Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “Ceramic materials”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 505 records · Page 28

Grinding Si3N4 Powder In Si3N4 Equipment

Three methods of grinding compared. Report based on study of grinding silicon nitride powder in preparation for sintering into solid ceramic material. Attrition, vibratory, and ball mills lined with reaction-bonded silicon nitride tested. Rates of reduction of particle sizes and changes in chemical compositions of powders measured so grinding efficiences and increases in impurity contents from wear of mills and media evaluated for each technique.

Herbell, Thomas P.↗

Sensors for ceramic components in advanced propulsion systems: Summary of literature survey and concept analysis, task 3 report

The results of a literature survey and concept analysis related to sensing techniques for measuring of surface temperature, strain, and heat flux for (non-specific) ceramic materials exposed to elevated temperatures (to 2200 K) are summarized. Concepts capable of functioning in a gas turbine hot section environment are favored but others are reviewed also. Recommendation are made for sensor development in each of the three areas.

Bennethum, W. H.↗

Rapid fabrication of lightweight ceramic mirrors via chemical vapor deposition

Lightweight Si/SiC mirrors of nominal diameter 7.5 cm have been fabricated via a scalable and rapid CVD process to demonstrate the CVD mirror fabrication technology. These mirrors consist of a faceplate of either Si or Si-coated SiC and a lightweight backstructure made of either Si or SiC. The mirrors were polished to a figure better than 1/5th of a wave at 0.6328 A and a finish of better than 10 A rms. A procedure for fabricating these mirrors is described. The CVD fabrication process is fast and has the potential to yield several mirrors in a few weeks time from a single reactor. The CVD mirror fabrication technology is quite general and can be extended to include mirrors of other ceramic materials such as TiB2 and B4C.

Goela, Jitendra S.↗

Friction And Wear Of Silicon Ceramics

Report presents results of experimental study of friction and wear in unlubricated sliding of silicon-based ceramics on Inconel(R) 718 nickel-based alloy. Both monolithic and fiber-reinforced ceramics tested at temperatures from 25 to 800 degrees C. Evaluates ceramic materials for potential use as cylinder liners, piston caps, and other engine parts subjected to sliding or rubbing.

Deadmore, Daniel L.↗

Temperature Rises In Pumps For Superfluid Helium

Report discusses increases in temperature of superfluid helium in centrifugal and fountain-effect pumps. Intended for use in transfers of superfluid helium in outer space. Increases in temperature significantly affect losses during transfers and are important in selection of temperatures of supply tanks. Purpose of study, increase in temperature in fountain-effect pump calculated on basis of thermodynamic considerations, starting from assumption of ideal pump. Results of recent tests of ceramic material intended for use in such pumps support this assumption. Overall, centrifugal pumps more effective because it produces smaller rise in temperature.

Kittel, Peter↗

Plasma-deposited amorphous hydrogenated carbon films and their tribological properties

Recent work on the properties of diamondlike carbon films and their dependence on preparation conditions are reviewed. The results of the study indicate that plasma deposition enables one to deposit a variety of amorphous hydrogenated carbon (a-C:H ) films exhibiting more diamondlike behavior to more graphitic behavior. The plasma-deposited a-C:H can be effectively used as hard, wear-resistant, and protective lubricating films on ceramic materials such as Si(sub 3)N(sub 4) under a variety of environmental conditions such as moist air, dry nitrogrn, and vacuum.

Miyoshi, Kazuhisa↗

Thermal/structural analyses of several hydrogen-cooled leading-edge concepts for hypersonic flight vehicles

The aerodynamic heating at high flight Mach numbers, when shock interference heating is included, can be extremely high and can exceed the capability of most conventional metallic and potential ceramic materials available. Numerical analyses of the heat transfer and thermal stresses are performed on three actively cooled leading-edge geometries (models) made of three different materials to address the issue of survivability in a hostile environment. These analyses show a mixture of results from one configuration to the next. Results for each configuration are presented and discussed. Combinations of enhanced internal film coefficients and high material thermal conductivity of copper and tungsten are predicted to maintain the maximum wall temperature for each concept within acceptable operating limits. The exception is the TD nickel material which is predicted to melt for most cases. The wide range of internal impingement film coefficients (based on correlations) for these conditions can lead to a significant uncertainty in expected leading-edge wall temperatures. The equivalent plastic strain, inherent in each configuration which results from the high thermal gradients, indicates a need for further cyclic analysis to determine component life.

Gladden, Herbert J.↗

Fracture toughness and crack growth of Zerodur

The fracture toughness and crack growth parameters of Zerodur, a low expansion glass ceramic material, were determined. The fracture toughness was determined using indentation techniques and was found to be 0.9 MPa x m(sup 1/2). The crack growth parameters were determined using indented biaxial specimens subjected to static and dynamic loading in an aqueous environment. The crack growth parameters n and 1n(B) were found to be 30.7 and -6.837, respectively. The crack growth parameters were also determined using indented biaxial specimens subjected to dynamic loading in an ambient 50 percent relative humidity environment. The crack growth parameters n and 1n(B) at 50 percent relative humidity were found to be 59.3 and -17.51, respectively.

Viens, Michael J.↗

Thermal/structural analyses of several hydrogen-cooled leading-edge concepts for hypersonic flight vehicles

The aerodynamic heating at high flight Mach numbers, when shock interference heating is included, can be extremely high and can exceed the capability of most conventional metallic and potential ceramic materials available. Numerical analyses of the heat transfer and thermal stresses are performed on three actively cooled leading-edge geometries (models) made of three different materials to address the issue of survivability in a hostile environment. These analyses show a mixture of results from one configuration to the next. Results for each configuration are presented and discussed. Combinations of enhanced internal film coefficients and high material thermal conductivity of copper and tungsten are predicted to maintain the maximum wall temperature for each concept within acceptable operating limits. The exception is the TD nickel material which is predicted to melt for most cases. The wide range of internal impingement film coefficients (based on correlations) for these conditions can lead to a significant uncertainty in expected leading-edge wall temperatures. The equivalent plastic strain, inherent in each configuration which results from the high thermal gradients, indicates a need for further cyclic analysis to determine component life.

Gladden, Herbert J.↗

Plasma-deposited amorphous hydrogenated carbon films and their tribological properties

Recent work on the properties of diamondlike carbon films and their dependence on preparation conditions are reviewed. The results of the study indicate that plasma deposition enables one to deposit a variety of amorphous hydrogenated carbon (a-C:H) films exhibiting more diamondlike behavior to more graphitic behavior. The plasma-deposited a-C:H can be effectively used as hard, wear-resistant, and protective lubricating films on ceramic materials such as Si(sub 3)N(sub 4) under a variety of environmental conditions such as moist air, dry nitrogen, and vacuum.

Miyoshi, K.↗

Making Three-Layer Solid Electrolyte/Electrode Sandwiches

Tape-casting-and-sintering process joins two ceramic materials having widely different sintering temperatures into integral sandwich structure. Layers retain their identities, without migration of constituents. Used to make three-layer structure composed of outer porous layers of strontium-doped lanthanum manganite and inner dense layer of yttria-stabilized zirconia. Structures used to make electrolytic and fuels cells with solid electrolytes for use at high temperatures. Other potential applications include oxygen pumps and oxygen sensors.

Schroeder, James E.↗

Survey of results from the Boeing modules on the M0003 experiment on LDEF

The Boeing modules on the M0003 experiment included fiber optics, ceramic materials, a variety of electronic piece parts, composites and thermal control paints, fasteners, thin film lubricants, anodized surfaces, and adhesives. These materials were flown on the leading and trailing edge exteriors, and on the interior portion of LDEF M0003 providing exposure under three distinct environments. The condition of each of these material types is described. Results of optical, surface, and mechanical properties are presented.

Pippin, H. Gary↗

Effect of thermal cycling on stress in metallic films on ceramic substrates

The hydrogen maser is the most stable frequency standard currently available for averaging intervals of hours to weeks. A major contributor to maser frequency variations is the maser's microwave resonant cavity: by means of the cavity pulling effect, a change in the cavity's resonance frequency produces a proportional change in the maser's output frequency. To minimize variations in the cavity's dimensions, and thus in its resonance frequency, maser cavities are often constructed of a low-expansivity glass-ceramic material coated on its surface with a conductive metallic film. It was previously shown that silver films like those used in SAO maser cavities develop tensile stress when cooled to room temperature after being fired onto the cavity, and that the stress in such films relaxes with time at a rate proportional to the level of stress. Stress relaxation in maser cavity coatings can alter the shape, and hence the resonance frequency, of the cavity, resulting in a slow variation in the maser's output frequency. The possibility was investigated of reversing the initial tensile stress by precooling the coated cavity material. It was hypothesized that cooling the material well below its normal working temperature and then warming it to its normal temperature would result in a lower tensile stress or even a compressive stress. Under such a condition stress relaxation, and thus any consequent frequency drifts, might be reduced or reversed.

Mattison, Edward M.↗

Steric stabilization of nonaqueous silicon slips. I - Control of particle agglomeration and packing. II - Pressure casting of powder compacts

The application of steric stabilization to control particle agglomeration and packing of silicon powder in benzene and trichloroethylene is reported. The results provide useful guidelines for controlling unfavorable particle-particle interactions during nonaqueous processing of silicon-based ceramic materials. The application of steric stabilization to the control and improvement of green processing of nonaqueous silicon slips in pressure consolidation is also demonstrated.

Kerkar, Awdhoot V.↗

Scanning electron acoustic microscopy of indentation-induced cracks and residual stresses in ceramics

The ability of scanning electron acoustic microscopy (SEAM) to characterize ceramic materials is assessed. SEAM images of Vickers indentations in SiC whisker-reinforced alumina clearly reveal not only the radial cracks, the length of which can be used to estimate the fracture toughness of the material, but also reveal strong contrast, interpreted as arising from the combined effects of lateral cracks and the residual stress field left in the SiC whisker-reinforced alumina by the indenter. The strong contrast is removed after the material is heat treated at 1000 C to relieve the residual stresses around the indentations. A comparison of these observations with SEAM and reflected polarized light observations of Vickers indentations in soda-lime glass both before and after heat treatment confirms the interpretation of the strong contrast.

Cantrell, John H.↗

Impact behavior of a SiC fiber-reinforced reaction bonded Si3N4 composite

Impact tests were performed on a series of ceramic plate specimens. Monolithic (unreinforced) and composite specimens with various fiber layups were tested to determine the effect that the fiber reinforcement has on impact damage initiation and dynamic response of the ceramic materials. Results show that a porous surface layer of Si3N4 on the composite specimens can enhance the energy absorbing capability of the composite specimens. The addition of SiC fiber reinforcement to the RBSN matrix material is also shown to significantly change the mode of failure and reduce the extent of damage due to impact.

Grady, J.↗

Chemical vapor deposition for silicon cladding on advanced ceramics

Polycrystalline Si was used to clad several advanced ceramic materials such as SiC, Si3N4, sapphire Al2O3, pyrolytic BN, and Si by a CVD process. The thickness of Si cladding ranged from 0.025 to 3.0 mm. CVD Si adhered quite well to all the above materials except Al3O, where the Si cladding was highly stressed and cracked or delaminated. A detailed material characterization of Si-clad SiC samples showed that Si adherence to SiC does not depend much on the substrate surface preparation; that the thermal cycling and polishing of the samples do not cause delamination; and that, in four-point bend tests, the Si-SiC bond remains intact, with the failure occurring in the Si.

Goela, Jitendra S.↗

Study of novel concepts of power transmission gears

Two concepts in power transmission gear design are proposed which provide a potential for large noise reduction and for improving weight to payload ratio due to use of advanced fiber reinforced and ceramic materials. These concepts are briefly discussed. Since both concepts use ultrathin layered rubber-metal laminates for accommodating limited travel displacements, properties of the laminates, such as their compressive strength, compressive and shear moduli were studied. Extensive testing and computational analysis were performed on the first concept gears (laminate coated conformal gears). Design and testing of the second conceptual design (composite gear with separation of sliding and rolling motions) are specifically described.

Rivin, Eugene I.↗