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At least 487 records · Page 27

All sources NASA NTRS DOE OSTI

DOE OSTI2023

Heterogeneous microstructural evolution during hydrodynamic penetration of a high-velocity copper microparticle impacting copper

Microparticle hydrodynamic penetration (HDP) may be associated with the erosion regime in cold spray processing and other high-velocity impact events. Here, in an experimental approach where we can individually launch particles and study the impact sites, we explore copper microparticles impacted on copper substrates at velocities above 900 m/s where HDP begins. We lift cross-sectional lamellae from the impact sites with a focused-ion beam for further microstructural characterization using electron backscatter diffraction and scanning transmission electron microscopy. Due to the gradients of strain, strain rate, and temperature associated with HDP, heterogeneous microstructures result. The structural evolution processes observed include deformation twinning and multiple dislocation-mediated grain recrystallization mechanisms—geometric dynamic recrystallization (gDRX), discontinuous DRX (dDRX), and meta DRX (mDRX). The higher strains at the interface lead to the most significant structural changes and complex mechanisms. In contrast, there is a gradient to more conventional dislocation plasticity away from the interface (on either the particle or substrate side). Here, these microstructural observations are consistent with the deformation map for copper and extend the observations of impact-induced recrystallization across new regimes of behavior.

Cold spray process↗

DOE OSTI2020

Open Source Visualization and Analysis Platform for 3D Reconstructions of Materials by Transmission Electron Microscopy

Three-dimensional characterization of materials at the nano- and meso-scale has become possible with transmission and scanning transmission electron microscopes (S/TEM). Its importance has extended to a wide class of nanomaterials such as hydrogen fuel cells, solar cells, industrial catalysts, new battery materials and semiconductor devices, as well as spanning high-tech industry, universities, and national labs. While capable instrumentation is abundant, this rapidly expanding demand for high-resolution tomography is bottlenecked by software that is instead tailored for lower-dose, biological applications and not optimized for higher-resolution materials applications. Existing tomography fails to utilize the chemical information provided by S/TEM spectrometers. To address this problem, this project delivered a scalable, fully functional, freely-distributable, open Source materials tomography package with a modern user interface that enables automated acquisition, alignment, and real-time reconstruction of raw tomography data, and provides advanced segmentation, three-dimensional chemical visualization and analysis optimized for materials applications. It has established an extendable framework capable of automation for high-throughput for the tomography of materials from data acquisition to visualization. Phase I and II delivered a full-featured, cross-platform, clean and integrated application for S/TEM materials tomography. It can read projection data from the microscope, with graphical tools for alignment of data, tomographic reconstruction, segmentation, and visualization of the reconstructed 3D volume. The entire pipeline can be saved to an XML state file, enabling fully reproducible data processing and analysis with a full Python environment for the development of custom algorithms, processing, and analysis requirements. Phase IIB extended the application to provide real-time tomographic reconstruction, "live updates" as data is processed, analysis of big data, and multi-channel tomography. Here, quantitative assessment of nanomaterials can occur as data is being recorded on a 3D visualization platform that accommodates additional information from multiple channels. We provide unmatched high-throughput tomography, where the complete tomographic pipeline from measurement to 3D visualization can occur rapidly. The project was extended to offer capabilities for micro-CT, X-ray, neutron, focused ion beam, atomic electron tomography and atom probe tomography. With over 600 transmission electron microscopes worldwide and approximately 50 coming online each year, the demand and impact of an open-source tomography tool is large. Significant opportunities exist in high-tech industry, universities, and national labs to enable or enhance three-dimensional imaging at the nanoscale and bring automated high-throughput approaches that will accelerate progress in materials characterization and metrology. The project supports a service based business model by enabling lab-specific acquisition and processing customization and integration-support and development that will be provided into Phase III and beyond.

36 MATERIALS SCIENCE↗

DOE OSTI2021

Cross Section Results from the MicroBooNE Experiment

The MicroBooNE detector is currently the largest operating liquid argon neutrino experiment in the world. Located at the Fermi National Accelerator Laboratory (Fermilab), MicroBooNE has been collecting both electron neutrino ($\nu _{e}$) and muon neutrino ($\nu _{\mu }$) interactions from both the Booster Neutrino Beam (BNB) and the Neutrino Main Injector (NuMI) since late 2015. During this time, MicroBooNE has measured a wide-variety of interaction topologies including $\nu _{\mu }$ charged current, $\nu _{e}$ charged current, resonant $\pi ^{0}$, and various high multiplicity interactions. To date, many of MicroBooNE’s measurements are either the first of their kind using liquid argon as a target material, or have the largest number of events collected using a liquid argon detector. All of these measurements combine to form a rich cross section programme, aiming to enhance understanding of GeV-range neutrino interaction on liquid argon for upcoming detectors such as SBND, ICARUS, and DUNE.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2026

Beam test results of the Intermediate Silicon Tracker for sPHENIX

The Intermediate Silicon Tracker (INTT), a two-layer barrel silicon strip tracker, is a key component of the tracking system for sPHENIX at the Relativistic Heavy Ion Collider (RHIC) at Brookhaven National Laboratory. The INTT is designed to enable the association of reconstructed tracks with individual RHIC bunch crossings. To evaluate the performance of preproduction INTT ladders and the readout chain, a beam test was conducted at the Research Center for Accelerator and Radioisotope Science, Tohoku University, Japan. This paper presents the performance of the INTT evaluated through studies of the signal-to-noise ratio, residual distribution, spatial resolution, hit-detection efficiency, and multiple track reconstruction.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2020

A design of resonant inelastic X-ray scattering (RIXS) spectrometer for spatial- and time-resolved spectroscopy

The optical design of a Hettrick–Underwood-style soft X-ray spectrometer with Wolter type 1 mirrors is presented. The spectrometer with a nominal length of 3.1 m can achieve a high resolving power (resolving power higher than 10000) in the soft X-ray regime when a small source beam (<3 µm in the grating dispersion direction) and small pixel detector (5 µm effective pixel size) are used. Adding Wolter mirrors to the spectrometer before its dispersive elements can realize the spatial imaging capability, which finds applications in the spectroscopic studies of spatially dependent electronic structures in tandem catalysts, heterostructures, etc . In the pump–probe experiments where the pump beam perturbs the materials followed by the time-delayed probe beam to reveal the transient evolution of electronic structures, the imaging capability of the Wolter mirrors can offer the pixel-equivalent femtosecond time delay between the pump and probe beams when their wavefronts are not collinear. In combination with some special sample handing systems, such as liquid jets and droplets, the imaging capability can also be used to study the time-dependent electronic structure of chemical transformation spanning multiple time domains from microseconds to nanoseconds. The proposed Wolter mirrors can also be adopted to the existing soft X-ray spectrometers that use the Hettrick–Underwood optical scheme, expanding their capabilities in materials research.

73 NUCLEAR PHYSICS AND RADIATION PHYSICS↗

DOE OSTI2023

Cavity and Cryomodule Developements for EIC

The EIC is a major new project under construction at BNL in partnership with JLab. It relies upon a number of new SRF cavities at 197 MHz, 394 MHz, 591 MHz and 1773 MHz to pre-bunch, accelerate, cool and crab the stored beams. R&D is focusing on the 591 MHz elliptical cavity and 197 MHz crab cavity first as these are the most challenging. Preliminary designs of these cavities are presented along with an R&D status report. To avoid developing multiple different cryostats a modular approach is adopted using a high degree of commonality of parts and systems. This approach may be easily adapted to other frequencies and applications.

Rimmer, R.A.↗

DOE OSTI2026

Measurement of gamma-induced reactions between 10 and 19 MeV on natural zinc with potential application to 67 Cu production

As part of a broader campaign to understand gamma-induced charged particle emission with multiple materials, the cross sections of the (γ, p), and (γ, α) reactions on a natural zinc target were measured. Here, these cross sections were measured experimentally using a kinematically-complete, event-by-event methodology, using monoenergetic gamma ray beams from the High Intensity Gamma Source (HIγS) facility, ranging from 10 to 19 MeV, to bombard a natural metallic zinc target in vacuum. The measured cross sections are compared with theoretical predictions using the statistical model approach, which is important for the use of such models in real-world applications such as the production of the 67 Cu theranostic via the 68 Zn(γ, p) reaction.

Gamma-induced reactions↗

DOE OSTI2025

Single-Objective Airy Light-Sheet Imaging

Despite its massive potential, standard light-sheet imaging (LSI) faces key challenges, such as the incompatibility with common sample mounting techniques and low-resolution imaging. Single-objective LSI attempts to address these issues but often suffers from limited fields-of-view and throughput rates, or requires multiple optics that increase costs, alignment complexity, and losses. To overcome these challenges of standard single-objective LSI, we introduce single-objective Airy light-sheet imaging (SoALSI). SoALSI leverages the extraordinary self-acceleration properties of the Airy beam, achieving 5× higher imaging rates and enhanced imaging efficiency than standard single-objective LSI. Here, we demonstrate SoALSI’s versatility through rigorous contrast and resolution characterizations and by high-resolution imaging of diverse biological specimens, including malaria parasite-infected red blood cells and plant root tissue. SoALSI seamlessly integrates with any standard inverted microscope frame, enabling broader accessibility for the bioimaging community to explore biological processes in a wide range of specimens with enhanced resolution and imaging contrast.

airy beam↗

DOE OSTI2022

A new μ -high energy resolution fluorescence detection microprobe imaging spectrometer at the Stanford Synchrotron Radiation Lightsource beamline 6-2

In this report we describe a new synchrotron X-ray Fluorescence (XRF) imaging instrument with an integrated High Energy Fluorescence Detection X-ray Absorption Spectroscopy (HERFD-XAS) spectrometer at the Stanford Synchrotron Radiation Lightsource at beamline 6-2. The X-ray beam size on the sample can be defined via a range of pinhole apertures or focusing optics. XRF imaging is performed using a continuous rapid scan system with sample stages covering a travel range of 250 × 200 mm 2 , allowing for multiple samples and/or large samples to be mounted. The HERFD spectrometer is a Johann-type with seven spherically bent 100 mm diameter crystals arranged on intersecting Rowland circles of 1 m diameter with a total solid angle of about 0.44% of 4π sr. A wide range of emission lines can be studied with the available Bragg angle range of ~64.5°–82.6°. With this instrument, elements in a sample can be rapidly mapped via XRF and then selected features targeted for HERFD-XAS analysis. Furthermore, utilizing the higher spectral resolution of HERFD for XRF imaging provides better separation of interfering emission lines, and it can be used to select a much narrower emission bandwidth, resulting in increased image contrast for imaging specific element species, i.e., sparse excitation energy XAS imaging. This combination of features and characteristics provides a highly adaptable and valuable tool in the study of a wide range of materials.

47 OTHER INSTRUMENTATION↗

DOE OSTI2024

Longer-lived mediators from charged mesons and photons at neutrino experiments

Since many of the dark-sector particles interact with Standard Model (SM) particles in multiple ways, they can appear in experimental facilities where SM particles appear in abundance. In this study, we explore a particular class of longer-lived mediators that are dominantly produced from photons and charged mesons that arise in proton-beam fixed-target-type neutrino experiments. This class of mediators encompasses light scalars that appear in theories like extended Higgs sectors, muon(electro)philic scalars, etc. We evaluate the sensitivities of these mediators at beam-based neutrino experiments such as the finished ArgoNeuT, ongoing MicroBooNE, SBND, ICARUS, and the upcoming DUNE experiment. We find that muonphilic scalars are more enhanced while produced from three-body decay of charged mesons. The above-mentioned experiments can probe unexplored regions of parameter space that can explain the current discrepancy in the anomalous magnetic moment of muons. We further find that Compton-like scattering of photons is the largest source of electrophilic scalars. By utilizing this, the DUNE Near Detector can explore new regions in the sensitivity space of electrophilic scalars. We also show that Bethe-Heitler scattering processes can be used to probe flavor-specific lepton final states even for the mediator masses below twice the lepton mass. Published by the American Physical Society 2024

Astronomy & Astrophysics↗

DOE OSTI2024

Fermilab Booster Beam Emittances from Quadrupole Modes Measured BPMs

The measurement of beam emittances by extracting the quadrupole mode signal from a 4 plate beam position monitor (BPM) was published at least 40 years ago. Unfortunately, in practice, this method suffers from poor signal to noise ratio and requires a lot of tuning to extract out the emittances. In this paper, an improved method where multiple BPMs are used together with better mathematical analysis is described. The BPM derived emittances are then compared with those measured by the Ion Profile Monitor (IPM). Surprisingly, the BPM measured emittances behave very well and are more realistic than those measured by the IPM.

43 PARTICLE ACCELERATORS↗

DOE OSTI2025

New Measurement of Electron Neutrino Interactions on Argon in MicroBooNE

MicroBooNE, located at the Fermi National Accelerator Laboratory, is an 85-tonne liquid argon time-projection chamber designed to study neutrinos from the Booster Neutrino Beam and Neutrinos at the Main Injector (NuMI) beam. Understanding neutrino-nucleon interactions is essential for improving the accuracy of neutrino event generators, which are critical for modelling neutrino behaviour and interpreting data from oscillation experiments. The NuMI beam's high electron neutrino flux relative to its muon neutrino flux makes it particularly suited to probe these interactions. This poster presents new single-differential cross-section measurements of charged-current electron-neutrino interactions on argon with protons and no pions in the final state. These results use data from NuMI beam operations in both neutrino and antineutrino modes. Cross sections are reported as functions of key kinematic observables, including electron energy, total visible energy, and the opening angle between the electron and leading proton. Interaction rates as a function of proton multiplicity are also shown. These results are compared to theoretical predictions generated by widely used neutrino event generators.

Barnard, Abbey G. [Oxford U.] (ORCID:0000000161171↗

DOE OSTI2024

Fermilab Booster Beam Emittances from Quadrupole Modes Measured by BPMs

43 PARTICLE ACCELERATORS↗

DOE OSTI2023

Spectroscopy of Mesons Produced by Linearly Polarized Photons

A formalism for the experimental analysis of mesons produced by a beam of linearly polarized photons is presented. This formalism introduces a more general use of the reflectivity operator. The goal is to recognize resonances in cross-sections, their associated quantum numbers, and production mechanisms by performing partial wave analysis of multiple-meson final states.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

DOE OSTI2023

Three-dimensional broadband nonlinear phased array imaging

System include an ultrasonic transducer configured to couple to a nondestructive testing (NDT) sample and configured to produce and direct an ultrasonic probe wave at a selected frequency into a subsurface region of the NDT sample, a 3D laser scanning vibrometer configured to direct a detection beam in a scan area on a surface of the NDT sample and to receive a return beam from the scan area, and to detect, based on the return beam, a 3D motion of the surface across a wideband frequency range, and a processor, and a memory configured with instructions that, when executed by the processor, cause the processor to produce sub-surface image data of the NDT sample at multiple harmonics of the selected frequency in the wideband frequency range based on the detected 3D surface motion, wherein the sub-surface image data describes a nonlinear defect response produced in the NDT sample by interaction of the ultrasonic probe wave with the subsurface region.

Remillieux, Marcel↗

DOE OSTI2022

Custom-designed heat treatment simultaneously resolves multiple challenges facing 3D-printed single-crystal superalloys

Single-crystal Ni-based superalloys are currently the material of choice for turbine blade applications, especially with the emerging additive manufacturing (AM) that facilitates the manufacture/repair of these single crystals. This promising AM route, however, comes with a dilemma: in the fusion and heat affected zones after e-beam or laser induced melting, one needs a solutionizing annealing to relieve the residual stresses and homogenize the chemical/microstructure. The super-solvus solutionizing temperature is usually adopted from the protocol for the cast superalloys, which almost always causes recrystallization and stray grain growth, resulting in a polycrystalline microstructure and degrading the high-temperature mechanical performance. Here, in this paper, we demonstrate a custom-designed post-printing heat treatment to replace the conventional super-solvus one. The recovery and relatively low temperature diminish the driving force for recrystallization and the movement of stray grain boundaries, without suffocating the chemical/microstructural homogenization thanks to the narrow dendrite width and short element segregation distance. The optimal duration of the heat treatment is proposed to achieve atomic-diffusion mediated chemical homogenization while limiting γ'-particle coarsening in the interdendritic regions. Our strategy makes it practically feasible to resolve several bottleneck problems with one processing/treatment, removing a seemingly formidable obstacle to effective additive manufacturing of superalloy single crystal products.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Multiplicity and pseudo-rapidity density distributions of charged particles produced in pp, pA and AA collisions at RHIC & LHC energies

Multiplicity and pseudorapidity (η) density (d N ch /dη) distributions of charged hadrons provide key information towards understanding the particle production mechanisms and initial conditions of high-energy heavy-ion collisions. However, detector constraints limit the η-range across which charged particle measurements can be carried out. Extrapolating the measured distributions to large η-range by parameterizing measured distributions and by using calculations from event generators, we characterize the production of charged particles over the full kinematic range. In the present study, we use three different ansätze to obtain quantitative descriptions of the shape of pseudorapidity distributions of charged hadrons produced in pp, p–A, and A–A collisions for beam energies ( s NN ) ranging from a few GeV to a few TeV corresponding to RHIC and LHC energies. We study the limiting fragmentation behavior in these collisions and report evidence for participant-scaling violations in high-energy collisions at the TeV scale. We additionally examine measured pseudorapidity distributions to constrain models describing initial conditions of particle production. We predict the centrality dependence of charged particle multiplicity distributions at FAIR and NICA energies and give an estimation of charged particle multiplicity at η = 0 for the proposed HE-LHC and FCC energies.

Physics↗

DOE OSTI2020

Imaging Polarity in Two Dimensional Materials by Breaking Friedel's Law

Friedel's law guarantees an inversion-symmetric diffraction pattern for thin, light materials where a kinematic approximation or a single-scattering model holds. Typically, breaking Friedel symmetry is ascribed to multiple scattering events within thick, non-centrosymmetric crystals. However, two-dimensional (2D) materials such as a single monolayer of MoS 2 can also violate Friedel's law, with unexpected contrast between conjugate Bragg peaks. Here, we show analytically that retaining higher order terms in the power series expansion of the scattered wavefunction can describe the anomalous contrast between hkl and $\bar{hkl}$ peaks that occurs in 2D crystals with broken in-plane inversion symmetry. These higher-order terms describe multiple scattering paths starting from the same atom in an atomically thin material. Furthermore, 2D materials containing heavy elements, such as WS 2 , always act as strong phase objects, violating Friedel's law no matter how high the energy of the incident electron beam. Experimentally, this understanding can enhance diffraction-based techniques to provide rapid imaging of polarity, twin domains, in-plane rotations, or other polar textures in 2D materials.

2D materials↗