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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 487 records · Page 27

Miniature triaxial metastable ionization detector for gas chromatographic trace analysis of extraterrestrial volatiles

The present investigation is concerned with a miniature metastable ionization detector featuring an unconventional electrode configuration, whose performance characteristics parallel those of traditional design. The ionization detector is to be incorporated in a flight gas chromatograph (GC) for use in the Space Shuttle. The design of the detector is discussed, taking into account studies which verified the sensitivity of the detector. The triaxial design of the detector is compared with a flat-plate style. The obtained results show that the principal goal of developing a miniature, highly sensitive ionization detector for flight applications was achieved. Improved fabrication techniques will utilize glass-to-metal seals and brazing procedures.

Woeller, F. H.↗

Hermetic Edge Seals for Photovoltaic Modules

Corrosive atmospheric agents excluded to prolong cell life. Combination of two sealing techniques makes possible to protect solar cells from water vapor, oxygen, and other corrosive atmospheric constituents. Using three-step process, glass-to-metal hermetic seal formed around edge of solar-cell module. Elastomer seals used previously not as effective because they are permeable to water vapor and atmospheric gases.

Nowlan, M. J.↗

Convection in a Solidifying Binary Mixture

Temperature and concentration profiles calculated. Study expands on earlier work including more realistic, mathematically complicating physical effects and yet retains simple geometry and enough simplifying assumptions to make equations solvable. Leads to improved understanding of metal and glass production, material processing in low low gravity other important material processing problems.

Antar, B.↗

Performance of the high speed anechoic wind tunnel at Lyon University

The characteristics of the feed duct, the wind tunnel, and the experiments run in the convergent-divergent anechoic wind tunnel at Lyon University are described. The wind tunnel was designed to eliminate noise from the entrance of air or from flow interactions with the tunnel walls so that noise caused by the flow-test structure interactions can be studied. The channel contains 1 x 1 x 0.2 m glass and metal foil baffles spaced 0.2 m apart. The flow is forced by a 350 kW fan in the primary circuit, and a 110 kW blower in the secondary circuit. The primary circuit features a factor of four throat reductions, followed by a 1.6 reduction before the test section. Upstream and downstream sensors permit monitoring of the anechoic effectiveness of the channel. Other sensors allow modeling of the flow structures in the tunnel. The tunnel was used to examine turbulent boundary layers in flows up to 140 m/sec, tubulence-excited vibrations in walls, and the effects of laminar and turbulent flows on the appearance and locations of noise sources.

Sunyach, M.↗

Mechanized Polishing of Optical Rod and Fiber Ends

Workpiece holder for standard grinding and polishing machine makes it easier to produce optical finish and shape on end of metal or glass rod or bundle of optical fibers. Previously, glass parts lapped and polished manually, time-consuming procedure calling for considerable skill.

Gum, J. S.↗

Attaching Copper Wires to Magnetic-Reed-Switch Leads

Bonding method reliably joins copper wires to short iron-alloy leads from glass-encased dry magnetic-reed switch without disturbing integrity of glass-to-metal seal. Joint resistant to high temperatures and has low electrical resistance.

Kamila, Rudolf↗

Chemical bonding technology

Primers employed in bonding together the various material interfaces in a photovoltaic module are being developed. The approach develops interfacial adhesion by generating actual chemical bonds between the various materials bonded together. The current status of the program is described along with the progress toward developing two general purpose primers for ethylene vinyl acetate (EVA), one for glass and metals, and another for plastic films.

Plueddemann, E.↗

Review on drop towers and long drop tubes

A drop tube is an enclosure in which a molten sample can be solidified while falling; three such large tubes are currently in existence, all at NASA research facilities, and are engaged in combustion and fluid physics-related experiments rather than in materials research. JPL possesses smaller tubes, one of which can be cryogenically cooled to produce glass and metal microshells. A new small drop tube will soon begin operating at NASA Lewis that is equipped with four high-speed two-color pyrometers spaced equidistantly along the column.

Bayuzick, R. J.↗

Infrared Pyrometry From Room Temperature To 700 Degrees C

Consistent readings obtained when specimens prepared appropriately. New method largely overcomes limitations. Transmission of infrared increased by replacing customary metal-coated glass viewing port with quartz viewing port covered with tantalum mesh. Commercially available infrared microscope with focal distance of 53 cm focuses on spot only 1 mm wide on specimen. Microscope operated as radiometer. Output of detector varies by several orders of magnitude, processed by logarithmic amplifier before reading.

Wheeler, Donald R.↗

Surface temperature determination in surface analytic systems by infrared optical pyrometry

An IR pyrometric technique for measuring the surface temperatures of metal specimens in an ultrahigh-vacuum analytic chamber is described and demonstrated. The experimental setup comprises a commercial IR microscope with a long-working-distance right-angle objective (focal spot diameter 1 mm at 53 cm), a metal-coated glass vacuum chamber with a Ta-mesh-covered quartz viewport, an Mo specimen stub with an internal heating element, and a Ta disk test specimen with a flat side coated with a high-emissivity graphite film. The results of an initial calibration test are presented graphically and briefly characterized. The measurement error at 450 C is found to be less than 10 C.

Wheeler, Donald R.↗

Fourier transform infrared (FTIR) fiber optic monitoring of composites during cure in an autoclave

Real-time in situ monitoring of the chemical states of epoxy resins was investigated during cure in an autoclave using infrared evanescent spectroscopy. Fiber evanescent sensors were developed which may be sandwiched between the plies of the prepreg sample. A short length of sapphire fiber was used as the sensor cell portion of the fiber probe. Heavy metal fluoride glass optical fiber cables were designed for connecting the FTIR spectrometer to the sensor fiber within the autoclave. The sapphire fibers have outstanding mechanical thermal properties which should permit their use as an embedded link in all thermoset composites. The system is capable of operation at a temperature of 250 C for periods up to 8 hours without major changes to the fiber transmission. A discussion of the selection of suitable sensor fibers, the construction of a fiber-optic interface, and the interpretation of in situ infrared spectra of the curing process is presented.

Druy, Mark A.↗

Lighted, Folding Inspection Mirror

Compact, inexpensive tool used in place of expensive borescopes. Shortens inspection/photographing process. Includes two small metal or glass mirrors hinged together. Two 3-V light bulbs attached along edges of one mirror and connected to battery of two cells. Inserted into narrow opening of clevis or tand, and surface viewed and photographed in opposite mirror. Useful in assembly of segments of solid rocket motors as well as in postflight assessment, engineering evaluation, and refurbishment. Also applied in general to inspection and photographing of inner sealing surfaces to which access difficult.

Roepe, Brian E.↗

Composite materials for space applications

The objectives of the program were to: generate mechanical, thermal, and physical property test data for as-fabricated advanced materials; design and fabricate an accelerated thermal cycling chamber; and determine the effect of thermal cycling on thermomechanical properties and dimensional stability of composites. In the current program, extensive mechanical and thermophysical property tests of various organic matrix, metal matrix, glass matrix, and carbon-carbon composites were conducted, and a reliable database was constructed for spacecraft material selection. Material property results for the majority of the as-fabricated composites were consistent with the predicted values, providing a measure of consolidation integrity attained during fabrication. To determine the effect of thermal cycling on mechanical properties, microcracking, and thermal expansion behavior, approximately 500 composite specimens were exposed to 10,000 cycles between -150 and +150 F. These specimens were placed in a large (18 cu ft work space) thermal cycling chamber that was specially designed and fabricated to simulate one year low earth orbital (LEO) thermal cycling in 20 days. With this rate of thermal cycling, this is the largest thermal cycling unit in the country. Material property measurements of the thermal cycled organic matrix composite laminate specimens exhibited less than 24 percent decrease in strength, whereas, the remaining materials exhibited less than 8 percent decrease in strength. The thermal expansion response of each of the thermal cycled specimens revealed significant reduction in hysteresis and residual strain, and the average CTE values were close to the predicted values.

Rawal, Suraj P.↗

Chemical stability of high-temperature superconductors

A review of the available studies on the chemical stability of the high temperature superconductors (HTS) in various environments was made. The La(1.8)Ba(0.2)CuO4 HTS is unstable in the presence of H2O, CO2, and CO. The YBa2Cu3O(7-x) superconductor is highly susceptible to degradation in different environments, especially water. The La(2-x)Ba(x)CuO4 and Bi-Sr-Ca-Cu-O HTS are relatively less reactive than the YBa2Cu3O(7-x). Processing of YBa2Cu3O(7-x) HTS in purified oxygen, rather than in air, using high purity noncarbon containing starting materials is recommended. Exposure of this HTS to the ambient atmosphere should also be avoided at all stages during processing and storage. Devices and components made out of these oxide superconductors would have to be protected with an impermeable coating of a polymer, glass, or metal to avoid deterioration during use.

Bansal, Narottam P.↗

Micrometeoroids and debris on LDEF

Part of the LDEF tray allocated to French Experiments (FRECOPA) was devoted to the study of dust particles. The tray was located on the face of LDEF directly opposed to the velocity vector. Two passive experiments were flown: a set of glass and metallic samples; and multilayer thin foil detectors. Crater size distribution made possible the evaluation of the incident microparticle flux in the near environment. Comparisons are made with measurements obtained on the other faces of LDEF and with results from similar experiments on the MIR. Of interest was the study of impact features on stacked thin foil detectors. The top foil acted as a shield, fragmenting the projectiles and spreading the fragments over the surface of the thick plate located underneath. EDS analysis has provided evidence of impactor fragments. Detectors consisting of a thin shield and thick bottom plate appear to offer a significantly higher return of data concerning chemical analysis of impactor residues than single plate detectors. The samples of various materials offer a unique opportunity for the study of the many processes involved upon hypervelocity impact phenomena.

Mandeville, Jean-Claude↗

Degradation of electro-optic components aboard LDEF

Re-measurement of the properties of a set of electro-optic components exposed to the low earth orbital environment aboard the Long Duration Exposure Facility (LDEF) indicates that most components survived quite well. Typical components showed some effects related to the space environment unless well protected. The effects were often small but significant. Results for semiconductor infrared detectors, lasers, LED's, filter, mirrors, and black paints will be presented. Semiconductor detectors and emitters were scarred but reproduced their original characteristics. Spectral characteristics of multi-layer dielectric filters and mirrors were found to be altered and degraded. Increased absorption in black paints indicates an increase in absorption sites, giving rise to enhanced performance as coatings for baffles and sunscreens. We find plastics and multi-layer dielectric coatings to be potentially unstable. Semiconductor devices, metal, and glass are more likely to be stable.

Blue, M. D.↗

Space Station Furnace Facility - A multipurpose, high temperature microgravity research facility

This paper describes the Space Station Furnace Facility (SSFF) program. The SSFF is a new development intended to provide an advanced facility for materials research in the microgravity environment of the Space Station. The SSFF will be designed for research in metals, oxides, glasses, and alloy solidification and crystal growth of electronic and electrooptical materials. The facility will be designed to process multiple samples in one or more furnaces in an automated mode. The SSFF will be built around a general facility core which will provide common support functions not provided by the Space Station, subsystems which could best be centralized, and common subsystems which could be distributed with each experiment module. The SSFF will be capable of operation in both the manned and unmanned mode and is scheduled for early deployment aboard the Space Station.

Kirkindall, Arthur S.↗

Space environmental effects on LDEF low Earth orbit exposed graphite reinforced polymer matrix composites

The Long Duration Exposure Facility (LDEF) was deployed on April 7, 1984 in low earth orbit (LEO) at an altitude of 482 kilometers. On board experiments experienced the harsh LEO environment including atomic oxygen (AO), ultraviolet radiation (UV), and thermal cycling. During the 5.8 year mission, the LDEF orbit decayed to 340 kilometers where significantly higher AO concentrations exist. LDEF was retrieved on January 12, 1990 from this orbit. One experiment on board LDEF was M0003, Space Effects on Spacecraft Materials. As a subset of M0003 nearly 500 samples of polymer, metal, and glass matrix composites were flown as the Advanced Composites Experiment M0003-10. The Advanced Composites Experiment is a joint effort between government and industry with the Aerospace Corporation serving as the experiment integrator. A portion of the graphite reinforced polymer matrix composites were furnished by the Boeing Defense and Space Group, Seattle, Washington. Test results and discussions for the Boeing portion of M0003-10 are presented. Experiment and specimen location on the LDEF are presented along with a quantitative summary of the pertinent exposure conditions. Matrix materials selected for the test were epoxy, polysulfone, and polyimide. These composite materials were selected due to their suitability for high performance structural capability in spacecraft applications. Graphite reinforced polymer matrix composites offer higher strength to weight ratios along with excellent dimensional stability. The Boeing space exposed and corresponding ground control composite specimens were subjected to post flight mechanical, chemical, and physical testing in order to determine any changes in critical properties and performance characteristics. Among the more significant findings are the erosive effect of atomic oxygen on leading edge exposed specimens and microcracking in non-unidirectionally reinforced flight specimens.

George, Pete↗