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Mass spectra of alkyl carbamates derived from primary, secondary, and teriary alcohols by use of deuterium labeling and high resolution mass spectroscopy
Apollo 12 lunar rock 12013, discussing major and trace elemental abundances determination by neutron activation analysis
Lunar soil samples 12001,1, 12037, 12042,25 and 12070,100 exterior morphology and chemistry, noting environmental temperature decrease, crater formation and meteorite impact
Dimensional analysis techniques are described and applied to the containment/deflection problem of bursting high-rpm rotating parts of turbojet engines. The use of dimensional analysis to select a feasible set of experiments and to determine the important parameters to be varied is presented. The determination of a containment coefficient based on the nondimensionalized parameters is developed for the reduction of experimental data and as an assist to designers of containment/deflection devices.
By use of rational approximation, a procedure was found which allows calculation of the z-transfer function from a restricted number of time sequence values. The order of the system need not be known. Transformation to the s-domain is easily provided.
Assumed-displacement versions of the finite-element method are developed to predict large-deformation elastic-plastic transient deformations of structures. Both the conventional and a new improved finite-element variational formulation are derived. These formulations are then developed in detail for straight-beam and curved-beam elements undergoing (1) Bernoulli-Euler-Kirchhoff or (2) Timoshenko deformation behavior, in one plane. For each of these categories, several types of assumed-displacement finite elements are developed, and transient response predictions are compared with available exact solutions for small-deflection, linear-elastic transient responses. The present finite-element predictions for large-deflection elastic-plastic transient responses are evaluated via several beam and ring examples for which experimental measurements of transient strains and large transient deformations and independent finite-difference predictions are available.
The mass spectra of twenty alkyl carbamates derived from primary, secondary, and tertiary alcohols are investigated, using deuterium labeling and high-resolution mass spectrometry. Several of the primary and secondary alcohol derivatives are found to yield an ion formally equivalent to the product ion of a McLafferty rearrangement. Deuterium labeling, however, revealed a lack, in these carbamate derivatives, of the usual site specificity associated with the McLafferty rearrangement. A double hydrogen rearrangement process was observed in the mass spectra of several carbamates derived from tertiary alcohols.
Petrological, mineralogical, and chemical investigations of the B-1 Luna 16 sample have revealed that the sample is a fine-grained ophitic basalt which is distinguished from the Apollo samples by containing a single pyroxene, an ilmenite content intermediate to that of the Apollo samples, and subequal amounts of pyroxene and plagioclase. It is also distinguished by a high Sr content and a high K/U value.
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Mathematical optimization of containment/deflection system would save time, effort, and material as well as afford designer greater opportunity to investigate new ideas and variety of materials.
An experiment investigating direct nuclear pumping of a gas laser using argon as lasing medium is described. Results show that light output in the form of a directional beam was obtained.
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