Nonhazardous acid etches weld samples
Nonhazardous citric acid solution used with 24 volt dc power supply etches weld samples. This etching method is limited to 300 stainless steel and a small range of other high temperature alloys.
Allen, B. C↗
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Results for “sampling methods”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
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Investigation of lunar surface chemical contamination by LEM descent engine and associated equipment Final report
Lunar surface contamination from LEM rocket exhaust - methods of minimizing sample contamination
LUNAR EXCURSION MODULE /LEM/↗
Blood oxygen saturation determined by transmission spectrophotometry of hemolyzed blood samples
Use of the Lambert-Beer Transmission Law determines blood oxygen saturation of hemolyzed blood samples. This simplified method is based on the difference in optical absorption properties of hemoglobin and oxyhemoglobin.
Malik, W. M.↗
Experimental prediction of performance by superconducting cables
Broken superconductor method of short sample testing makes possible the prediction of the performance of well cooled, stabilized, superconducting cable coils. It yields a field-versus-current curve for a short sample of cable. Plots are given for the superconductor and copper currents at various magnetic field strengths.
Brooks, J. M.↗
Acceptance sampling for the normal distribution - Standard deviation unknown but assumed constant
Standard deviation estimates causing operating characteristic curves to be random variables in quality control acceptance sampling plans and methods for computing confidence limits
Sidik, S. M.↗
Digital-computer normal shock position and restart control of a Mach 2.5 axisymmetric mixed-compression inlet
Digital computer control of a mixed-compression inlet is discussed. The inlet was terminated with a choked orifice at the compressor face station to dynamically simulate a turbojet engine. Inlet diffuser exit airflow disturbances were used. A digital version of a previously tested analog control system was used for both normal shock and restart control. Digital computer algorithms were derived using z-transform and finite difference methods. Using a sample rate of 1000 samples per second, the digital normal shock and restart controls essentially duplicated the inlet analog computer control results. At a sample rate of 100 samples per second, the control system performed adequately but was less stable.
Neiner, G. H.↗
Infrared absorptivities of transition metals at room and liquid-helium temperatures.
Evaluation of experimental data concerning the normal spectral absorptivities of the transition metals, nickel, iron, platinum, and chromium, at both room and liquid-helium temperatures in the wavelength range from 2.5 to 50 microns. The absorptivities were derived from reflectivity measurements made relative to a room-temperature vapor-deposited gold reference mirror. The absorptivity of the gold reference mirror was measured calorimetrically, by use of infrared laser sources. Investigation of various methods of sample-surface preparation resulted in the choice of a vacuum-annealing process as the final stage. The experimental results are discussed on the basis of the anomalous-skin-effect theory modified for multiple conduction bands. As predicted, the results approach a single-band model toward the longer wavelengths. Agreement between theory and experiment is considerably improved by taking into account the modification of the relaxation time due to the photon-electron-phonon interaction proposed by Holstein (1954) and Gurzhi (1958); but, particularly at helium temperatures, the calculated curve is consistently below the experimental results.
Jones, M. C.↗
Electrical properties of dry rocks
The mechanism by which atmospheric moisture affects the conductivity and dielectric constant of rock specimens was studied in time and frequency domains. It is suggested that adsorbed water molecules alter the surface conductivity in a manner similar to that observed in semiconductors and insulators. Powdered basalts show a low-frequency dispersion produced by the atmospheric moisture remaining in the pore system of the sample in a high vacuum; this effect is attributed to isolated adsorption centers. Simulated lunar permafrost at 100 K and a vacuum of 10 to the -8th power torr together with data on lunar samples contaminated with atmospheric moisture and the dielectric properties of ice at various temperatures indicate that, if permafrost exists in the moon it should present a relaxation peak at approximately 300 Hz; for temperatures up to 263 K it may go up to 20 KHz. It is concluded that in order to have electrical steady state conditions in rock samples it is necessary to have volume charge accumulations at interfaces within the sample and at the electrode sample interface. A method for measuring heterogeneous dielectrics with non-negligible ohmic and dielectric conductivities is proposed and experimentally verified.
Morrison, H.↗
Comparison of inert-gas-fusion and modified Kjeldahl techniques for determination of nitrogen in niobium alloys
This report compares results obtained for the determination of nitrogen in a selected group of niobium-base alloys by the inert-gas-fusion and the Kjeldahl procedures. In the inert-gas-fusion procedure the sample is heated to approximately 2700 C in a helium atmosphere in a single-use graphite crucible. A platinum flux is used to facilitate melting of the sample. The Kjeldahl method consisted of a rapid decomposition with a mixture of hydrofluoric acid, phosphoric acid, and potassium chromate; distillation in the presence of sodium hydroxide; and highly sensitive spectrophotometry with nitroprusside-catalyzed indophenol. In the 30- to 80-ppm range, the relative standard deviation was 5 to 7 percent for the inert-gas-fusion procedure and 2 to 8 percent for the Kjeldahl procedure. The agreement of the nitrogen results obtained by the two techniques is considered satisfactory.
Merkle, E. J.↗
Hydrocarbons identified in extracts from estuarine water accommodated no. 2 fuel oil by gas chromatography-mass spectrometry
Results are presented on a computerized gas chromatograph-mass spectrometer analysis of methylene chloride and n-heptane extracts of a No. 2 fuel oil accommodated estuarine water sample. The analytical method is briefly described, and the limitations on the identifications are categorized. Some attempt was made to determine major and trace constituents in the water accommodate. Altogether 66 hydrocarbon compounds were identified specifically, and 75 compounds were partially identified. Seven compounds could be recognized as major constituents of the water accommodated oil and ten were present only as traces. The aromatic compounds found were alkyl benzenes, naphthalene, tetralin, indane, biphenyl, fluorene, anthracene, and some of their alkyl substituted isomers in the range of carbon numbers C7 to C15. Four n-alkanes, C10 to C13, were found along with four other assorted hydrocarbons.
Lewis, B. W.↗
Automated mass spectrometer/analysis system: A concept
System performs rapid multiple analyses of entire compound classes or individual compounds on small amounts of sample and reagent. Method will allow screening of large populations for metabolic disorders and establishment of effective-but-safe levels of therapeutic drugs in body fluids and tissues.
Boettger, H. G.↗
Uniform sampling analysis of a hybrid phase-locked loop with a sample-and-hold phase detector
Phase-locked-loop (PLL) bit synchronizers often employ integrate-and-dump type phase detectors that provide phase error information only at discrete points in time. Usually these phase detectors are followed by sample-and-hold circuits to produce a stairstep error voltage as the input to a standard analog circuit loop filter. When the loop is configured in this manner, it is referred to as a hybrid PLL. Sampled-data analysis methods (Z transforms) are used to determine the stability and transient response of this loop.
Barab, S.↗
Satellite information on Orlando, Florida
A land use map of Orange County, Florida was prepared from EREP photography while LANDSAT and EREP multispectral scanner data were used to provide more detailed information on Orlando and its suburbs. The generalized maps were prepared by tracing the patterns on an overlay, using an enlarging viewer. Digital analysis of the multispectral scanner data was basically the maximum likelihood classification method with training sample input and computer printer mapping of the results. Urban features delineated by the maps are discussed. It is concluded that computer classification, accompanied by human interpretation and manual simplification can produce land use maps which are useful on a regional, county, and city basis.
Hannah, J. W.↗
Hybrid methods are helpful
Multiple scattering problems in a plane layer often permit the convenient use of different methods joined together. Sample numerical results to illustrate this point refer to X- and Y-functions, asymptotic fitting, the small-loss approximations, polarization in high orders, and photon path distribution.
Vandehulst, H. C.↗
A gas filter correlation monitor for CO, CH4, and HCl
A fast response instrument for monitoring the atmospheric constituents CO, CH4, and HCl, using a modified nondispersive infrared technique, was designed, assembled, and tested. This gas filter correlation method uses a sample of gas to provide a selective filter for radiation absorbed in a gas mixture containing the specified gas. Depending on the spectral line broadening, temperature, and optical depth of the gas selected, exceptionally high spectral resolution may be attained. A description of the single beam rotating cell system and its specific application is presented along with the signal processing circuit. Calibrations of the instrument show that the technique can be used to measure CO, CH4, and HCl concentrations as small as 5 ppm-m. A field version was employed to measure diurnal variations of CO and CH4 and the interfering effects of other atmospheric gases were analyzed.
Sebacher, D. I.↗
Scientific investigations in the Gulf of Mexico and Caribbean Sea during the 1974-1975 Calypso cruise, parts 1 and 2
The distribution and concentrations of the standing crop of phytoplankton and nutrient salts in the Gulf of Mexico and the Caribbean Sea were investigated to provide ground truth for correlating temperature and chlorophyll-a measurements with observations from NASA U-2 aircraft equipped with specially designed sensors for measuring ocean color phenomena. The physical, chemical, and biological data obtained is summarized. Sampling procedures and methods used for determining plant pigments, species composition of phytoplankton, nutrient salt analysis, and the euphotic zones are described.
Elsayed, S. Z.↗
The earth radiation budget satellite system for climate research
The mission implications of providing earth radiation budget data for climate studies have been thoroughly studied. The results of these studies indicate the need for a multisensor, multisatellite system consisting of high and midinclination orbits. To meet this need, NASA and NOAA are planning a joint Earth Radiation Budget Satellite System (ERBSS) composed of instruments on two of NOAA's near-polar Sun-synchronous TIROS-N/NOAA A through G series of operational satellites and on an NASA midinclination satellite of the Applications Explorer Mission (AEM) type referred to as ERBS-A/AEM. This paper describes the scientific objectives of ERBSS, the associated data analysis methods, mission analysis (sampling), and instrument definition.
Woerner, C. V.↗
Reliability of nondestructive evaluation data
Program calculates probability of defects at selected confidence levels from nondestructive evaluation data. It provides alternate method of grouping sample data to obtain reasonable value for lower confidence limit with small sample size.
Couchman, J. C.↗