimeter wavelengths. This kind of survey acts as a complement to a degree angular resolution survey. The delensing survey requires a nearly uniform distribution of cameras per frequency band across the focal plane. We present a large-throughput, large-aperture (5-meter diameter) freeform three-mirror anastigmatic telescope and an array of 85 cameras for CMB observations at arcminute resolutions, which meets the needs of the delensing survey of CMB-S4. A detailed prescription of this three-mirror telescope and cameras is provided, with a series of numerical calculations that indicate expected optical performance and mechanical tolerance.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

Structural and physical properties of two distinct 2D lead halides with intercalated Cu( II )

Transition metal cation intercalation between the layers of two-dimensional (2D) metal halides is an underexplored research area. In this work we focus on the synthesis and physical property characterizations of two layered hybrid lead halides: a new compound [Cu(O 2 C–CH 2 –NH 2 ) 2 ]Pb 2 Br 4 and the previously reported [Cu(O 2 C–(CH 2 ) 3 –NH 3 ) 2 ]PbBr 4 . These compounds exhibit 2D layered crystal structures with incorporated Cu 2+ between the metal halide layers, which is achieved by combining Cu(II) and lead bromide with suitable amino acid precursors. The resultant [Cu(O 2 C–(CH 2 ) 3 –NH 3 ) 2 ]PbBr 4 adopts a 2D layered perovskite structure, whereas the new compound [Cu(O 2 C–CH 2 –NH 2 ) 2 ]Pb 2 Br 4 crystallizes with a new structure type based on edge-sharing dodecahedral PbBr5O3 building blocks. [Cu(O 2 C–CH 2 –NH 2 ) 2 ]Pb 2 Br 4 is a semiconductor with a bandgap of 3.25 eV. It shows anisotropic charge transport properties with a semiconductor resistivity of 1.44 × 10 10 Ω cm (measured along the a-axis) and 2.17 × 10 10 Ω cm (along the bc-plane), respectively. The fabricated prototype detector based on this material showed response to soft low-energy X-rays at 8 keV with a detector sensitivity of 1462.7 μCGy –1 cm –2 , indicating its potential application for ionizing radiation detection. Finally, these encouraging results are discussed together with the results from density functional theory calculations, optical, magnetic, and thermal property characterization experiments.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Correcting thermal-emission-induced detector saturation in infrared spectroscopy

We found that temperature-dependent infrared spectroscopy measurements (i.e., reflectance or transmittance) using a Fourier-transform spectrometer can have substantial errors, especially for elevated sample temperatures and collection using an objective lens. These errors can arise as a result of partial detector saturation due to thermal emission from the measured sample reaching the detector, resulting in nonphysical apparent reduction of reflectance or transmittance with increasing sample temperature. Here, we demonstrate that these temperature-dependent errors can be corrected by implementing several levels of optical attenuation that enable convergence testing of the measured reflectance or transmittance as the thermal-emission signal is reduced, or by applying correction factors that can be inferred by looking at the spectral regions where the sample is not expected to have a substantial temperature dependence.

47 OTHER INSTRUMENTATION↗
DOE OSTI2021

Core–Shell Gold Nanoparticle-Star Copolymer Composites with Gradient Transfer and Transport Properties: Toward Electro-Optical Sensors and Catalysis

A series of hybrid core–shell nanomaterials was prepared by solvent phase transfer methods with gold (Au) nanoparticles (NPs) as a core and star copolymers (h-PEI-b-PCL-Cbz) as a shell—consisting of hyperbranched polyethyleneimine (h-PEI) with different poly(ε-caprolactone) (PCL) chain lengths and a carbazole-contained terminating agent (Cbz). By varying the PCL chain length, these core–shell nanomaterials exhibited gradient energy transfer properties, surface hydrophobicity, electropolymerizability, and ionic probe transport and diffusion properties. The systematic copolymer formation was verified with quadruple-detector size exclusion chromatography (SEC) and 1H nuclear magnetic resonance (NMR). High-resolution atomic force microscopy-infrared spectroscopy (AFM-IR) chemical mapping verified nanoparticle-substrate adhesion and film formation. The design of these hybrid NPs and elucidation of gradient properties will be useful for future applications of the core–shell systems in electro-optical sensing and catalysis.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Measurement of the total cross section and $\rho$-parameter from elastic scattering in pp collisions at $\sqrt{s}=13$ TeV with the ATLAS detector

In a special run of the LHC with β* = 2.5 km, proton–proton elastic-scattering events were recorded at $\sqrt{s}=13$ TeV with an integrated luminosity of $340$ μb -1 using the ALFA subdetector of ATLAS in 2016. The elastic cross section was measured differentially in the Mandelstam t variable in the range from - t = 2.5 · 10 -4 GeV 2 to - t = 0.46 GeV 2 using 6.9 million elastic-scattering candidates. This paper presents measurements of the total cross section σ tot , parameters of the nuclear slope, and the p -parameter defined as the ratio of the real part to the imaginary part of the elastic-scattering amplitude in the limit t → 0. These parameters are determined from a fit to the differential elastic cross section using the optical theorem and different parameterizations of the t-dependence. The results for σ tot and p are σ tot (pp → X) = 104.7 ± 1.1 mb, p = 0.098 ± 0.011. The uncertainty in σ tot is dominated by the luminosity measurement, and in p by imperfect knowledge of the detector alignment and by modelling of the nuclear amplitude.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2021

Determination of X-ray detection limit and applications in perovskite X-ray detectors

X-ray detection limit and sensitivity are important figure of merits for perovskite X-ray detectors, but literatures lack a valid mathematic expression for determining the lower limit of detection for a perovskite X-ray detector. In this work, we present a thorough analysis and new method for X-ray detection limit determination based on a statistical model that correlates the dark current and the X-ray induced photocurrent with the detection limit. The detection limit can be calculated through the measurement of dark current and sensitivity with an easy-to-follow practice. Alternatively, the detection limit may also be obtained by the measurement of dark current and photocurrent when repeatedly lowering the X-ray dose rate. While the material quality is critical, we show that the device architecture and working mode also have a significant influence on the sensitivity and the detection limit. Our work establishes a fair comparison metrics for material and detector development.

47 OTHER INSTRUMENTATION↗
DOE OSTI2024

Optimizing the spatial resolution and gamma discrimination of SiPM-based Anger cameras

SiPM Anger cameras have been designed for use as 2-dimensional thermal neutron detectors for scientific applications such as at single crystal diffraction instruments. These cameras utilize a neutron sensitive scintillator and an array of SiPM photosensors, separated by a light spreading glass. While this optics package is very effective at detecting and positioning neutrons, it is also sensitive to gamma rays, which are a source of unwanted noise. In this work, we underwent a search of scintillator and spreader glass thicknesses to determine the optimal combination for maximizing spatial resolution. Both experimental results and GEANT4 simulations are presented. Further, to address the issue of gamma ray detection, we have also designed and presented a multi-layer scintillator that reduces the amount of scintillation light produced via gamma-ray energy deposition, allowing for easier pulse-height discrimination. A sample of this geometry has been produced that results in a factor of 2 improvement over an equivalent thickness monolithic scintillator.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2021

The multi-optics high-resolution absorption x-ray spectrometer (HiRAXS) for studies of materials under extreme conditions

We report the development of a high-resolution spectrometer for extended x-ray absorption fine structure (EXAFS) studies of materials under extreme conditions. A curved crystal and detector in the spectrometer are replaceable such that a single body is employed to perform EXAFS measurements at different x-ray energy intervals of interest. Two configurations have been implemented using toroidal crystals with Ge 311 reflection set to provide EXAFS at the Cu K-edge (energy range 8.9–9.8 keV) and Ge 400 reflection set to provide EXAFS at the Ta L3-edge (9.8–10.7 keV). Key performance characteristics of the spectrometer were found to be consistent with design parameters. The data generated at the National Ignition Facility have shown an ≃3 eV spectral resolution for the Cu K-edge configuration and ≃6 eV for the Ta L3-edge configuration.

Stoupin, S. (ORCID:0000000226225270)↗
DOE OSTI2022

SPT-3G+: mapping the high-frequency cosmic microwave background using kinetic inductance detectors

We present the design and science goals of SPT-3G+, a new camera for the South Pole Telescope, which will consist of a dense array of 34100 kinetic inductance detectors measuring the cosmic microwave background (CMB) at 220, 285 and 345 GHz. The SPT-3G+ dataset will enable new constraints on the process of reionization, including measurements of the patchy kinematic Sunyaev-Zeldovich effect and improved constraints on the optical depth due to reionization. At the same time, it will serve as a pathfinder for the detection of Rayleigh scattering, which could allow future CMB surveys to constrain cosmological parameters better than from the primary CMB alone. In addition, the combined, multi-band SPT-3G and SPT-3G+ survey data, will have several synergies that enhance the original SPT-3G survey, including: extending the redshift-reach of SZ cluster surveys to z > 2; understanding the relationship between magnetic fields and star formation in our Galaxy; improved characterization of the impact of dust on inflationary B-mode searches; and characterizing astrophysical transients at the boundary between mm and sub-mm wavelengths. Finally, the modular design of the SPT-3G+ camera allows it to serve as an on-sky demonstrator for new detector technologies employing microwave readout, such as the on-chip spectrometers that we expect to deploy during the SPT-3G+ survey. In this paper, we describe the science goals of the project and the key technology developments that enable its powerful yet compact design.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2024

Characterization of the response of radiochromic film to quasi-monoenergetic x rays through a cross-calibration with image plates

Radiochromic film (RCF) and image plates (IPs) are both commonly used detectors in diagnostics fielded at inertial confinement fusion (ICF) and high-energy-density physics (HEDP) research facilities. Due to the intense x-ray background in all ICF/HEDP experiments, accurately calibrating the optical density of RCF as a function of x-ray dose, and the photostimulated luminescence per photon of IPs as a function of x-ray energy, is necessary for interpreting experimental results. Various measurements of the sensitivity curve of different IPs to x rays have been performed [Izumi et al., Proc. SPIE 8850, 885006 (2013) and Rosenberg et al., Rev. Sci. Instrum. 90(1), 013506 (2019)]; however, calibrating RCF is a tedious process that depends on factors such as the orientation in which the RCF is scanned in the film scanner and the batch of RCF used. These issues can be mitigated by cross-calibrating RCF with IPs to enable the use of IPs for the determination of dose on the RCF without scanning the RCF. Here, the first cross-calibration of RCF with IPs to quasi-monoenergetic titanium, copper, and molybdenum K-line x rays is presented. It is found that the IP-inferred dose rates on the RCF for the Ti and Mo x rays agree well with the measured dose rates, while the IP-inferred dose rate for the Cu x rays is larger than the measured dose rate by ∼2×. Explanations for this discrepancy and plans for future work are discussed.

Instruments & Instrumentation↗
DOE OSTI2023

A sub-picosecond digital clock monitoring system

We describe a low-cost system designed to monitor wander in digital clocks with a precision of ≤ 1 ps. With this system we have shown that it is possible to track phase variations at the sub-picosecond level by adding noise to a reference clock. As in many cases where a clock is part of a complex distribution network small changes in temperature and other effects can lead to small changes in the clock's phase. As a further demonstration of the system, we have used it to measure the phase changes induced in optical signals in fibers.

47 OTHER INSTRUMENTATION↗
DOE OSTI2023

Resonator-based ion-selective sensor

The present disclosure relates to systems and methods suitable to measure trace amounts of specific ions in fluid samples. An example system includes a resonator having an input coupler and an output coupler. The example system also includes an ion-selective membrane (ISM) optically coupled to at least a portion of the resonator. The system additionally includes a light source configured to illuminate the resonator by way of the input coupler. Furthermore, the system includes a detector configured to receive output light by way of the output coupler and provide information indicative a concentration of a specific ion proximate to tire ISM.

Zhang, Xufeng↗
DOE OSTI2023

Microscale device and method for purification of radiopharmaceuticals

A microfluidic chip device for the purification of radiochemical compounds includes a chip having an injection channel and intersecting branch channels with a plurality of valves are located along the injection channel and branch channels and configured to retain a plug of solution containing the radiochemical compound. The chip further includes a serpentine channel segment (for separation) coupled to the output of the injection channel. A high voltage power source advances the plug of solution through the purification region and into the downstream fraction collection channel. The chip includes a downstream fraction collection channel coupled to the serpentine channel segment and having an optical and radiation detection regions. One or more branch fraction channels intersect with the fraction collection channel and include valves located therein so that the radiochemical compound that is detected using a radiation detector is directed into the desired branch fraction channel for subsequent use.

Van Dam, R. Michael↗
DOE OSTI2026

Physics potential of the IceCube Upgrade for atmospheric neutrino oscillations

The IceCube Upgrade is an extension of the existing IceCube Neutrino Observatory and will be deployed in the 2025–2026 austral summer. It will significantly improve the sensitivity of the detector to atmospheric neutrino oscillations. The existing 86-string IceCube array contains a dense in-fill known as DeepCore which is optimized to measure neutrinos with energies down to a few GeV. The IceCube Upgrade will consist of seven new densely instrumented strings placed within the DeepCore volume to further enhance the performance in the GeV energy range. The additional strings will feature new optical modules, each containing multiple photomultiplier tubes (PMTs), in contrast to the existing modules that each contain a single PMT. This will more than triple the number of PMT channels with respect to the current IceCube configuration, allowing for improved detection efficiency and reconstruction performance at GeV energies. We describe necessary updates to simulation, event selection, and reconstruction to accommodate the higher data rates observed by the upgraded detector and the addition of multi-PMT modules. We determine the expected sensitivity of the IceCube Upgrade to the atmospheric neutrino oscillation parameters sin 2 ⁡𝜃 23 and Δ⁢𝑚$^{2}_{32}$, the appearance of tau neutrinos and the neutrino mass ordering. The IceCube Upgrade will provide neutrino oscillation measurements that are of similar precision to those from accelerator experiments, while providing complementarity by probing higher energies and longer baselines, and with different sources of systematic uncertainties.

artificial neural networks↗
DOE OSTI2024

Sensitive proton-radiation detectors

In this study, halide perovskite nanocrystal scintillators detect high-energy protons with sensitivity suitable for clinical applications.

36 MATERIALS SCIENCE↗
DOE OSTI2022

Method and apparatus for measuring optical pulses

A pulse analysis system or method includes a frequency filter that receives an ultrafast pulse under test and disperses the pulse under test over a frequency range. The frequency filter separates the pulse under test into component frequency slices and provides the frequency slices to a detector coupled to a digitizer, which processes the digitized signal and collects a sonogram characteristic of the pulse under test. The frequency slices are arranged to overlap. Ptychography is performed on the sonogram to obtain characteristics of the pulse under test.

Kane, Daniel J.↗